CN104825361A - Natural shampoo containing camellia saponin - Google Patents

Abstract

The invention discloses a natural shampoo containing camellia saponin. The natural shampoo comprises (1) basic functional components, which are extracted from natural plants such as wheat leaf, green tea, rosemary, bitter garden sorrel, ginger, pseudostellaria root, radix scutellariae, tansy, pepper, stephania cepharantha, and the like; (2) emulsifier and foaming agent, which are composed of camellia saponin, soapberry saponin, aescine, alginic acid, and the like; and (3) safe components such as wild tea oil, lactic acid, sodium lactate, sodium chloride, and the like. The provided shampoo can supply nutrients to scalp, is capable of promoting blood circulation, conditioning and wetting the hair, preventing bacteria including malassezia, which can cause dandruff, eliminating inflammation, and reducing the irritation, and has good effects on cleaning hair, removing dandruff, relieving itch, preventing alopecia and sun-burn, and nourishing, protecting and blackening the hairs.

Description

A kind of natural shampoo containing Tsubaki-saponin

Technical field

The invention belongs to bath article field, be specifically related to a kind of natural shampoo containing Tsubaki-saponin and preparation method thereof.

Background technology

shampoo is the cosmetics of everyday use that people often use, but the shampoo used is chemosynthesis is substantially raw material, wash away the sebum of its protective effect on scalp, dry scalp is caused to be subject to the infection of dermatophytes thus to produce the dandruff, also hair is made to dry up, some even has certain stimulation to scalp and hair-care, sensitization, damages etc. produce irritated, itch, the impact that the dandruff etc. are bad, the such as nipalgin that adds of some chemosynthesis antiseptic has been generally acknowledged have carcinogenesis, the use of people to daily use chemicals is allowed to feel fear deeply, scalp can be made under the radiation of solar ultraviolet, hair occurs dry, chap, the bad realizations such as damage, therefore with plant, agricultural byproducts are that the daily chemical products that is developed to of raw material is deeply by the welcome of enterprise and consumer, therefore the present invention also develops a safety as original intention, green, natural shampoo, not only there is good protection, the effect of nutrition scalp also has well anti-dandruff, antipruritic, Anti-hair loss, hair care, the effect of hair care etc.

Summary of the invention

The object of the present invention is to provide a kind of natural shampoo containing Tsubaki-saponin and preparation method thereof, with wheat leaf, Folium Camelliae sinensis, Herba Rosmarini Officinalis, picric acid mould, Rhizoma Zingiberis Recens, Radix Pseudostellariae, Radix Scutellariae, tansy, Fructus Capsici, the extracted form natural plant compositions such as headdress flower Radix Stephaniae Japonicae are as basic function composition, Tsubaki-saponin, sapindoside, aescine, alginic acid etc. are as emulsifying agent and suds booster, wild Oleum Camelliae, lactic acid, lactylate salt, the security elements such as sodium chloride are developed to a kind of natural shampoo, good nutrition is had to scalp, short blood circulation, conditioning, moistening, antibacterial (comprising the chlosma causing scurf), antiinflammatory, reduce the effects such as zest, have well clean to hair, anti-dandruff, antipruritic, Anti-hair loss, sun-proof, hair care, nutrition, hair care, the effects such as hair color.

For achieving the above object, the technical solution used in the present invention is:

Containing a natural shampoo for Tsubaki-saponin, primary raw material is by following weight parts: wild Oleum Camelliae 5-10 part, wheat leaf 4-8 part, Folium Camelliae sinensis 4-8 part, Tsubaki-saponin 3-8 part, Herba Rosmarini Officinalis 3-5 part, sapindoside 2-5 part, aescine 2-5 part, Radix Pseudostellariae 1-3 part, picric acid mould 1-3 part, Rhizoma Zingiberis Recens 1-5 part, Radix Scutellariae 1-3 part, tansy 1-3 part, headdress flower Radix Stephaniae Japonicae 0.1-0.5 part, lactic acid 1-3 part, Pseudotsuga menziesii (Mirbel) Franco 1-3 part, lactylate salt 1-3 part, sodium alginate 0.5-1 part, Fructus Capsici 0.5-1 part, sodium chloride 1.5-2.5 part.

