CN114469791A - Compound specially developed for scalp care and preparation method and application thereof - Google Patents
Compound specially developed for scalp care and preparation method and application thereof Download PDFInfo
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- CN114469791A CN114469791A CN202210160951.XA CN202210160951A CN114469791A CN 114469791 A CN114469791 A CN 114469791A CN 202210160951 A CN202210160951 A CN 202210160951A CN 114469791 A CN114469791 A CN 114469791A
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- 210000004761 scalp Anatomy 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 150000001875 compounds Chemical class 0.000 title abstract description 18
- 239000000284 extract Substances 0.000 claims abstract description 105
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 34
- 241001643642 Viticis Species 0.000 claims abstract description 23
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical compound CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims abstract description 18
- 241001289529 Fallopia multiflora Species 0.000 claims abstract description 13
- 241001071795 Gentiana Species 0.000 claims abstract description 10
- 229940002508 ginger extract Drugs 0.000 claims abstract description 10
- 235000020708 ginger extract Nutrition 0.000 claims abstract description 10
- 229940107131 ginseng root Drugs 0.000 claims abstract description 10
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims abstract description 7
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims abstract description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 5
- 235000001287 Guettarda speciosa Nutrition 0.000 claims abstract description 5
- 244000061520 Angelica archangelica Species 0.000 claims abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 126
- 238000000605 extraction Methods 0.000 claims description 60
- 239000000843 powder Substances 0.000 claims description 51
- 238000010298 pulverizing process Methods 0.000 claims description 42
- 238000010438 heat treatment Methods 0.000 claims description 33
- 238000002156 mixing Methods 0.000 claims description 33
- 238000003756 stirring Methods 0.000 claims description 32
- 238000001035 drying Methods 0.000 claims description 30
- 238000004140 cleaning Methods 0.000 claims description 25
- 238000007873 sieving Methods 0.000 claims description 24
- 238000000643 oven drying Methods 0.000 claims description 21
- 238000001291 vacuum drying Methods 0.000 claims description 21
- 238000010992 reflux Methods 0.000 claims description 18
- 238000001914 filtration Methods 0.000 claims description 17
- 238000001816 cooling Methods 0.000 claims description 16
- 241000208340 Araliaceae Species 0.000 claims description 12
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims description 12
- 235000003140 Panax quinquefolius Nutrition 0.000 claims description 12
- 229940102465 ginger root Drugs 0.000 claims description 12
- 235000008434 ginseng Nutrition 0.000 claims description 12
- 239000001841 zingiber officinale Substances 0.000 claims description 12
- 239000008367 deionised water Substances 0.000 claims description 11
- 229910021641 deionized water Inorganic materials 0.000 claims description 11
- 241000382455 Angelica sinensis Species 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 6
- BJRNKVDFDLYUGJ-RMPHRYRLSA-N hydroquinone O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-RMPHRYRLSA-N 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 239000006228 supernatant Substances 0.000 claims description 6
- 235000013399 edible fruits Nutrition 0.000 claims description 5
- 239000004744 fabric Substances 0.000 claims description 5
- 238000007689 inspection Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 238000005070 sampling Methods 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 4
- 240000001341 Reynoutria japonica Species 0.000 claims description 3
- 235000018167 Reynoutria japonica Nutrition 0.000 claims description 3
- 239000009188 angelicae sinensis extract Substances 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- 239000001243 zingiber officinale rosc. root absolute Substances 0.000 claims description 3
- 240000007228 Mangifera indica Species 0.000 claims description 2
- 235000014826 Mangifera indica Nutrition 0.000 claims description 2
- 239000002131 composite material Substances 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 1
- 239000003973 paint Substances 0.000 claims 1
- 230000036541 health Effects 0.000 abstract description 4
- 208000001840 Dandruff Diseases 0.000 abstract description 3
- 230000002401 inhibitory effect Effects 0.000 abstract description 2
