CN105249524A - Fragrance type heating nonflammable tobacco product and preparation method thereof - Google Patents
Fragrance type heating nonflammable tobacco product and preparation method thereof Download PDFInfo
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- CN105249524A CN105249524A CN201510500587.7A CN201510500587A CN105249524A CN 105249524 A CN105249524 A CN 105249524A CN 201510500587 A CN201510500587 A CN 201510500587A CN 105249524 A CN105249524 A CN 105249524A
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Abstract
The invention relates to a fragrance type heating nonflammable tobacco product. The fragrance type heating nonflammable tobacco product includes the following materials by weight: 1 to 6 parts of tobacco extract, 0.5 to 5 parts of tobacco flavor, 0.5 to 3 parts of taste and flavor conditioning agent, 0.5 to 6 parts of fragrance type liquor, 0.5 to 15 parts of fogging agent, and 75 to 95 parts of tobacco carrier. The invention also provides a preparation method of the tobacco product. According to the invention, the tobacco product is low in danger to a human body and an environment; the tobacco extract is added to improve the tobacco flavor concentration of the tobacco product at the low temperature, and meanwhile, smoke vigor and satisfaction can be improved; the fragrance type liquor is added to allow smoke to be fragrant, prominent, elegant and exquisite, and the liquor is rich and is long in aftertaste; the content of the fogging agent is improved, so that the amount of the smoke can be assured to the greatest extent when a consumer smokes at the low temperature, and the feel more similar to the feel of the traditional cigarettes is provided.
Description
Technical field
The invention belongs to novel tobacco product technique field, be specifically related to a kind of preparation method heating not burning tobacco goods, the preparation method of especially a kind of heating containing delicate fragrance type aroma feature not burning tobacco goods.
Background technology
Traditional cigarette is sucked in the mode of lighting suction.Wherein, tobacco material carries out imperfect combustion under 700 ~ 900 DEG C of high temperature, the flue gas produced comprises nicotine, tobacco flavor composition and some harmful components etc., therefore while the consumption meeting consumer requires, produces harm to a certain degree again to the health of consumer.Under Tobacco Control is increasingly strict and consumer health realizes the overall situation day by day strengthened, change the research and development emphasis that traditional cigarette consumption pattern becomes each large tobacco enterprise.Wherein, heat the cigarette that do not burn and provide nicotine and tobacco characteristic perfume by the mode heating not burning tobacco to consumer.Correlative study shows, tobacco or tobacco extract are after (less than 500 DEG C) are heated at a lower temperature, and nicotine wherein and part aroma component shift by flue gas, for smoker provides satisfaction.New cigarette changes traditional cigarette combustion system, takes to heat incombustible mode, compared with traditional cigarette, because high-temp combustion cracking process does not occur for it, thus significantly can reduce the burst size of tar and harmful substance in main flume.Meanwhile, suction tempus intercalare cigarette core is in not heated condition, and thus it is substantially without side-stream smoke, greatly reduces the harm of second-hand-cigarette.From the disclosed patent delivered, the study hotspot of new cigarette mainly concentrates on the exploitation of smoking set particularly heater.Under cryogenic conditions, novel characteristic tobacco material preparation is that new cigarette product moves towards the key in market in the future.
Patent document CN104544553A provides a kind of delicate fragrance type tobacco juice for electronic smoke, and its raw materials by weight meter, comprises following component: leaf tobacco extract: 1-30%; Flavouring essence for tobacco: 0.5-10%; Fen-flavor type white spirit: 0.5-15%; Mouthfeel fragrance conditioning agent: 0.5-10%; Deionized water: 1-15%; Edible glycerol: 1-25%; Propane diols: surplus.A kind of delicate fragrance type tobacco juice for electronic smoke that this patent provides, the extract adopting fen-flavor type white spirit wine cellar to store sth. in a cellar tobacco leaf is raw material, and add mouthfeel fragrance conditioning agent, fen-flavor type white spirit, thus make tobacco juice not only have strong this perfume of tobacco, there is again unique delicate fragrance simultaneously.But this patent only relates to electronic cigarette, and electronic cigarette atomizing belongs to physical change process, not containing tar in the steam produced, satisfaction is poor, and fragrance level is lower, and this perfume (or spice) of tobacco is weak, there is larger gap with traditional cigarette.Tobacco extract does not carry out meticulous segmentation purification simultaneously, still also has the related component that part has a negative impact to smog in extract.The present invention with delicate fragrance type wine liquid and tobacco extract etc. for odourant ingredients, coat tobacco carrier is prepared into and heat not burning tobacco goods, there is physical change and chemical reaction process in such tobacco product in a heated condition simultaneously, not only can produce obvious haze effect, can be there is thermal cracking chemical reaction in tobacco carrier material simultaneously in heating process, produce tar, how extra this fragrant fragrance component of tobacco is provided, make it closer to traditional cigarette impression suck custom; Utilize molecular clock to carry out segmentation essence to extract to carry simultaneously, obtain that fragrance is pure, the fragrant significant essential oil of tobaccos of cigarette.Compared with electronic cigarette, heating of the present invention not burning tobacco goods solves the difficult problem that electronic cigarette is difficult to show this perfume (or spice) of tobacco largely, obtain the novel tobacco goods that a kind of less harmful, this perfume of tobacco and aroma merge mutually.