Preparation method comprises the following steps:

1) by wheat leaf and the wild Oleum Camelliae lixiviate of tansy, lixiviating solution 1 is obtained;

2) by Radix Pseudostellariae distilled water lixiviate of boiling, Radix Pseudostellariae Aqueous extracts is obtained; The wild Oleum Camelliae of filtering residue carries out lixiviate, obtains lixiviating solution 2;

3) by the Aqueous extracts of picric acid mould, Radix Scutellariae, Radix Pseudostellariae, Sucus Zingberis, with Folium Camelliae sinensis, Herba Rosmarini Officinalis, Fructus Capsici, Pseudotsuga menziesii (Mirbel) Franco, headdress flower Radix Stephaniae Japonicae alcohol extract mixing, be heated to 75 DEG C, add lixiviating solution 1 and lixiviating solution 2, constant temperature 70 DEG C, add Tsubaki-saponin, sapindoside and aescine, stirring and emulsifying 20min, is cooled to 60 DEG C, adds sodium alginate, lactic acid, regulate pH=6-7 with lactylate salt, use sodium chloride adjusting viscosity.

Step 1) is by the wheat leaf of drying and crushing and fresh tansy, and lixiviate 5d in Oleum Camelliae out of office, filters.

Step 2) by the Radix Pseudostellariae of drying and crushing distilled water lixiviate 1.5h, the solid-liquid ratio 1:10 of boiling, filter, concentrated by rotary evaporation; The wild Oleum Camelliae of filtering residue carries out room temperature lixiviate 5d, and solid-liquid ratio is 1:6, filters.

Prepared by picric acid mould Aqueous extracts: by the picric acid mould of drying and crushing, with the distilled water extraction 30min that boils, solid-liquid ratio 1:10, decompress filter;

Prepared by Radix Scutellariae Aqueous extracts: Radix Scutellariae drying, pulverizing, 60 DEG C of distilled water ultrasonic extraction 1.5h, and solid-liquid ratio is 1:10, filters, concentrated by rotary evaporation.

Stir-frying with ginger juice is standby: first adopt method of squeezing the juice, then carry out decompress filter.

Prepared by Folium Camelliae sinensis alcohol extract: will be ground into the dry Folium Camelliae sinensis 40wt.% alcoholic solution of 20-40 object 80 DEG C of lixiviate 30min, solid-liquid ratio is 1:10, filtration under diminished pressure, revolves to steam and reclaims ethanol;

Prepared by Pseudotsuga menziesii (Mirbel) Franco alcohol extract: dry star-spangled banner Folium Pini 45wt.% alcoholic solution 80 DEG C of lixiviate 5h, and solid-liquid ratio is 1:6, decompress filter;

Prepared by capsanthol extract: Fructus Capsici drying, pulverizing, with 45wt.% alcohol solution dipping 3d, and solid-liquid ratio 1:6, decompress filter;

Herba Rosmarini Officinalis, headdress flower Radix Stephaniae Japonicae alcohol extract preparation: be dried and crushed into 10 object Herba Rosmarini Officinaliss, headdress flower Radix Stephaniae Japonicae 20wt.% alcoholic solution 60 DEG C of lixiviate 8h, solid-liquid ratio 1:6, decompress filter, revolve steam reclaim ethanol.

The preparation of Tsubaki-saponin: after being pulverized by dry Flos Camelliae Japonicae cake, with deionized water lixiviate 3h, temperature is 100 DEG C, solid-liquid ratio 1:6, filters, concentrated by rotary evaporation;

The preparation of sapindoside: by the Fructus Sapindi Mukouossi seed coat of drying and crushing, with deionized water lixiviate 2h, temperature is 100 DEG C, and solid-liquid ratio is 1:10, filters, concentrated by rotary evaporation;

The preparation of aescine: Semen Aesculi seed drying, pulverizing, with deionized water lixiviate 3.5h, temperature is 100 DEG C, and solid-liquid ratio is 1:10, filters, concentrated by rotary evaporation.