- 230000003859 lipid peroxidation Effects 0.000 abstract description 2
- 230000003647 oxidation Effects 0.000 abstract description 2
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 210000002374 sebum Anatomy 0.000 abstract description 2
- 230000028327 secretion Effects 0.000 abstract description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
- 239000000047 product Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 239000011780 sodium chloride Substances 0.000 description 4
- 201000004384 Alopecia Diseases 0.000 description 3
- 239000003708 ampul Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000002453 shampoo Substances 0.000 description 3
- 241000125175 Angelica Species 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 241000989077 Vitex rotundifolia Species 0.000 description 2
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 description 2
- 231100000360 alopecia Toxicity 0.000 description 2
- 229940057950 sodium laureth sulfate Drugs 0.000 description 2
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- FKMHSNTVILORFA-UHFFFAOYSA-N 2-[2-(2-dodecoxyethoxy)ethoxy]ethanol Chemical compound CCCCCCCCCCCCOCCOCCOCCO FKMHSNTVILORFA-UHFFFAOYSA-N 0.000 description 1
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 description 1
- 244000303965 Cyamopsis psoralioides Species 0.000 description 1
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 1
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 1
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 1
- FPVVYTCTZKCSOJ-UHFFFAOYSA-N Ethylene glycol distearate Chemical group CCCCCCCCCCCCCCCCCC(=O)OCCOC(=O)CCCCCCCCCCCCCCCCC FPVVYTCTZKCSOJ-UHFFFAOYSA-N 0.000 description 1
- 241001416997 Mandelia Species 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 229960000458 allantoin Drugs 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 description 1
- 229940073507 cocamidopropyl betaine Drugs 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 229940125898 compound 5 Drugs 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000249 desinfective effect Effects 0.000 description 1
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 1
- WSDISUOETYTPRL-UHFFFAOYSA-N dmdm hydantoin Chemical compound CC1(C)N(CO)C(=O)N(CO)C1=O WSDISUOETYTPRL-UHFFFAOYSA-N 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 208000024963 hair loss Diseases 0.000 description 1
- 230000003676 hair loss Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 229940057905 laureth-3 Drugs 0.000 description 1
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 description 1
- 229960003415 propylparaben Drugs 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 229940048109 sodium methyl cocoyl taurate Drugs 0.000 description 1
- KKDONKAYVYTWGY-UHFFFAOYSA-M sodium;2-(methylamino)ethanesulfonate Chemical compound [Na+].CNCCS([O-])(=O)=O KKDONKAYVYTWGY-UHFFFAOYSA-M 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a compound specially developed for scalp care and a preparation method and application thereof, and relates to the technical field of scalp care. The compound specially developed for scalp care comprises the following components in parts by weight: phase A comprises 100 parts of water and 40-60 parts of dipropylene glycol; the phase B comprises 2-5 parts of ginseng root extract, 1-5 parts of rhizoma anemarrhenae extract, 5-10 parts of ginger extract, 2-5 parts of angelica extract, 2-5 parts of lateral bur leaf extract, 1-5 parts of polygonum multiflorum root extract, 5-10 parts of fructus viticis extract and 2-5 parts of gentian extract; phase C comprises polysorbate-205-10 parts, 1, 2-ethanediol 0.5-1 part, p-hydroxyacetophenone 0.5-1 part and butanediol 3-10 parts. The compound has the advantages of effectively relieving scalp discomfort, reducing dandruff generation, resisting oxidation, effectively removing free radicals, reducing sebum secretion and inhibiting scalp lipid peroxidation; protecting resident flora and maintaining scalp health.
Description
Technical Field
The invention relates to the technical field of scalp care, in particular to a compound specially developed for scalp care and a preparation method and application thereof.
Background
According to the investigation of Weijian Commission, China has about 2.5 hundred million alopecia people, wherein 90 th day accounts for more than festival. The hair loss crowd is increased, the attention and consciousness of people on scalp care are higher and higher, so the demand on scalp care products is gradually increased, white collars and students are mainly used, the average age is 34 years old, the attention on scalp care is higher, and the scalp care products account for the main crowd in scalp care product consumption number.
