EP0560878B1 - Verfahren zur herstellung von isolierenden, aus untereinander verbundenen stabförmigen mineralfaserelementen bestehenden platten - Google Patents

Verfahren zur herstellung von isolierenden, aus untereinander verbundenen stabförmigen mineralfaserelementen bestehenden platten Download PDF

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Publication number
EP0560878B1
EP0560878B1 EP92901216A EP92901216A EP0560878B1 EP 0560878 B1 EP0560878 B1 EP 0560878B1 EP 92901216 A EP92901216 A EP 92901216A EP 92901216 A EP92901216 A EP 92901216A EP 0560878 B1 EP0560878 B1 EP 0560878B1
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EP
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Prior art keywords
lamellae
web
fibres
fibre
fibre web
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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EP92901216A
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English (en)
French (fr)
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EP0560878A1 (de
Inventor
Bent Jacobsen
Luis Jorgen Norgaard
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Rockwool AS
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Rockwool International AS
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Classifications

    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
    • D04H1/72—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
    • D04H1/732—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by fluid current, e.g. air-lay
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4209—Inorganic fibres
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4209—Inorganic fibres
    • D04H1/4218—Glass fibres
    • D04H1/4226—Glass fibres characterised by the apparatus for manufacturing the glass fleece
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/58—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives
    • D04H1/64—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives the bonding agent being applied in wet state, e.g. chemical agents in dispersions or solutions
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
    • D04H1/74—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being orientated, e.g. in parallel (anisotropic fleeces)
    • E—FIXED CONSTRUCTIONS
    • E04—BUILDING
    • E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
    • E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
    • E04B1/62—Insulation or other protection; Elements or use of specified material therefor
    • E04B1/74—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
    • E04B1/76—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only
    • E04B2001/7683—Fibrous blankets or panels characterised by the orientation of the fibres