The component such as unsaturated oleic acid, linoleic acid abundant containing wild Oleum Camelliae in the natural shampoo of Tsubaki-saponin of the present invention plays moisturizing, irritation, anti-allergic effects, Squalene wherein can antiinflammatory and antibacterial, well can there be antibacterial, antioxidation, anticorrosion, Anti-hair loss stimulate natural on-off cycles of hair growth component in lixiviate wheat leaf, tansy, have on scalp, hair its extractum and well shortly ooze effect; Tsubaki-saponin is pentacyclic triterpene saponins, and HLB value is 16, has good emulsifying, dispersion, washability, can strengthen the immunocompetence of scalp, has good anti-skin pathomycete, antiinflammatory, antisepsis simultaneously, reaches hair washing, anti-dandruff, antipruritic effect; Containing compositions such as tea polyphenols, free amino acid, theophylline, caffeine in Folium Camelliae sinensis, tea polyphenols not only makes good antioxidant absorb the effect of ultraviolet, sterilization, antiinflammatory suppression Achorion schoenleini in addition, so have good astriction, nutrition hair follicle, hair care (protection hair follicle), hair color effect to scalp, there is good antioxidation to shampoo itself; The compositions such as the carnosic acid in Herba Rosmarini Officinalis, carnosol, rosmarinic acid, ursolic acid, pinane are rare have antibacterial, antiinflammatory, anticorrosion, antioxidation, absorption ultraviolet are sun-proof, Herba Rosmarini Officinalis fragrance can also as the fragrance of the body note part of shampoo; Main component picric acid mould in picric acid mould have softening scalp, suppresses the effect of sebum secretion, and have the effect of extremely strong killing fungus, to causing the fungus of scurf to have good killing action, picric acid mould also has good antioxidation to shampoo itself; The main component of Radix Pseudostellariae has polysaccharide, triterpene saponin, cyclic peptide, aminoacid, the composition such as fat-soluble, wherein aminoacid can nutrition hair follicle thus play the effect reaching Anti-hair loss, triterpene saponin has antivirus action that scalp, polysaccharide component can be protected also can to improve the immunity of scalp, also reaches the effect of protection scalp, hair; Radix Scutellariae mainly containing baicalin, neobaicalein, sitosterol, benzoic acid more composition, have in shampoo well antibacterial, antiinflammatory, antiinflammatory, antipruritic, absorb ultraviolet etc. and reach skin protection, the secretion of sebum can be suppressed, antiseptical effect is played to shampoo itself; Sapindoside in Fructus Sapindi Mukouossi has good surface activity, and can remove the sebum of smegma well, have antibiotic property, especially dermatophytes has stronger killing action, thus plays antipruritic, anti-dandruff etc. effect; Have the compositions such as certain gingerol, zingiberone, gingerol in Rhizoma Zingiberis Recens, its permeability is comparatively strong, have good Anti-hair loss, invigorate blood circulation stimulate hair growth promoting, anti-dandruff, in and superoxide radical, the effect such as sun-proof, have good antioxidation, antibacterial action to shampoo itself; Aescin not only has and well helps emulsifying, foam enhancing effect, has good opsonic action to scalp and skin; Alginic acid can play the effect of emulsifying and thickening; The headdress flower a thousand li rattan alkali of headdress flower a thousand li rattan has the circulation of promotion scalp blood to stimulate hair growth promoting, also has opsonic action, also have certain antibiotic property for scalp and hair-care; Yew foline in Pseudotsuga menziesii (Mirbel) Franco can increase DNA activity, is hair follicle cell propagation, can plays growth-promoting and send out, improve quality and the intensity of hair, anti-loss; Fructus Capsici contains abundant piquancy component, in shampoo, not only can assist anti-bacteria fungus, can also relieving itching and removing dandruff.