The scalp is one of special skin areas in the whole skin, but people pay little attention to the scalp, and the scalp is rarely treated like skin. Common problems with the scalp are: alopecia, dandruff, pimple, pruritus, and aging. In the existing products for scalp care in the market, chemical components are excessively added, the scalp is greatly stimulated, skin is damaged to a certain extent, and an ideal care effect cannot be achieved, so that scalp health management is the best stage of the current research, and a safe and effective scalp care compound needs to be researched.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a compound specially developed for scalp care and a preparation method and application thereof, and solves the problems that the existing products for scalp care in the market have excessive chemical component addition, great irritation to the scalp, certain damage to the skin and unsatisfactory care effect, so that scalp health management is the best stage of the current research, and a safe and effective scalp care compound needs to be researched.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: a compound specially developed for scalp care comprises the following components in parts: the phase A comprises 100 parts of water and 40-60 parts of dipropylene glycol; the phase B comprises 2-5 parts of ginseng root extract, 1-5 parts of rhizoma anemarrhenae extract, 5-10 parts of ginger extract, 2-5 parts of angelica extract, 2-5 parts of lateral bur leaf extract, 1-5 parts of polygonum multiflorum root extract, 5-10 parts of fructus viticis extract and 2-5 parts of gentian extract; phase C comprises polysorbate-205-10 parts, 1, 2-ethanediol 0.5-1 part, p-hydroxyacetophenone 0.5-1 part and butanediol 3-10 parts.
Preferably, the preparation process of the ginseng root extract, the rhizoma anemarrhenae extract, the ginger extract, the angelica sinensis extract, the bur leaf extract, the polygonum multiflorum root extract, the vitex rotundifolia fruit extract and the gentian extract is as follows:
ginseng root extract: pretreatment: cleaning fresh Ginseng radix, oven drying, and slicing; extraction: adding 10 times of deionized water into Ginseng radix for the first time, heating to boiling, maintaining the temperature, and extracting for 2 hr; adding deionized water 5 times the amount of the filtrate in the second and third times, heating to boiling, extracting for 1 hr, and centrifuging to obtain centrifugate; concentration: adding the ginseng centrifugate into a concentration tank, and concentrating to obtain thick paste; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow Ginseng radix extract powder;
rhizoma anemarrhenae extract: pretreatment: cleaning dried rhizome of rhizoma anemarrhenae, oven drying, and pulverizing into coarse powder; extraction: adding processed rhizoma anemarrhenae into an extraction tank, adding 8 times of 75% ethanol, heating to 50 deg.C, extracting for 1h, adding 6 times of 75% ethanol, heating to 50 deg.C, extracting for 1h, filtering with 800 mesh sieve, and mixing the extractive solutions; concentration: adding the prepared rhizoma anemarrhenae extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow rhizoma anemarrhenae extract powder;
ginger extract: pretreatment: cleaning fresh ginger root, drying at low temperature, and slicing; extraction: adding processed ginger root into an extraction tank, adding 75% ethanol 8 times the weight of ginger root for the first time, heating to 50 deg.C, extracting for 1.5h, adding 75% ethanol 5 times the weight of ginger root for the second time and the third time, heating to 50 deg.C, extracting for 1.5h, filtering with 800 mesh, and mixing the extractive solutions; concentration: adding the prepared ginger root extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain yellow rhizoma Zingiberis recens extract powder;
and (3) Chinese angelica extract: pretreatment: cleaning dried radix Angelicae sinensis, oven drying, and pulverizing into coarse powder; extraction: adding the processed radix Angelicae sinensis into an extraction tank, adding 8 times of 90% ethanol for reflux extraction for 2 hr for the first time, adding 6 times of 90% ethanol for reflux extraction for 2 hr for the second time, and collecting to obtain extractive solution; concentration: adding the prepared angelica sinensis extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed soft extract, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow radix Angelicae sinensis extract powder;
extract of lateral bur leaves: pretreatment: cleaning dried folium Platycladi, oven drying, and pulverizing;
