CN104068469A - Nicotine liquid with smoky aromas - Google Patents
Nicotine liquid with smoky aromas Download PDFInfo
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- CN104068469A CN104068469A CN201410287752.0A CN201410287752A CN104068469A CN 104068469 A CN104068469 A CN 104068469A CN 201410287752 A CN201410287752 A CN 201410287752A CN 104068469 A CN104068469 A CN 104068469A
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- smoky
- aromas
- nicotine liquid
- electronic cigarette
- cigarette
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Abstract
The invention discloses nicotine liquid with smoky aromas, and a method for preparing the nicotine liquid comprises the following steps of: heating under reflux for 10-40 minutes at 240-600 degrees centigrade after wrapping either tobacco powders or tobacco shreds with tin foil paper or aluminized paper, then soaking and extracting a reflux heating product wrapped with the tin foil paper or the aluminized paper for 30-60 minutes by mixed liquor of water, glycerol and ethyl alcohol at 30-40 degrees centigrade, finally preparing into the nicotine liquid; the mass-volume concentration of the reflux heating product to the mixed liquor is in the range of 1:8-12, the mass unit is g and the volume unit is ml. The nicotine liquid selects the tobacco powders, the tobacco shreds or cigarette ashes as raw materials which are distillated at a definite high temperature to obtain a substance with the smoky aromas, the aroma substance is very similar with the smoky aromas ingredient burnt in the traditional cigarette, after the nicotine liquid with the smoky aromas is atomized by an atomizer, a smoker feels that the nicotine liquid is in accordance with the traditional cigarette, namely including the smoky aromas from the burnt cigarette.
Description
Technical field
The invention belongs to electronic cigarette technical field, be specifically related to a kind of electronic cigarette liquid with sootiness fragrance.
Background technology
In recent years, along with occurring stagnating even in some developed country markets, the sales volume of conventional smoke straw-made articles declines, and the continuing to increase of many states public places in Nan Chongs ban on opium-smoking and the opium trade dynamics, the novel tobacco goods such as low temperature cigarette, smoke-free tobacco product, electronic cigarette are just in rapid rising, and the transnational tobacco companies such as the Fei Mo world, BAT, Japan Tobacco also actively research and develop and promote novel tobacco goods from strategic height.Electronic cigarette profile is similar to common cigarette, is a kind of device that nicotine solution can be vaporized into fog, smokes very by simulation, brings excitement to smoker.It is made up of elements such as lithium battery (chargeable), atomizer (heating element heater), cigarette bullets (cigarette holder of conventionally seeing).Electronic cigarette is by containing the solution atomization of nicotine, by pulmonary absorption, makes consumer obtain similar satisfaction of sucking traditional cigarette.
Electronic cigarette has reduced the injury of the health to people in the custom that meets people's smoking.Generally, electronic cigarette has following principal characters: the one, do not need burning, and greatly reduce the tar and the harmful components that produce because of burning, compare traditional cigarette harmfulness less; The 2nd, can not produce second-hand flue gas, can not exert an influence to PE, alleviate to a certain extent the contradiction of smoking and public place ban on opium-smoking and the opium trade; The 3rd, can adapt to a certain extent and meet consumer's physiological requirements.Electronic cigarette is through the development of several generations, and basically identical with traditional cigarette external form at present, taste can be realized variation, does not contain tar in electronic cigarette simultaneously, less to person injury.