Remarkable advantage of the present invention is: primarily of different botanical extract and the high composition of natural safety, not only there is the effect such as good nutrition, short blood circulation, conditioning, moistening, antibacterial (comprising the chlosma causing scurf), antiinflammatory, reduction zest to scalp, hair is had to the effect of good clean, anti-dandruff, antipruritic, Anti-hair loss, sun-proof, hair care, nutrition, hair care, hair color etc.

Detailed description of the invention

embodiment 1

Primary raw material: by following weight parts, wild Oleum Camelliae 10 parts, wheat leaf 4 parts, Folium Camelliae sinensis 8 parts, Tsubaki-saponin 6 parts, Herba Rosmarini Officinalis 3 parts, sapindoside 3 parts, aescine 3 parts, Radix Pseudostellariae 3 parts, picric acid mould 1 part, 3 parts, Rhizoma Zingiberis Recens, Radix Scutellariae 3 parts, tansy 2 parts, Pseudotsuga menziesii (Mirbel) Franco 3 parts, headdress flower Radix Stephaniae Japonicae 0.3 part, lactic acid 2 parts, lactylate salt 1 part, sodium alginate 1 part, 0.5 part, Fructus Capsici, 0.5 part, sodium chloride, essence (cinnamic aldehyde oil, laurel) are in right amount.

Preparation technology: wild Oleum Camelliae, wheat leaf, tansy, Radix Pseudostellariae second time extract is component 1, Folium Camelliae sinensis, Herba Rosmarini Officinalis, picric acid mould, Radix Scutellariae, Pseudotsuga menziesii (Mirbel) Franco, Fructus Capsici, headdress flower Radix Stephaniae Japonicae, Radix Pseudostellariae first time extract and Sucus Zingberis are component 2, Tsubaki-saponin, sapindoside, aescine is component 3, component 2 is heated to 75 DEG C, component 1 is joined in component 2, temperature remains on more than 70 DEG C, add component 3 gradually, and constantly carry out stirring and emulsifying 20min, band temperature drops to 60 DEG C and adds sodium alginate, lactic acid, adding sodium lactate regulates pH at about 6-7.0, sodium chloride adjusting viscosity, and constantly stirring successively adds cinnamic aldehyde oil and laurel.

embodiment 2

Primary raw material: by following weight parts, wild Oleum Camelliae 5 parts, wheat leaf 8 parts, Folium Camelliae sinensis 8 parts, Tsubaki-saponin 6 parts, Herba Rosmarini Officinalis 3 parts, sapindoside 3 parts, aescine 3 parts, Radix Pseudostellariae 3 parts, picric acid mould 3 parts, 3 parts, Rhizoma Zingiberis Recens, Radix Scutellariae 3 parts, tansy 2 parts, Pseudotsuga menziesii (Mirbel) Franco 3 parts, headdress flower Radix Stephaniae Japonicae 0.3 part, lactic acid 2 parts, lactylate salt 1 part, sodium alginate 1 part, 0.5 part, Fructus Capsici, 0.5 part, sodium chloride, essence (cinnamic aldehyde oil, laurel) are in right amount.

Preparation technology: wild Oleum Camelliae, wheat leaf, tansy, Radix Pseudostellariae second time extract is component 1, Folium Camelliae sinensis, Herba Rosmarini Officinalis, picric acid mould, Radix Scutellariae, Pseudotsuga menziesii (Mirbel) Franco, Fructus Capsici, headdress flower Radix Stephaniae Japonicae, Radix Pseudostellariae first time extract and Sucus Zingberis are component 2, Tsubaki-saponin, sapindoside, aescine is component 3, component 2 is heated to 75 DEG C, component 1 is joined in component 2, temperature remains on more than 70 DEG C, add component 3 gradually, and constantly carry out stirring and emulsifying 20min, band temperature drops to 60 DEG C and adds sodium alginate, lactic acid, adding sodium lactate regulates pH at about 6-7.0, sodium chloride adjusting viscosity, and constantly stirring successively adds cinnamic aldehyde oil and laurel.

hair washingdew physical and chemical index

1, pH is 6.5, meets the requirement of shampoo between 4.0 ~ 8.5, and the structure of shampoo is finer and smoother.