extraction: adding the processed cacumen Platycladi powder into an extraction tank, adding 8 times of 60% ethanol for reflux extraction for 2 hr for the first time, adding 6 times of 60% ethanol for reflux extraction for 2 hr for the second time, collecting extractive solution, and filtering to obtain supernatant;
concentration: adding the prepared supernatant of the cacumen biotae extracting solution into a concentration tank for concentration, and recovering ethanol under reduced pressure;
drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow folium Platycladi extract powder;
the polygonum multiflorum root extract: pretreatment: cleaning dried tuber fleeceflower root, oven drying, and pulverizing into coarse powder; extraction: adding processed radix Polygoni Multiflori into an extraction tank, adding 8 times of 75% ethanol, heating to 50 deg.C for 1 hr, adding 6 times of 75% ethanol, heating to 50 deg.C for 1 hr, filtering with 800 mesh sieve, and mixing the extractive solutions; concentration: adding the prepared polygonum multiflorum extracting solution into a concentrating tank for concentrating, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow Polygoni Multiflori radix extract powder;
fructus viticis extract: pretreatment: cleaning fructus Viticis Cannabifoliae, oven drying, and pulverizing; extraction: adding the processed fructus Viticis negundo powder into an extraction tank, adding 90% ethanol with 10 times of the amount of the fructus Viticis negundo powder for reflux extraction for 2h for the first time, adding 90% ethanol with 6 times of the amount of the fructus Viticis negundo powder for reflux extraction for 2h for the second time, and collecting to obtain extractive solution; concentration: adding the prepared fructus Viticis Cannabifoliae extract into a concentration tank, concentrating, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed soft extract, pulverizing, sieving with 80 mesh sieve, and mixing to obtain brown yellow Mangifera indica fruit extract powder;
and (3) gentian extract: pretreatment: cleaning dried radix Gentianae, oven drying at low temperature, and pulverizing; extraction: soaking the treated fel Ursi powder with 85% ethanol for 6 hr, adding the soaked fel Ursi powder into a percolating cylinder, and percolating with 8 times volume of 85% ethanol to remove air in the cylinder; concentration: recovering ethanol under reduced pressure; drying and crushing: drying at 50 deg.C, pulverizing, sieving with 80 mesh sieve, and mixing to obtain brown yellow radix Gentianae extract powder.
A preparation method and application of a compound specially developed for scalp care comprise the following preparation procedures:
s1: preparing water by using a deionized water device for later use;
s2: c, heating relative hydroxyacetophenone to 60 ℃ by using butanediol in advance until the hydroxyacetophenone is completely dissolved for later use;
s3: sequentially adding the phase A raw materials into a homogenizing pot, heating to 85-95 ℃, stirring and preserving heat for 0.5h, wherein the stirring speed is 200 rpm/min;
s4: cooling to 45 ℃, sequentially adding the phase B and uniformly stirring at the stirring speed of 200 rpm/min;
s5: cooling to 40 ℃, adding the phase C, and uniformly stirring at the stirring speed of 200 rpm/min;
s6: cooling to 38 ℃, and stirring for 10 min;
s7: sampling and inspecting, and filtering and discharging by using 600-mesh filter cloth;
s8: and (6) warehousing after inspection.
(III) advantageous effects
The invention provides a compound specially developed for scalp care and a preparation method and application thereof. The method has the following beneficial effects:
the compound has the advantages of effectively relieving scalp discomfort, reducing dandruff generation, resisting oxidation, effectively removing free radicals, reducing sebum secretion and inhibiting scalp lipid peroxidation; protecting resident flora and maintaining scalp health.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the embodiment of the invention provides a compound specially developed for scalp care, which comprises the following components in parts: the phase A comprises 100 parts of water and 40-60 parts of dipropylene glycol; the phase B comprises 2-5 parts of ginseng root extract, 1-5 parts of rhizoma anemarrhenae extract, 5-10 parts of ginger extract, 2-5 parts of angelica extract, 2-5 parts of lateral bur leaf extract, 1-5 parts of polygonum multiflorum root extract, 5-10 parts of fructus viticis extract and 2-5 parts of gentian extract; phase C comprises polysorbate-205-10 parts, 1, 2-ethanediol 0.5-1 part, p-hydroxyacetophenone 0.5-1 part and butanediol 3-10 parts.