Definitions

  • This invention relates to a method of manufacturing insulating boards composed of interconnected rod-shaped mineral fibre elements (in the following referred to as lamellae) comprising converting a melt of a mineral fibre forming starting material into fibres, supplying a binder to said fibres, collecting the fibres on a conveyor belt so as to form a primary fibre web.
  • rod-shaped mineral fibre elements in the following referred to as lamellae
  • a method of the type defined above is disclosed in DE patent publication No. 2307577 C3.
  • the melt is converted into fine mineral fibres by being thrown out from one or more rapidly rotating spinning wheels under the simultaneous supply of a binder capable of being cured, and the fibres thus formed are caught on an endless belt in the form of a fibre web wherein the fibres predominantly are oriented parallel to the surface of the web.
  • the fibre web is cut longitudinally into lamellae and the lamellae thus formed are turned 90° about their longitudinal axis whereafter the lamellae thus oriented are bonded together to form a web-like product which is then cut into desired lengths to form board elements.
  • CA-A-1209893 discloses a method of producing a fibrous material product made from a laminar mat of glass fibres containing a bonding substance and having fibre lamination extending parallel to the surface of the mat, said method comprising the steps of a) crimping the mat in the longitudinal direction so as to dispose a major portion of said laminations in directions extending across the thickness of the mat, b) heat-curing the bonding substance, c) cutting the mat in the longitudinal direction to farm mat strips, d) rotating the strips 90° and e) securing adjacent strips to each other to form a board.
  • each lamella When such a web is cut longitudinally into lamellae and the lamellae are turned 90° and bonded together to form a lamella board, each lamella will exhibit a folded layer structure, the folds extending perpendicularly to the main surfaces of the lamella board and thereby imparting a greater stiffness and strength (area strength) to the lamella board than in the case where a lamella board is composed of rectilinear layers.
  • Boards produced by the prior art methods described above are suitable for many applications, but for certain applications, e.g. exterior insulation of roofs and/or building fronts and insulation of floors, the boards possess an insufficient stiffness or strength and/or insulating property.
  • the invention is based on the discovery that a board, wherein both the foldings formed by a longitudinal compression of the web to be cut to form lamellae and the individual fibres are positioned perpendicularly to the plane of the board, has superior stiffness and strength over a board, wherein only foldings extend perpendicularly to the surface of the board, whereas the fibres are positioned with arbitrary orientation in a plane perpendicular to the surface of the board.
  • a board having such a construction may be provided by using lamellae made from a secondary fibre web formed by transverse doubling of a primary web having a fibre orientation parallel to the surface of the web and predominantly in the longitudinal direction of the web.
  • the method of the invention has provided a possibility of producing a lamella board having a greatly increased stiffness and area strength compared to lamellae boards made from primary fibre webs, wherein the fibres are positioned with arbitrary orientation in a plane parallel to the plane of the web.
  • a particularly high stiffness is obtained with boards made from lamellae obtained by cutting a secondary web longitudinally and subsequently turning them 90° about their longitudinal axis because the fibres being predominantly oriented transversely to the secondary web will be positioned perpendicularly to the plane of the board.
  • a fibre web can be produced by initially producing a relatively thin primary web and subsequently doubling the primary web to form a secondary relatively thick fibre web comprising partially overlapping layers of the primary web, see DE patent publication No. 3501897.
  • the fibres are collected on a high-velocity conveyor belt, e.g. running with a velocity of 130 m/min, in the form of a thin fibre layer, e.g. having a weight of 0.3 kg/m2.
  • a high-velocity conveyor belt e.g. running with a velocity of 130 m/min
  • the fibres will be deposited on the conveyor belt in directions parallel to the surface of the web and predominantly parallel to the direction of movement of the belt.
  • the fibre web will obtain a tensile strenght which is about twice as high in the longitudinal direction of the fibre web as in the transverse direction.
  • the secondary fibre web is formed by laying by means of pendulum belts the thin primary web in a number of layers, e.g. 20, transversely to the longitudinal direction of the secondary web, the number of layers being determined by the desired area weight of the secondary web.
  • the fibres are predominantly oriented transversely to the web when the layers of the primary web extend transversely to the secondary web.
  • the purpose of doubling a fibre web is ordinarily to obtain a secondary web having a relatively great thickness and having a small variation in density in the longitudinal direction.
  • lamellae made from a doubled fibre web comprising from 4 to 25 layers and having a surface weight of from 1 to 8 kg/m2 are preferably used.
  • the longitudinal compression may also be effected when the web has been cut into lamellae.
  • lamellae made from fibre webs which have been compressed longitudinally in a ratio of from 1.5:1 to 4:1 are preferred.
  • the longitudinal compression should be effected following the vortical compression and when using a heat curable binder, the said longitudinal compression is effected before the fibre web is introduced into a curing oven.
  • Methods for subjecting a fibre web to a surface compression are also well known.
  • the fibre web to be compressed is introduced into the space between the rollers in a series of roller sets, the spacing between the rollers in the roller sets decreasing in the direction of movement of the fibre web.
  • lamellae made from a fibre web which has been surface compressed in a ratio of from 3:1 to 6:1 are preferred.
  • the cutting of the fibre web to form lamellae is preferably effected by means of saws which may have the form of compass saws, cf. DE patent publication No. 2307577, or circular saws, cf. SE published patent application No. 441764 and DE patent publication No. 2032624.
  • the rod-shaped fibre elements are cut into desired lengths before being turned 90° and combined into lamella boards.
  • Such turning may e.g. be effected in connection with the transfer of the cut lamellae from one conveyor belt upon which they are advanced in the longitudinal direction of the lamellae onto another conveyor belt moving perpendicularly to the first belt and upon which the lamellae are conveyed in a direction perpendicularly to their longitudinal direction.
  • This embodiment is advantageous in that the apparatus used for such turning of the lamellae requires little space.
  • the turning of the lamellae can be effected during the cutting of the web into lamellae, e.g. as described in DE patent publication No. 2307577 or DE 2032624.
  • the properly oriented lamellae which are to form a lamella board can be bonded together, preferably by means of a binder which is applied to the upper side of the fibre web and optionally to the lower side thereof, and preferably before the web is cut into lamellae.
  • the binders can be cured in one step by conveying the properly oriented and combined lamellae through a curing oven in which they are heated to curing temperature, which is preferably between 210 and 260°C when phenol formaldehyd resin is used as a binder.
  • the binder for bonding together the lamellae may also be supplied after the fibre web/lamellae have been heated in a curing oven to cure the binder supplied to the fibres in connection with their formation.
  • FIG. 1 designates an oven for manufacturing a mineral fibre forming melt which is supplied to a spinner 3 having four rapidly rotating spinning wheels 4 via a melt outlet 2. Simultaneously with the introduction of melt onto the outer surfaces of the spinning wheels and binder is sprayed, a strong gas stream is passed across the surfaces of the spinning wheels in the axial direction, thereby causing the formation of fibres 5 which are collected on an endless perforated conveyor belt 6 which is supported by three rollers 7, one of which is driven by driving means (not shown). As a result thereof a fibre web 8 (the primary web) is formed and this web is introduced into the space between two pendulum belts 10 and 11 by means of a further endless conveyor belt 9. The lower ends of the pendulum belts are located pivotally in a direction perpendicularly to the direction of movement of a further endless conveyor belt 12 which is supported by two rollers 13, one of which is driven by driving means (not shown).
  • the amplitude of the oscillation of the lower part of the pendulum belts 10 and 11 corresponds to the width of the conveyor belt 12 and a doubled fibre web 14 of partially overlapping fibre layers 8 is thus formed on the belt 12.
  • the fibre web 14 is subsequently introduced into a surface compression section consisting of three sets of co-operating rollers 15, 16 and 17, the spacing between the rollers in the roller sets decreasing in the longitudinal direction of the fibre web. Subsequently the fibre web 14 is introduced into the longitudinal compression section which also consists of three roller sets 18, 19 and 20, the rollers of the latter sets of rollers rotating with the same velocity, which velocity is lower than that of the sets of rollers 15, 16 and 17.
  • the fibre web which has been compressed longitudinally is then introduced into a curing oven 21 in which it is heated to a temperature which is sufficiently high to cure the binder and to fix the fibres relatively to one another.
  • the heat treated fibre web 14 is cut in the longitudinal direction by means of saws 22 so as to form lamellae 23 which are subsequently cut transversely by means of a transverse saw 24.
  • the lamellae 23 thus cut are then turned 90° and combined to form a board element 25 on a conveyor belt 26 and at the same time a binder is applied to the contact surfaces by means of an application apparatus (not shown) to bond together the lamellae 23.
  • the fibre layers formed from the primary web 8 extend substantially perpendicularly to the surface of the finished board element, and as they are also folded they are highly resistant against compression.
  • the lamellae can be joined together by means of e.g. strips, strings, non-woven fabric or paper on one side or both sides of the boards.

