CN1140035A - Method for preparing liquid cigarette - Google Patents
Method for preparing liquid cigarette Download PDFInfo
- Publication number
- CN1140035A CN1140035A CN 95107265 CN95107265A CN1140035A CN 1140035 A CN1140035 A CN 1140035A CN 95107265 CN95107265 CN 95107265 CN 95107265 A CN95107265 A CN 95107265A CN 1140035 A CN1140035 A CN 1140035A
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- China
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- tobacco
- tobacco juice
- liquid
- liquid cigarette
- cigarette
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Abstract
A liquid cigarette is made from tobacco through gasifying tobacco at 300-800 deg.C and 300-500 mmHg, cooling tobacco gas at 10- -20 deg.C, filtering tobacco liquid to remove tar, deeply cooling, extraction with ether, or alcohol, or chloroform, or benzene for removal of nicotine, drying, preservation treatment and compounding with essence. Said liquid cigarette features no need of ignition, no smoke and harm, and simple technology.
Description
The present invention relates to the processing of tobacco, belong to a kind of tobacco is purified and be preparation method smokeless, that do not have fiery, harmless liquid cigarette.
At present traditional cigarette only is tobacco to be processed as the cigarette of making raw material with pipe tobacco offer the smoker, owing to do not destroy many aromatic rings hydro carbons harmful substances such as nicotine Ben Peng pyrene that tobacco or pipe tobacco contain, make the smoker be not only from suffering, surrounding environment is polluted, and make other people suffer the harm of passive smoking, the fire that causes by smoking, generation is also often arranged, therefore, solve the three disasters problem of existing cigarette, must solve deep processing problem, provide a kind of smokeless tobacco, there is not fire, harmless liquid cigarette satisfies the needs and the purpose of people's smoking.
The objective of the invention is in order to solve the deep processing problem of tobacco, a kind of smokeless, preparation method of not having fire, harmless liquid cigarette is provided.
Concrete scheme of the present invention is that tobacco is vaporized, vapourizing temperature is 300～800 ℃, pressure is that tobacco is vaporized into flue gas under 300～500mmHg post, flue gas is cooled off, chilling temperature is 10～-20 ℃, flue gas is cooled to tobacco juice, tobacco juice is filtered tar, tobacco juice removes the defocused deep cooling that carries out again, tobacco juice behind the deep cooling at room temperature extracts with solvent ether or ethanol or chloroform or benzene, and the tobacco juice after the extraction is distilled, and its temperature is controlled at below 100 ℃, remove nicotine in the tobacco juice and be 10% of nicotine content in the tobacco, again the tobacco juice of removing nicotine is carried out drying, tobacco juice reaches dehydration by drying bed and concentrates and filter cleaner, and the tobacco juice after will concentrating and filter again carries out Preservation Treatment, carry out the odor type allotment then, obtain the liquid cigarette of required odor type.
The present invention has fundamentally solved the three disasters problem of cigarette, and a kind of preparation method who does not have fire, smokeless, harmless liquid cigarette is provided, and its technological process is simple, easy to operate, work efficiency is big.
Fig. 1 is a process chart of the present invention.
Referring to Fig. 1,1. vaporization 2. elementary cooling 3. filter tar 4. deep coolings 5. remove dry 7. Preservation Treatment, the 8. odor types allotment of nicotine 6. ageings.
Embodiment 1
Take by weighing 2 kilograms of tobaccos (pipe tobacco or tobacco leaf) and put into the storage compartment of gasification burner, after electric ignition, tobacco is burnt reposefully, temperature during burning is controlled at 600 ℃ ± 10 ℃, the pressure gas that produces that burns under 480 ± 5mmHg post enters cooling chamber or cooling tower by passage, and chilling temperature is at-20 ℃.Adopt the refrigeration case of refrigerator-freezer formula, cooling obtains tobacco juice, enter again in the filter tar jar and filter Jiao, filter defocused tobacco juice divides secondary to extract except that nicotine with 1000 milliliters of ethanol at every turn, in the tobacco juice after the extraction nicotine content only be in the tobacco nicotine content 1%, again tobacco juice is put into the ageing drying bed, at room temperature stopped 3 hours, at this moment obtaining tobacco juice weight is 28% of tobacco weight, the yield that is tobacco juice is 28%, carries out Preservation Treatment then, adds the antistaling agent of nontoxic antioxygen mildew-resistant, carry out the odor type allotment again, obtain the liquid cigarette of required odor type.Embodiment 2
Method is with embodiment 1, but vapourizing temperature is 500 ℃, and pressure is the 500mmHg post.Embodiment 3
Method is with embodiment 1, but vapourizing temperature is 700 ℃, and pressure is the 500mmHg post.
Claims (4)
1, a kind of preparation method of liquid cigarette, it is characterized in that: tobacco is vaporized, the temperature of vaporization is 300～800 ℃, pressure is under the 300-500mmHg post, tobacco is vaporized into flue gas, flue gas is cooled off, cooling degree is 10--20 ℃, flue gas is cooled to tobacco juice, tobacco juice is filtered tar, the defocused deep cooling that carries out again of liquid smoke filter, tobacco juice behind the deep cooling at room temperature extracts with solvent ether or ethanol or chloroform or benzene, tobacco juice after the extraction is advanced distillation, remove nicotine in the tobacco juice and be 10% of nicotine content in the tobacco, again the tobacco juice of removing nicotine is carried out drying, making tobacco juice reach dehydration by drying bed concentrates and filter cleaner, tobacco juice after will concentrating and filter again carries out Preservation Treatment, carries out the odor type allotment then, obtains the liquid cigarette of required odor type.
2, the preparation method of liquid cigarette according to claim 1 is characterized in that: vapourizing temperature is 500-700 ℃.