Preferably, the preparation process of the ginseng root extract, the rhizoma anemarrhenae extract, the ginger extract, the angelica sinensis extract, the bur leaf extract, the polygonum multiflorum root extract, the vitex rotundifolia fruit extract and the gentian extract is as follows:
ginseng root extract: pretreatment: cleaning fresh Ginseng radix, oven drying, and slicing; extraction: adding 10 times of deionized water into Ginseng radix for the first time, heating to boiling, maintaining the temperature, and extracting for 2 hr; adding deionized water 5 times the amount of the filtrate in the second and third times, heating to boiling, extracting for 1 hr, and centrifuging to obtain centrifugate; concentration: adding the ginseng centrifugate into a concentration tank, and concentrating to obtain thick paste; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow Ginseng radix extract powder;
rhizoma anemarrhenae extract: pretreatment: cleaning dried rhizome of rhizoma anemarrhenae, oven drying, and pulverizing into coarse powder; extraction: adding processed rhizoma anemarrhenae into an extraction tank, adding 8 times of 75% ethanol, heating to 50 deg.C, extracting for 1h, adding 6 times of 75% ethanol, heating to 50 deg.C, extracting for 1h, filtering with 800 mesh sieve, and mixing the extractive solutions; concentration: adding the prepared rhizoma anemarrhenae extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow rhizoma anemarrhenae extract powder;
ginger extract: pretreatment: cleaning fresh ginger root, drying at low temperature, and slicing; extraction: adding processed ginger root into an extraction tank, adding 75% ethanol 8 times the weight of ginger root for the first time, heating to 50 deg.C, extracting for 1.5h, adding 75% ethanol 5 times the weight of ginger root for the second time and the third time, heating to 50 deg.C, extracting for 1.5h, filtering with 800 mesh, and mixing the extractive solutions; concentration: adding the prepared ginger root extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain yellow rhizoma Zingiberis recens extract powder;
and (3) Chinese angelica extract: pretreatment: cleaning dried radix Angelicae sinensis, oven drying, and pulverizing into coarse powder; extraction: adding the processed radix Angelicae sinensis into an extraction tank, adding 8 times of 90% ethanol for reflux extraction for 2 hr for the first time, adding 6 times of 90% ethanol for reflux extraction for 2 hr for the second time, and collecting to obtain extractive solution; concentration: adding the prepared angelica sinensis extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed soft extract, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow radix Angelicae sinensis extract powder;
extract of lateral bur leaves: pretreatment: cleaning dried folium Platycladi, oven drying, and pulverizing;
extraction: adding the processed cacumen Platycladi powder into an extraction tank, adding 8 times of 60% ethanol for reflux extraction for 2 hr for the first time, adding 6 times of 60% ethanol for reflux extraction for 2 hr for the second time, collecting extractive solution, and filtering to obtain supernatant;
concentration: adding the prepared supernatant of the cacumen biotae extracting solution into a concentration tank for concentration, and recovering ethanol under reduced pressure;
drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow folium Platycladi extract powder;
the polygonum multiflorum root extract: pretreatment: cleaning dried tuber fleeceflower root, oven drying, and pulverizing into coarse powder; extraction: adding processed radix Polygoni Multiflori into an extraction tank, adding 8 times of 75% ethanol, heating to 50 deg.C for 1 hr, adding 6 times of 75% ethanol, heating to 50 deg.C for 1 hr, filtering with 800 mesh sieve, and mixing the extractive solutions; concentration: adding the prepared polygonum multiflorum extracting solution into a concentrating tank for concentrating, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow Polygoni Multiflori radix extract powder;
fructus viticis extract: pretreatment: cleaning fructus Viticis Cannabifoliae, oven drying, and pulverizing; extraction: adding the processed fructus Viticis negundo powder into an extraction tank, adding 90% ethanol with 10 times of the amount of the fructus Viticis negundo powder for reflux extraction for 2h for the first time, adding 90% ethanol with 6 times of the amount of the fructus Viticis negundo powder for reflux extraction for 2h for the second time, and collecting to obtain extractive solution; concentration: adding the prepared fructus Viticis Cannabifoliae extract into a concentration tank, concentrating, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed soft extract, pulverizing, sieving with 80 mesh sieve, mixing to obtain brown yellow Mandelia tree fruit extract powder;
and (3) gentian extract: pretreatment: cleaning dried radix Gentianae, oven drying at low temperature, and pulverizing; extraction: soaking the treated fel Ursi powder with 85% ethanol for 6 hr, adding the soaked fel Ursi powder into a percolating cylinder, and percolating with 8 times volume of 85% ethanol to remove air in the cylinder; concentration: recovering ethanol under reduced pressure; drying and crushing: drying at 50 deg.C, pulverizing, sieving with 80 mesh sieve, and mixing to obtain brown yellow radix Gentianae extract powder.