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Nonwoven Fabrics (AREA)
  • Laminated Bodies (AREA)
  • Thermal Insulation (AREA)
  • Insulating Bodies (AREA)
  • Ladders (AREA)
  • Ultra Sonic Daignosis Equipment (AREA)
  • Porous Artificial Stone Or Porous Ceramic Products (AREA)

Claims (5)

  1. Verfahren zur Herstellung von aus miteinander verbundenen, stabförmigen Mineralfaserelementen zusammengesetzten Isoliertafelelementen, umfassend Umwandeln einer Schmelze eines Mineralfasern bildenden Ausgangsmaterials zu Fasern, Zuführen eines Bindemittels zu den Fasern, Sammeln der Fasern auf einem Förderband zur Bildung einer primären Fasermatte, gekennzeichnet durch Bilden einer sekundären Fasermatte mittels Dublieren der primären Matte, in dem sie in eine Anzahl von schräg zur Längsrichtung der sekundären Matte verlaufende Lagen gelegt wird, Schneiden der sekundären Fasermatte in Längsrichtung zur Bildung von Lamellen, Schneiden der Lamellen auf gewünschte Längen, Wenden der Lamellen um 90° um ihre Längsachse und Verbinden der Lamellen miteinander zur Bildung von Tafeln und Unterziehen der Lamellen einer Oberflächenpressung gefolgt von einer Längspressung entweder bevor die Fasermatte in Lamellen geschnitten wird, oder danach.
  2. Verfahren nach Anspruch 1, gekennzeichnet durch die Verwendung von Lamellen, die in Längsrichtung auf ein Verhältnis im Bereich von 1,5:1 bis 4:1 gepreßt wurden.
  3. Verfahren nach Anspruch 1 oder 2, gekennzeichnet durch die Verwendung von Lamellen, die einer Oberflächenpressung auf ein Verhältnis im Bereich von 3:1 bis 6:1 unterzogen wurden.
  4. Verfahren nach einem der Ansprüche 1 bis 3, dadurch gekennzeichnet, daß die Fasermatte in Lamellen mit gewünschten Längen geschnitten wird, bevor sie um 90° gewendet und zu Lamellentafeln vereinigt wird.
  5. Verfahren nach einem der Ansprüche 1 bis 4 und umfassend das Zuführen eines wärmehärtenden Bindemittels zu den Fasern, dadurch gekennzeichnet, daß die Oberflächenpressung und die Längspressung bewirkt werden, bevor die Fasermatte einer Wärmebehandlung zum Härten des Bindemittels unterzogen wird.
EP92901216A 1990-12-07 1991-12-06 Verfahren zur herstellung von isolierenden, aus untereinander verbundenen stabförmigen mineralfaserelementen bestehenden platten Expired - Lifetime EP0560878B1 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DK291590A DK165926B (da) 1990-12-07 1990-12-07 Fremgangsmaade til fremstilling af isoleringsplader sammensat af indbyrdes forbundne stavformede mineralfiberelementer
DK2915/90 1990-12-07
PCT/DK1991/000383 WO1992010602A1 (en) 1990-12-07 1991-12-06 Method of manufacturing insulating boards composed of interconnected rod-shaped mineral fibre elements