Chinese patent CN201310030100.4 discloses a kind of tobacco juice for electronic smoke that utilizes discarded tobacco leaf to prepare.By discarded tobacco leaf extract 10～15%, flavouring essence for tobacco 5～10%, tobacco aromatics using 1～5%, deionized water 5～10%, glycerine 10～20%, surplus is propane diols, after mixing, makes.The disclosed atomized liquid of electronic smoke of Chinese patent 200910310536.2, with leaf tobacco extract 3-5% w/v, tobacco essence 3-5% w/v, nicotine 0-3% w/v pure water 5-10% w/v, the allotments such as propane diols 50-70% w/v form, although used leaf tobacco extract, but still be the product of simulated cigarette taste with leaf tobacco extract and the allotment of other essence and flavoring agents.Because increasing smoker starts to accept to use electronic cigarette to replace cigarette, also more and more obvious for the some shortcomings of the electronic cigarette liquid of these electronic cigarettes.Research according to investigations, electronic cigarette is compared with regular-size cigarette, although perceptual image cigarette such as shape, feel, smog, but the smog producing for these electronic cigarette liquids is aspect fragrance, taste, apart from larger, these deficiencies, have affected the quality of electronic cigarette greatly with real cigarette perceptual difference.Smoker generally reflects, electronic cigarette is compared with cigarette, although perceptual image cigarettes such as shape, feel, smog, but at the aspect such as fragrance, taste, larger with the perceptual difference distance of cigarette, the product being especially deployed into various essence and flavoring agents, they are difficult to accept or be accustomed to its fragrance and taste.These deficiencies have affected the quality of electronic cigarette greatly, are also restricting the universal and popular of electronic cigarette simultaneously.In addition, traditional leaf tobacco extract is mainly by tobacco leaf or pipe tobacco ethanol or water refluxing extraction at a certain temperature, is difficult to the sootiness fragrance in tobacco leaf to extract.
Summary of the invention
The object of the invention is to for existing tobacco juice for electronic smoke in the deficiency of the suction such as fragrance, mouthfeel aspect sensation, a kind of electronic cigarette liquid with sootiness fragrance that utilizes offal or pipe tobacco at high temperature to heat to distill out is provided.
In order to achieve the above object, technical scheme provided by the invention is:
The described electronic cigarette liquid with sootiness fragrance, its preparation method is as follows:
By offal or pipe tobacco with after masking foil or aluminium-foil paper parcel under 240-600 DEG C of conditions reflux heating 10-40min, then the reflux heating product 30-60min of the mixed liquor lixiviate masking foil of water, glycerine and ethanol or aluminium-foil paper parcel under 30-40 DEG C of conditions, obtains electronic cigarette liquid; The mass volume ratio of the mixed liquor of described reflux heating product and water, glycerine and ethanol is 1:8-12, is preferably 1:10, and in mass volume ratio, mass unit is g, and volume unit is mL.
Preferably, in the mixed liquor of described water, glycerine and ethanol, the mass percent of water is 10～15%, the mass percent of glycerine is 60～70%, the mass percent of ethanol is 10～20%.
Compared with prior art, beneficial effect of the present invention is:
The present invention heats still-process and does not use solvent, and offal or pipe tobacco are placed directly in glass container and heat, the existence inhomogeneous phenomenon of being heated, therefore the present invention uses masking foil that offal or pipe tobacco are wrapped completely, put into again round-bottomed flask and add hot reflux, offal or pipe tobacco are heated evenly, obtain having in tobacco leaf the material of sootiness fragrance, in this process, produce be charred the assorted gas materials such as taste can be less.
Electronic cigarette liquid of the present invention is taking the product of distillation of offal or pipe tobacco as main component, makes the sootiness fragrance of fragrance, mouthfeel and traditional cigarette of electronic cigarette very close.In still-process of the present invention, do not use solvent, directly, with masking foil parcel, simple to operation, the heat time is short.This electronic cigarette liquid can improve the inherent suction quality of electronic cigarette, makes electronic cigarette more approach fragrance, the taste of cigarette.
Choosing offal, pipe tobacco or cigarette ash in the present invention is in a word raw material, high temperature distillation at a certain temperature, obtain having the material of sootiness perfume (or spice), this odor type cause perfumery and in traditional cigarette combustion process, to produce sootiness fragrance component similar, this electronic cigarette liquid with sootiness odor type is after atomizer atomization, smoker feels that this electronic cigarette liquid is consistent with the impression in traditional cigarette combustion process, has the sootiness perfume (or spice) in cigarette burning process.