A preparation method and application of a compound specially developed for scalp care comprise the following preparation procedures:
s1: preparing water by using a deionized water device for later use;
s2: c, heating relative hydroxyacetophenone to 60 ℃ by using butanediol in advance until the hydroxyacetophenone is completely dissolved for later use;
s3: sequentially adding the phase A raw materials into a homogenizing pot, heating to 85-95 ℃, stirring and preserving heat for 0.5h, wherein the stirring speed is 200 rpm/min;
s4: cooling to 45 ℃, sequentially adding the phase B and uniformly stirring at the stirring speed of 200 rpm/min;
s5: cooling to 40 ℃, adding the phase C, and uniformly stirring at the stirring speed of 200 rpm/min;
s6: cooling to 38 ℃, and stirring for 10 min;
s7: sampling and inspecting, and filtering and discharging by using 600-mesh filter cloth;
s8: and (6) warehousing after inspection.
Example two:
a compound specially developed for scalp care is applied to scalp cleansing cream, shampoo, scalp ampoule, scalp essence, etc.;
the preparation method of the scalp care compound in the scalp ampoule essence comprises the following steps:
the raw materials in parts by weight are as follows: the phase A comprises 88.65% of water, 0.1% of xanthan gum, 3.0% of dipropylene glycol, 0.05% of EDAT disodium, 0.2% of allantoin, urea and 0.2% of water; phase B is dipropylene glycol 2.0, p-hydroxyacetophenone 0.5 and 1, 2-ethanediol 0.5; phase C is scalp care complex 5.0.
The preparation process of the scalp ampoule essence comprises the following steps:
1. preparing water by using a deionized water device for later use;
2. b, heating the hydroxyacetophenone to 60 ℃ in advance by using dipropylene glycol until the hydroxyacetophenone is completely dissolved for later use;
3. sequentially adding the phase A raw materials into a homogenizing pot, heating to 85-95 ℃, stirring and preserving heat for 0.5h, wherein the stirring speed is 200 rpm/min;
4. cooling to 45 ℃, sequentially adding B, C phases, and uniformly stirring at the stirring speed of 200 rpm/min;
5. cooling to 38 ℃, and stirring for 10 min;
6. sampling and inspecting, and filtering and discharging by using 400-mesh filter cloth;
7. and warehousing after the inspection is qualified.
The preparation method of the scalp care compound in the shampoo comprises the following steps:
the raw materials in parts by weight are as follows: the A1 phase is guar hydroxypropyl trimethyl ammonium chloride 0.2, the A2 phase is water 70.82, the A3 phase is citric acid 0.08, the A4 phase is water, cocamidopropyl betaine, sodium chloride and sodium benzoate 2; phase B is ethylene glycol distearate 1, sodium laureth sulfate, water, laureth-3, ammonium sulfate 10, sodium laureth sulfate 3.8, disodium EDTA and water 0.05; the phase C is palm kernel oil amide DEA, glycerin, palm kernel oleic acid, water 2, water, polyquaternium-7, methyl hydroxybenzoate, propyl hydroxybenzoate 1, water, sodium methyl cocoyl taurate, sodium chloride, coconut oil acid, and sodium methyl taurate 2; phase D is phenoxyethanol 0.05, DMDM hydantoin and water 0.2; phase E is (daily) essence 0.3, sodium chloride 1.5 and scalp care compound 5.