Summary of the invention
For solving prior art Problems existing and shortcoming, the invention provides a kind of delicate fragrance type and heat not burning tobacco goods, this tobacco product is in conjunction with delicate fragrance type wine liquid and tobacco extract, not only can promote this perfume of tobacco and satisfaction further, the flue gas delicate fragrance alcohol simultaneously produced is just, leisurely simple and elegant, and all tastes are coordinated, pure and sweet soft, pleasant impression is refreshing clean.
The invention provides a kind of delicate fragrance type and heat not burning tobacco goods, be prepared from by the raw material comprising following weight portion: tobacco extract 1 ~ 6 part, flavouring essence for tobacco 0.5 ~ 5 part, mouthfeel fragrance conditioning agent 0.5 ~ 3 part, delicate fragrance type wine liquid 0.5 ~ 6 part, Alevaire 0.5 ~ 15 part, 75 ~ 95 parts, tobacco carrier.
Preferably, described tobacco product is prepared from by the raw material comprising following weight portion: tobacco extract 1 ~ 5.5 part, flavouring essence for tobacco 1 ~ 5 part, mouthfeel fragrance conditioning agent 0.5 ~ 2 part, delicate fragrance type wine liquid 1 ~ 6 part, Alevaire 2 ~ 12 parts, 76 ~ 87 parts, tobacco carrier.
Further preferably, described tobacco product is prepared from by the raw material comprising following weight portion: tobacco extract 2 ~ 4 parts, flavouring essence for tobacco 1 ~ 3 part, mouthfeel fragrance conditioning agent 0.5 ~ 1.5 part, delicate fragrance type wine liquid 2 ~ 4 parts, Alevaire 7 ~ 9 parts, 80 ~ 85 parts, tobacco carrier.
Tobacco extract of the present invention is the extract of tobacco material.Described tobacco material be preferably flue-cured tobacco, air-curing of tobacco leaves or suncured tabacco in one or more.Described flue-cured tobacco is divided into Luzhou-flavor, flat-flavor and delicate fragrance type, is preferably delicate fragrance type flue-cured tobacco; Described air-curing of tobacco leaves is selected from one or more the combination in burley tobaccos or Maryland, is preferably burley tobaccos; Described suncured tabacco is selected from one or more the combination in Turkish tobaccos, Dark sun-cured, Sun cured tobacco or Nicotiniana rustica, is preferably Turkish tobaccos.Tobacco extract of the present invention is preferably the extract of delicate fragrance type flue-cured tobacco, burley tobaccos or Turkish tobaccos.
Tobacco extract of the present invention is extracted by the method comprised the following steps and forms: get tobacco material, grinding and sieving, add solvent and mix, ultrasonic extraction, after sedimentation, filtration, reduced pressure concentration, molecular clock, to obtain final product.
Described tobacco extract preferably stores sth. in a cellar modulation and forms in wine cellar, make its taste more alcohol and.The water content of described tobacco material is preferably 8 ~ 15%.The order number of described grinding and sieving is preferably 40 ~ 100 orders, more preferably 40 ~ 60 orders.The amount ratio of described tobacco material and solvent is preferably 1g:2 ~ 5ml.Described solvent is preferably one or both mixing in deionized water or ethanol.Described ultrasonic extraction is preferably: at 30 ~ 60 DEG C, extracts 2 ~ 5h with supersonic frequency 30 ~ 50KHz.The object of described filtration, for removing residue, retaining filtrate, is specially and adopts funnel and filtering with microporous membrane successively.The aperture of described miillpore filter is preferably not more than 0.5 μm, more preferably 0.45 μm.Gained reduced pressure concentration preferably carries out reduced pressure concentration at 50 ~ 90 DEG C.Described molecular clock is specially: with the speed charging of 2 ~ 10ml/min, under the condition of vacuum 15 ~ 20Pa, rotating speed 300 ~ 400r/min, heating-up temperature 60 ~ 80 DEG C, chilling temperature 10 ~ 20 DEG C, carry out molecular clock.