2, return to room temperature at-5 DEG C ~-15 DEG C 24h, after 40 DEG C of 24h, return to room temperature all without oil-water separation, illustrate that to have good stability cold-resistant, heat-resisting.

3, the sun-proof ability of shampoo measures: method adopts SPF vitro assay, namely the instrument and equipment of SPF external test is adopted directly to measure, the spf value of measurement result display case 1 and case 2 can reach 10,8 respectively, illustrate that there is certain anti-sunlight function, use shampoo of the present invention to have certain effect for sun-proof, the minimizing hair damage of hair.

4, using method is, is put on by shampoo in hair gently to smear to stop 2 ~ 5 minutes after having certain foam, rinses afterwards with water.Have more oil phase in case 1, be comparatively applicable to the use of dry hair people, this formula is also comparatively applicable to people's use of mixed type hair quality simultaneously; More suppression sebum secretion is contained so be comparatively suitable for the use of oily hair in case 2.

5, spumescence

Adopt Roche foam meter to measure, and contrast with daily Pantene shampoo, result is as table 1, and result represents that this product has higher foaming capacity and foam has higher stability.

Table 1 shampoo foamability and Stability Determination result

6, antibacterial experiment in vitro

Assay method, experimental group be two kinds of natural shampoo dilute 10 times afterwards for disinfectant act on mycete, the experiment of acrothesium floccosum bacterium liquid, sampling also pours into inoculation with agar, matched group does same operation after then diluting 10 times with Pantene shampoo, and cultivate 15d together under 37 DEG C of conditions, and observed result.Result is as table 2; result shows; natural shampoo of the present invention has well suppression and bactericidal effect; illustrate that shampoo well can be killed and suppresses dermatophytes and play the generation protected skin, reduce scurf, particularly with several natural plants saponin, Radix Scutellariae, Herba Rosmarini Officinalis, Rhizoma Zingiberis Recens, tansy etc. play an important role for main active component.

The bactericidal effect of table 2 shampoo

7, shampoo result of use investigation

Tried out one month continuously by 80 volunteers, the result of use of examination shampoo each side.Test event standards of grading, for being satisfied with very much 5 points, being satisfied with 4 points, general 3 points, dissatisfied 2 points, very dissatisfied 1 point, the results are shown in Table 3.Tested volunteer all represents shampoo of the present invention and feels quite pleased.

Table 3 shampoo result of use

The foregoing is only preferred embodiment of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to covering scope of the present invention.

Claims (8)

1., containing a natural shampoo for Tsubaki-saponin, it is characterized in that: primary raw material is by following weight parts: wild Oleum Camelliae 5-10 part, wheat leaf 4-8 part, Folium Camelliae sinensis 4-8 part, Tsubaki-saponin 3-8 part, Herba Rosmarini Officinalis 3-5 part, sapindoside 2-5 part, aescine 2-5 part, Radix Pseudostellariae 1-3 part, picric acid mould 1-3 part, Rhizoma Zingiberis Recens 1-5 part, Radix Scutellariae 1-3 part, tansy 1-3 part, headdress flower Radix Stephaniae Japonicae 0.1-0.5 part, lactic acid 1-3 part, Pseudotsuga menziesii (Mirbel) Franco 1-3 part, lactylate salt 1-3 part, sodium alginate 0.5-1 part, Fructus Capsici 0.5-1 part, sodium chloride 1.5-2.5 part.