3, liquid cigarette preparation method according to claim 1 is characterized in that: pressure for vaporization is the 480-500mmHg post.
4, liquid cigarette preparation method according to claim 1 is characterized in that: tobacco juice stopped 3 hours under ageing drying bed room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95107265 CN1140035A (en) | 1995-07-08 | 1995-07-08 | Method for preparing liquid cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95107265 CN1140035A (en) | 1995-07-08 | 1995-07-08 | Method for preparing liquid cigarette |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1140035A true CN1140035A (en) | 1997-01-15 |
Family
ID=5076241
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 95107265 Pending CN1140035A (en) | 1995-07-08 | 1995-07-08 | Method for preparing liquid cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1140035A (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1742636B (en) * | 2004-09-02 | 2010-10-06 | 邹宝安 | Technology for producing pollution-free liquid cigarette |
| CN101626700B (en) * | 2006-11-06 | 2011-08-03 | 坚石Sci有限责任公司 | Mechanically regulated vaporization pipe |
| CN102715640A (en) * | 2011-11-17 | 2012-10-10 | 湖北中烟工业有限责任公司 | Preparation method of tobacco leaves of smokeless and fireless cigarette |
| CN104068469A (en) * | 2014-06-25 | 2014-10-01 | 湖南中烟工业有限责任公司 | Nicotine liquid with smoky aromas |
| CN104432486A (en) * | 2014-12-06 | 2015-03-25 | 中国农业科学院烟草研究所 | Device and method for manufacturing low-temperature cigarette raw material |
| CN104522877A (en) * | 2014-12-06 | 2015-04-22 | 中国农业科学院烟草研究所 | Method for manufacturing low temperature cigarette raw materials |
| CN104921287A (en) * | 2015-06-05 | 2015-09-23 | 浙江中烟工业有限责任公司 | Tobacco extract and preparing method and application thereof |
| CN104983064A (en) * | 2015-06-05 | 2015-10-21 | 浙江中烟工业有限责任公司 | Electronic cigarette liquid and preparation method thereof |
| CN105167170A (en) * | 2015-09-14 | 2015-12-23 | 浙江中烟工业有限责任公司 | Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis |
| CN105661622A (en) * | 2016-02-16 | 2016-06-15 | 中国农业科学院烟草研究所 | Nicotine liquid raw material of electronic cigarette and preparation device and method of nicotine liquid raw material |
| CN106923373A (en) * | 2016-12-30 | 2017-07-07 | 中国烟草总公司广东省公司 | A kind of mint aroma smears cigarette and preparation method thereof |
| CN109480327A (en) * | 2017-09-11 | 2019-03-19 | 湖南中烟工业有限责任公司 | A kind of preparation method and applications of tobacco purification high-temperature retorting object |
-
1995
- 1995-07-08 CN CN 95107265 patent/CN1140035A/en active Pending
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1742636B (en) * | 2004-09-02 | 2010-10-06 | 邹宝安 | Technology for producing pollution-free liquid cigarette |
| CN101626700B (en) * | 2006-11-06 | 2011-08-03 | 坚石Sci有限责任公司 | Mechanically regulated vaporization pipe |
| CN102715640A (en) * | 2011-11-17 | 2012-10-10 | 湖北中烟工业有限责任公司 | Preparation method of tobacco leaves of smokeless and fireless cigarette |
| CN102715640B (en) * | 2011-11-17 | 2014-11-26 | 湖北中烟工业有限责任公司 | Preparation method of tobacco leaves of smokeless and fireless cigarette |
| CN104068469B (en) * | 2014-06-25 | 2016-07-27 | 湖南中烟工业有限责任公司 | A kind of electronic cigarette liquid with sootiness fragrance |
| CN104068469A (en) * | 2014-06-25 | 2014-10-01 | 湖南中烟工业有限责任公司 | Nicotine liquid with smoky aromas |
| CN104432486B (en) * | 2014-12-06 | 2016-11-02 | 中国农业科学院烟草研究所 | A kind of method making low temperature cigarette raw material |
| CN104522877A (en) * | 2014-12-06 | 2015-04-22 | 中国农业科学院烟草研究所 | Method for manufacturing low temperature cigarette raw materials |
| CN104432486A (en) * | 2014-12-06 | 2015-03-25 | 中国农业科学院烟草研究所 | Device and method for manufacturing low-temperature cigarette raw material |
| CN104921287A (en) * | 2015-06-05 | 2015-09-23 | 浙江中烟工业有限责任公司 | Tobacco extract and preparing method and application thereof |
| CN104983064A (en) * | 2015-06-05 | 2015-10-21 | 浙江中烟工业有限责任公司 | Electronic cigarette liquid and preparation method thereof |
| CN105167170A (en) * | 2015-09-14 | 2015-12-23 | 浙江中烟工业有限责任公司 | Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis |
| CN105661622A (en) * | 2016-02-16 | 2016-06-15 | 中国农业科学院烟草研究所 | Nicotine liquid raw material of electronic cigarette and preparation device and method of nicotine liquid raw material |
| CN105661622B (en) * | 2016-02-16 | 2018-03-23 | 中国农业科学院烟草研究所 | A kind of tobacco juice for electronic smoke raw material and its preparation facilities and method |
| CN106923373A (en) * | 2016-12-30 | 2017-07-07 | 中国烟草总公司广东省公司 | A kind of mint aroma smears cigarette and preparation method thereof |
| CN109480327A (en) * | 2017-09-11 | 2019-03-19 | 湖南中烟工业有限责任公司 | A kind of preparation method and applications of tobacco purification high-temperature retorting object |
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| WD01 | Invention patent application deemed withdrawn after publication |