The preparation process of the shampoo comprises the following steps:
1. preparing water by using a deionized water device for later use;
2. cleaning and disinfecting required equipment and appliances;
3. a3 is dispersed with water in advance for use;
4. e-phase sodium chloride 7 is dispersed by water in advance for later use;
5. pumping A2 water into a homogenizing pot, adding A1 phase under a homogeneous state until the A2 water is uniformly dispersed without particles;
6. adding A3, stirring, adding A4, and stirring;
7. sequentially adding the B-phase materials into a homogenizing pot, heating to 90 ℃ while stirring until the materials are completely dissolved, and preserving the temperature for 20 minutes;
8. cooling to 65 ℃, adding the C phases in sequence, stirring uniformly, and continuously cooling;
9. cooling to 45 ℃, sequentially adding the D-phase materials, and uniformly stirring;
10. cooling to 40 ℃, sequentially adding the E-phase materials, and uniformly stirring;
11. cooling to 36 deg.C, sampling, inspecting, and filtering with 200 mesh filter cloth;
12. and warehousing after the inspection is qualified.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (3)
1. A composite developed specifically for scalp care characterized by: the paint comprises the following components in parts by weight: the phase A comprises 100 parts of water and 40-60 parts of dipropylene glycol; the phase B comprises 2-5 parts of ginseng root extract, 1-5 parts of rhizoma anemarrhenae extract, 5-10 parts of ginger extract, 2-5 parts of angelica extract, 2-5 parts of lateral bur leaf extract, 1-5 parts of polygonum multiflorum root extract, 5-10 parts of fructus viticis extract and 2-5 parts of gentian extract; phase C comprises polysorbate-205-10 parts, 1, 2-ethanediol 0.5-1 part, p-hydroxyacetophenone 0.5-1 part and butanediol 3-10 parts.
2. A composite developed specifically for scalp care according to claim 1, characterized in that: the preparation process of the ginseng root extract, the rhizoma anemarrhenae extract, the ginger extract, the angelica extract, the bur leaf extract, the polygonum multiflorum root extract, the fructus viticis extract and the gentian extract is as follows:
ginseng root extract: pretreatment: cleaning fresh Ginseng radix, oven drying, and slicing; extraction: adding 10 times of deionized water into Ginseng radix for the first time, heating to boiling, maintaining the temperature, and extracting for 2 hr; adding deionized water 5 times the amount of the filtrate in the second and third times, heating to boiling, extracting for 1 hr, and centrifuging to obtain centrifugate; concentration: adding the ginseng centrifugate into a concentration tank, and concentrating to obtain thick paste; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow Ginseng radix extract powder;
rhizoma anemarrhenae extract: pretreatment: cleaning dried rhizome of rhizoma anemarrhenae, oven drying, and pulverizing into coarse powder; extraction: adding processed rhizoma anemarrhenae into an extraction tank, adding 8 times of 75% ethanol, heating to 50 deg.C, extracting for 1h, adding 6 times of 75% ethanol, heating to 50 deg.C, extracting for 1h, filtering with 800 mesh sieve, and mixing the extractive solutions; concentration: adding the prepared rhizoma anemarrhenae extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow rhizoma anemarrhenae extract powder;
ginger extract: pretreatment: cleaning fresh ginger root, drying at low temperature, and slicing; extraction: adding processed ginger root into an extraction tank, adding 75% ethanol 8 times the weight of ginger root for the first time, heating to 50 deg.C, extracting for 1.5h, adding 75% ethanol 5 times the weight of ginger root for the second time and the third time, heating to 50 deg.C, extracting for 1.5h, filtering with 800 mesh, and mixing the extractive solutions; concentration: adding the prepared ginger root extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain yellow rhizoma Zingiberis recens extract powder;