2. prepare a method for the natural shampoo containing Tsubaki-saponin as claimed in claim 1, it is characterized in that: comprise the following steps:

1) by wheat leaf and the wild Oleum Camelliae lixiviate of tansy, lixiviating solution 1 is obtained;

2) by Radix Pseudostellariae distilled water lixiviate of boiling, Radix Pseudostellariae Aqueous extracts is obtained; The wild Oleum Camelliae of filtering residue carries out lixiviate, obtains lixiviating solution 2;

3) by the Aqueous extracts of picric acid mould, Radix Scutellariae, Radix Pseudostellariae, Sucus Zingberis, with Folium Camelliae sinensis, Herba Rosmarini Officinalis, Fructus Capsici, Pseudotsuga menziesii (Mirbel) Franco, headdress flower Radix Stephaniae Japonicae alcohol extract mixing, be heated to 75 DEG C, add lixiviating solution 1 and lixiviating solution 2, constant temperature 70 DEG C, add Tsubaki-saponin, sapindoside and aescine, stirring and emulsifying 20min, is cooled to 60 DEG C, adds sodium alginate, lactic acid, regulate pH=6-7 with lactylate salt, use sodium chloride adjusting viscosity.

3. method according to claim 2, is characterized in that: step 1) is by the wheat leaf of drying and crushing and fresh tansy, and lixiviate 5d in Oleum Camelliae out of office, filters.

4. method according to claim 2, is characterized in that: step 2) by the Radix Pseudostellariae of the drying and crushing distilled water lixiviate 1.5h that boils, solid-liquid ratio 1:10, filter, concentrated by rotary evaporation; The wild Oleum Camelliae of filtering residue carries out room temperature lixiviate 5d, and solid-liquid ratio is 1:6, filters.

5. method according to claim 2, is characterized in that: prepared by picric acid mould Aqueous extracts: by the picric acid mould of drying and crushing, with the distilled water extraction 30min that boils, solid-liquid ratio 1:10, decompress filter;

Prepared by Radix Scutellariae Aqueous extracts: Radix Scutellariae drying, pulverizing, 60 DEG C of distilled water ultrasonic extraction 1.5h, and solid-liquid ratio is 1:10, filters, concentrated by rotary evaporation.

6. method according to claim 2, is characterized in that: stir-frying with ginger juice is standby: first adopt method of squeezing the juice, then carry out decompress filter.

7. method according to claim 2, is characterized in that: prepared by Folium Camelliae sinensis alcohol extract: will be ground into the dry Folium Camelliae sinensis 40wt.% alcoholic solution of 20-40 object 80 DEG C of lixiviate 30min, solid-liquid ratio is 1:10, filtration under diminished pressure, revolves to steam and reclaims ethanol;

Prepared by Pseudotsuga menziesii (Mirbel) Franco alcohol extract: dry star-spangled banner Folium Pini 45wt.% alcoholic solution 80 DEG C of lixiviate 5h, and solid-liquid ratio is 1:6, decompress filter;

Prepared by capsanthol extract: Fructus Capsici drying, pulverizing, with 45wt.% alcohol solution dipping 3d, and solid-liquid ratio 1:6, decompress filter;

Herba Rosmarini Officinalis, headdress flower Radix Stephaniae Japonicae alcohol extract preparation: be dried and crushed into 10 object Herba Rosmarini Officinaliss, headdress flower Radix Stephaniae Japonicae 20wt.% alcoholic solution 60 DEG C of lixiviate 8h, solid-liquid ratio 1:6, decompress filter, revolve steam reclaim ethanol.

8. method according to claim 2, is characterized in that: the preparation of Tsubaki-saponin: after being pulverized by dry Flos Camelliae Japonicae cake, with deionized water lixiviate 3h, temperature is 100 DEG C, solid-liquid ratio 1:6, filters, concentrated by rotary evaporation;

The preparation of sapindoside: by the Fructus Sapindi Mukouossi seed coat of drying and crushing, with deionized water lixiviate 2h, temperature is 100 DEG C, and solid-liquid ratio is 1:10, filters, concentrated by rotary evaporation;

The preparation of aescine: Semen Aesculi seed drying, pulverizing, with deionized water lixiviate 3.5h, temperature is 100 DEG C, and solid-liquid ratio is 1:10, filters, concentrated by rotary evaporation.