Detailed description of the invention
embodiment 1
The preparation method of the described electronic cigarette liquid with sootiness fragrance is as follows:
By logical 10g Yunnan Shao B
3f offal with after masking foil parcel under 240 DEG C of conditions reflux heating 10min, the reflux heating product 30-60min of the mixed liquor lixiviate masking foil parcel of the glycerine that the water that is then 15% by 100mL mass percent under 30-40 DEG C of conditions, mass percent are 65%, the ethanol that mass percent is 20%, obtains electronic cigarette liquid; The mass volume ratio of the mixed liquor of described reflux heating product and water, glycerine and ethanol is 1:10, and in mass volume ratio, mass unit is g, and volume unit is mL.
Get 1mL electronic cigarette liquid and add in atomizer, the personnel that smoke panel test that please be professional smoke panel test, and have cured tobacco leaf sootiness perfume (or spice).
embodiment 2
By 10g Zimbabwe offal with after aluminium-foil paper parcel under 350 DEG C of conditions reflux heating 10min, the reflux heating product 30-60min of the mixed liquor lixiviate aluminium-foil paper parcel of the glycerine that is then 70% by the water that is 10% by 100mL mass percent, mass percent under 30-40 DEG C of conditions, ethanol that mass percent is 20%, obtains electronic cigarette liquid; The mass volume ratio of the mixed liquor of described reflux heating product and water, glycerine and ethanol is 1:10, and in mass volume ratio, mass unit is g, and volume unit is mL.
Get 1mL electronic cigarette liquid and add in atomizer, the personnel that smoke panel test that please be professional smoke panel test, and have cured tobacco leaf sootiness perfume (or spice), also have a small amount of burning.
embodiment 3
By 10g Sangzhi B
3f with after aluminium-foil paper parcel under 500 DEG C of conditions reflux heating 10min, the reflux heating product 30-60min of the mixed liquor lixiviate aluminium-foil paper parcel of the glycerine that is then 70% by the water that is 10% by 80mL mass percent, mass percent under 30-40 DEG C of conditions, ethanol that mass percent is 20%, obtains electronic cigarette liquid; The mass volume ratio of the mixed liquor of described reflux heating product and water, glycerine and ethanol is 1:10, and in mass volume ratio, mass unit is g, and volume unit is mL.
Get 1mL electronic cigarette liquid and add in atomizer, the personnel that smoke panel test that please be professional smoke panel test, and have cured tobacco leaf sootiness perfume (or spice), also have a small amount of burning.
Claims (2)
1. an electronic cigarette liquid with sootiness fragrance, is characterized in that, described electronic cigarette liquid preparation method is as follows:
By offal or pipe tobacco with after masking foil or aluminium-foil paper parcel under 240-600 DEG C of conditions reflux heating 10-40min, then the reflux heating product 30-60min of the mixed liquor lixiviate masking foil of water, glycerine and ethanol or aluminium-foil paper parcel under 30-40 DEG C of conditions, obtains electronic cigarette liquid; The mass volume ratio of the mixed liquor of described reflux heating product and water, glycerine and ethanol is 1:8-12, and in mass volume ratio, mass unit is g, and volume unit is mL.