and (3) Chinese angelica extract: pretreatment: cleaning dried radix Angelicae sinensis, oven drying, and pulverizing into coarse powder; extraction: adding the processed radix Angelicae sinensis into an extraction tank, adding 8 times of 90% ethanol for reflux extraction for 2 hr for the first time, adding 6 times of 90% ethanol for reflux extraction for 2 hr for the second time, and collecting to obtain extractive solution; ③ concentrating: adding the prepared angelica sinensis extract into a concentration tank for concentration, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed soft extract, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow radix Angelicae sinensis extract powder;
extract of lateral bur leaves: pretreatment: cleaning dried folium Platycladi, oven drying, and pulverizing;
extraction: adding the processed cacumen Platycladi powder into an extraction tank, adding 8 times of 60% ethanol for reflux extraction for 2 hr for the first time, adding 6 times of 60% ethanol for reflux extraction for 2 hr for the second time, collecting extractive solution, and filtering to obtain supernatant;
③ concentrating: adding the prepared supernatant of the cacumen biotae extracting solution into a concentration tank for concentration, and recovering ethanol under reduced pressure;
drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow folium Platycladi extract powder;
the polygonum multiflorum root extract: pretreatment: cleaning dried tuber fleeceflower root, oven drying, and pulverizing into coarse powder; extraction: adding processed radix Polygoni Multiflori into an extraction tank, adding 8 times of 75% ethanol, heating to 50 deg.C for 1 hr, adding 6 times of 75% ethanol, heating to 50 deg.C for 1 hr, filtering with 800 mesh sieve, and mixing the extractive solutions; ③ concentrating: adding the prepared polygonum multiflorum extracting solution into a concentrating tank for concentrating, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed thick paste, pulverizing, sieving with 80 mesh sieve, and mixing to obtain light yellow Polygoni Multiflori radix extract powder;
fructus viticis extract: pretreatment: cleaning fructus Viticis Cannabifoliae, oven drying, and pulverizing; extraction: adding the processed fructus Viticis negundo powder into an extraction tank, adding 90% ethanol with 10 times of the amount of the fructus Viticis negundo powder for reflux extraction for 2h for the first time, adding 90% ethanol with 6 times of the amount of the fructus Viticis negundo powder for reflux extraction for 2h for the second time, and collecting to obtain extractive solution; concentration: adding the prepared fructus Viticis Cannabifoliae extract into a concentration tank, concentrating, and recovering ethanol under reduced pressure; drying and crushing: vacuum drying the concentrated and condensed soft extract, pulverizing, sieving with 80 mesh sieve, and mixing to obtain brown yellow Mangifera indica fruit extract powder;
and (3) extracting gentian: pretreatment: cleaning dried radix Gentianae, oven drying at low temperature, and pulverizing; extraction: soaking the treated fel Ursi powder with 85% ethanol for 6 hr, adding the soaked fel Ursi powder into a percolating cylinder, and percolating with 8 times volume of 85% ethanol to remove air in the cylinder; concentration: recovering ethanol under reduced pressure; drying and crushing: drying at 50 deg.C, pulverizing, sieving with 80 mesh sieve, and mixing to obtain brown yellow radix Gentianae extract powder.
3. A method for preparing and using a composition specifically developed for scalp care, characterized in that: the method comprises the following preparation processes:
s1: preparing water by using a deionized water device for later use;
s2: c, heating relative hydroxyacetophenone to 60 ℃ by using butanediol in advance until the hydroxyacetophenone is completely dissolved for later use;
s3: sequentially adding the phase A raw materials into a homogenizing pot, heating to 85-95 ℃, stirring and preserving heat for 0.5h, wherein the stirring speed is 200 rpm/min;
s4: cooling to 45 ℃, sequentially adding the phase B and uniformly stirring at the stirring speed of 200 rpm/min;
s5: cooling to 40 ℃, adding the phase C, and uniformly stirring at the stirring speed of 200 rpm/min;
s6: cooling to 38 ℃, and stirring for 10 min;
s7: sampling and inspecting, and filtering and discharging by using 600-mesh filter cloth;
s8: and (6) warehousing after inspection.
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