Publications (2)

Publication Number Publication Date
EP0560878A1 EP0560878A1 (de) 1993-09-22
EP0560878B1 true EP0560878B1 (de) 1994-10-19

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Application Number Title Priority Date Filing Date
EP92901216A Expired - Lifetime EP0560878B1 (de) 1990-12-07 1991-12-06 Verfahren zur herstellung von isolierenden, aus untereinander verbundenen stabförmigen mineralfaserelementen bestehenden platten

Country Status (12)

Country Link
EP (1) EP0560878B1 (de)
AT (1) ATE113087T1 (de)
AU (1) AU9080591A (de)
CA (1) CA2095532C (de)
CZ (1) CZ282594B6 (de)
DE (1) DE69104730T2 (de)
DK (1) DK165926B (de)
ES (1) ES2062884T3 (de)
FI (1) FI112953B (de)
PL (1) PL168628B1 (de)
SK (1) SK282244B6 (de)
WO (1) WO1992010602A1 (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11590747B2 (en) * 2016-05-13 2023-02-28 Rockwool International A/S Method of producing a mineral wool product comprising a multiple of lamellae and a product of such kind

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EP2100992A1 (de) * 2008-03-12 2009-09-16 Paroc Oy Ab Verfahren und Anordnung zur Verbesserung der Lauffähigkeit eines durchgehenden Mineralfasernetzes
FI20096094A (fi) * 2009-10-23 2011-04-24 Finnfoam Oy Menetelmä eristelevyn valmistamiseksi ja eristelevy
FI20105564A0 (fi) * 2010-05-21 2010-05-21 Saint Gobain Rakennustuotteet Eristyspala, eristysmenetelmä ja eristyspakkaus
CN108589029B (zh) 2011-09-30 2021-03-12 欧文斯科宁知识产权资产有限公司 玻璃纤维的分层的叠毡及其形成方法
RU2506158C1 (ru) * 2012-05-29 2014-02-10 Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Южно-Уральский государственный университет" (национальный исследовательский университет) (ФГБОУ ВПО "ЮУрГУ" (НИУ)) Способ производства минераловатных изделий
SI2931955T1 (sl) * 2012-12-11 2017-04-26 Rockwool International A/S Postopek za oblikovanje izdelka iz utrjenih mineralnih vlaken
RU2694377C2 (ru) * 2014-11-24 2019-07-12 Роквул Интернэшнл А/С Способ производства сердцевины сэндвич-панели из волокон минеральной ваты
PL412081A1 (pl) 2015-04-21 2016-10-24 Tabor Aneta Tomisol Mata izolacyjna lamelowa i linia produkcyjna do wytwarzania maty izolacyjnej lamelowej
FR3052762B1 (fr) 2016-06-17 2020-09-25 Saint Gobain Isover Installation de traitement d'un matelas de fibres minerales par detection et evacuation de defauts localises, et procede correspondant
PL3276064T3 (pl) 2016-07-27 2021-03-08 Technische Universität Dresden Rdzeń warstwowy zawierający materiał włóknisty i sposób jego wytwarzania oraz płyta warstwowa
CA3061973A1 (en) 2017-05-11 2018-11-15 Rockwool International A/S A method of manufacturing a moulded mineral wool product and a product of such kind
PL3628481T3 (pl) 2018-09-27 2023-01-16 Rockwool International A/S Płyta warstwowa

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US11590747B2 (en) * 2016-05-13 2023-02-28 Rockwool International A/S Method of producing a mineral wool product comprising a multiple of lamellae and a product of such kind
US11865826B2 (en) 2016-05-13 2024-01-09 Rockwool A/S Method of producing a mineral wool product comprising a multiple of lamellae and a product of such kind

Also Published As

Publication number Publication date
SK282244B6 (sk) 2001-12-03
DK291590A (da) 1992-06-17
WO1992010602A1 (en) 1992-06-25
DE69104730D1 (de) 1994-11-24
AU9080591A (en) 1992-07-08
CA2095532C (en) 2000-11-07
CZ282594B6 (cs) 1997-08-13
FI932566A0 (fi) 1993-06-04
PL168628B1 (pl) 1996-03-29
ATE113087T1 (de) 1994-11-15
CZ106793A3 (en) 1993-11-17
ES2062884T3 (es) 1994-12-16
SK56293A3 (en) 1994-05-11
DE69104730T2 (de) 1995-05-04
FI112953B (fi) 2004-02-13
CA2095532A1 (en) 1992-06-08
EP0560878A1 (de) 1993-09-22
FI932566A (fi) 1993-06-04
DK291590D0 (da) 1990-12-07
DK165926B (da) 1993-02-08

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