2. electronic cigarette liquid as claimed in claim 1, is characterized in that, in the mixed liquor of water, glycerine and ethanol, the mass percent of water is 10～15%, the mass percent of glycerine is 60～70%, the mass percent of ethanol is 10～20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410287752.0A CN104068469B (en) | 2014-06-25 | 2014-06-25 | A kind of electronic cigarette liquid with sootiness fragrance |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410287752.0A CN104068469B (en) | 2014-06-25 | 2014-06-25 | A kind of electronic cigarette liquid with sootiness fragrance |
Publications (2)
| Publication Number | Publication Date |
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| CN104068469A true CN104068469A (en) | 2014-10-01 |
| CN104068469B CN104068469B (en) | 2016-07-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410287752.0A Active CN104068469B (en) | 2014-06-25 | 2014-06-25 | A kind of electronic cigarette liquid with sootiness fragrance |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104585860A (en) * | 2015-01-15 | 2015-05-06 | 中国烟草总公司郑州烟草研究院 | Preparation method for electronic cigarette juice having baking fragrant characteristic |
| CN104489910B (en) * | 2014-11-24 | 2016-06-29 | 安徽中烟工业有限责任公司 | A kind of fire-cured tobacco type electronic cigarette liquid |
| CN108385442A (en) * | 2018-03-05 | 2018-08-10 | 滁州卷烟材料厂 | A kind of scent aluminium-foil paper |
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| CN1140035A (en) * | 1995-07-08 | 1997-01-15 | 李吉荣 | Method for preparing liquid cigarette |
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| EP2444384A1 (en) * | 2009-06-19 | 2012-04-25 | Wenbo Li | Use of neophytadiene as additive for liquid cigarette |
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| CN102972861A (en) * | 2011-09-07 | 2013-03-20 | 姚继徳 | Flue-cured tobacco type electronic cigarette solution |
| RU2489948C2 (en) * | 2011-11-17 | 2013-08-20 | Общество с ограниченной ответственностью "Научно-производственное объединение ЗДОРОВЬЕ" ("НПО ЗДОРОВЬЕ") | Smoke-generating composition for electronic devices imitating tobacco smoking, such composition production and application method |
| CN103263080A (en) * | 2013-05-23 | 2013-08-28 | 红云红河烟草(集团)有限责任公司 | Preparation method of sweet and fragrant type electric heating cigarette liquid |
| CN103462218A (en) * | 2013-09-12 | 2013-12-25 | 湖北中烟工业有限责任公司 | Cigarette producing smoke based on combination of combustion and distillation |
| CN103589514A (en) * | 2013-11-14 | 2014-02-19 | 上海烟草集团有限责任公司 | Method for preparing nose characteristic aroma components of tobacco or tobacco products |
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2014
- 2014-06-25 CN CN201410287752.0A patent/CN104068469B/en active Active
Patent Citations (10)
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| CN1140035A (en) * | 1995-07-08 | 1997-01-15 | 李吉荣 | Method for preparing liquid cigarette |
| EP2444384A1 (en) * | 2009-06-19 | 2012-04-25 | Wenbo Li | Use of neophytadiene as additive for liquid cigarette |
| RU94815U1 (en) * | 2010-03-18 | 2010-06-10 | Евгений Иванович Евсюков | ELECTRONIC CIGARETTE |
| CN102972861A (en) * | 2011-09-07 | 2013-03-20 | 姚继徳 | Flue-cured tobacco type electronic cigarette solution |
| RU2489948C2 (en) * | 2011-11-17 | 2013-08-20 | Общество с ограниченной ответственностью "Научно-производственное объединение ЗДОРОВЬЕ" ("НПО ЗДОРОВЬЕ") | Smoke-generating composition for electronic devices imitating tobacco smoking, such composition production and application method |
| CN102499465A (en) * | 2011-11-21 | 2012-06-20 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of tobacco essence |
| CN102813278A (en) * | 2012-08-09 | 2012-12-12 | 深圳瀚星翔科技有限公司 | Mixed electronic cigarette tobacco liquid |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104489910B (en) * | 2014-11-24 | 2016-06-29 | 安徽中烟工业有限责任公司 | A kind of fire-cured tobacco type electronic cigarette liquid |
| CN104585860A (en) * | 2015-01-15 | 2015-05-06 | 中国烟草总公司郑州烟草研究院 | Preparation method for electronic cigarette juice having baking fragrant characteristic |
| CN104585860B (en) * | 2015-01-15 | 2016-11-30 | 中国烟草总公司郑州烟草研究院 | There is the preparation method of the tobacco juice for electronic smoke of the fragrant feature of baking |
| CN108385442A (en) * | 2018-03-05 | 2018-08-10 | 滁州卷烟材料厂 | A kind of scent aluminium-foil paper |
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| Publication number | Publication date |
|---|---|
| CN104068469B (en) | 2016-07-27 |
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