Alevaire of the present invention is selected from the ester derivative of polyalcohol or polyalcohol; Described polyalcohol comprises propane diols, triethylene glycol, 1,3-BDO, glycerine, DPG, polyethylene glycol; The ester derivative of described polyalcohol comprise glycerine single, two, triacetate, polycarboxylic single, two, polynary ester; Described Alevaire is preferably polyalcohol, more preferably glycerine.
Tobacco carrier of the present invention can be selected from flue-cured tobacco, burley tobaccos, Turkish tobaccos or Sun cured tobacco any one or a few mixing, is preferably flue-cured tobacco, burley tobaccos or Turkish tobaccos.
Described tobacco carrier specifically comprises pipe tobacco, cut tobacco, stem or reconstituted tobacoo; Be preferably tissue looseness and there is the pipe tobacco of good suction capacity, the expansive cut tobacco formed through expansion process or expanded cut stem or the reconstituted tobacoo that has compared with the strong adsorption capacity of Large ratio surface sum.
As preferred version of the present invention, described tobacco carrier is positioned in wine cellar and stores sth. in a cellar, and refines at least more than half a year, the flavor matter of white wine is infiltrated in tobacco material equably, make its taste more alcohol and.
The present invention can select commercially available delicate fragrance type wine liquid to described delicate fragrance type wine liquid, specifically can be selected from any one or multiple combination in the fen-flavor type white spirits such as Fenyang wine, Erguotou wine, Baofeng wine, Green Bamboo Leaf Liquor, Yutang wine brewed in spring, six bent cordiales, the Lushui River wine, Jinmen Chinese sorghum, cattle pen mountain, Xing Jingfang, Yanggao wine, eight or eight tunnels.
Preferably, delicate fragrance type of the present invention heats not burning tobacco goods and is prepared from by the raw material comprising following weight portion: delicate fragrance type flue-cured tobacco extract 2 ~ 4 parts, flavouring essence for tobacco 1 ~ 3 part, mouthfeel fragrance conditioning agent 0.5 ~ 1.5 part, 2 ~ 4 parts, Fenyang wine, glycerine 7 ~ 9 parts, delicate fragrance type flue-cured tobacco reconstituted tobacoo 80 ~ 85 parts;
Wherein, described flue-cured tobacco extract is prepared from by following steps: the cured tobacco leaf of modulation is stored sth. in a cellar in wine cellar of learning from else's experience, 40 ~ 60 mesh sieves are crossed after pulverizer is pulverized, mix with ethanol with 1g/2 ~ 5ml, with frequency 30 ~ 50kHz ultrasonic extraction 2 ~ 5h under 30 ~ 60 DEG C of conditions, after standing sedimentation, use the filtering with microporous membrane in sand core funnel and 0.45 μm, aperture successively, reduced pressure concentration at 50 ~ 90 DEG C, with the charging rate of 2 ~ 10ml/min, at vacuum 15 ~ 20Pa, rotating speed 300 ~ 400r/min, heating-up temperature 60 ~ 80 DEG C, molecular clock is carried out under the condition that chilling temperature is 10 ~ 20 DEG C, obtain flue-cured tobacco essential oil, i.e. flue-cured tobacco extract.
The present invention does not have special restriction to the kind of described flavouring essence for tobacco and source, adopts flavouring essence for tobacco well known to those skilled in the art.Described flavouring essence for tobacco can be selected from vanillic aldehyde, benzoic acid, phenylacetic acid, Peru's medicinal extract, tree moss concrete, caryophyllus oil, anisic aldehyde, pineapple ketone, phenmethylol, benzyl carbinol, toluene ethyl ketone, ethyl phenylacetate, small bell plum medicinal extract, phenylacetaldehyde, acetophenone, angelica lactone, method Buddhist nun ketone, dodecoic acid, isovaleric acid, benzyl butyrate, octanol, Tetramethylpyrazine, citric acid, ethyl maltol, sclareol, Clary sage lactone, dragon saliva ether, davana oil, petit grain oil, valerian oil, vetiver oil, labdanum concrete, storax medicinal extract, angelica grosseserrata root tincture, tart fruit liquid extract, tamarind medicinal extract, yellow chamomile medicinal extract, vanilla medicinal extract, fig medicinal extract, cider, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone, palmitic acid, one or more in geranyl acetone.The solvent of described flavouring essence for tobacco can select in propane diols, ethanol, water one or more.Described flavouring essence for tobacco all commercially.
As one of preferred version of the present invention, described flavouring essence for tobacco is mixed by the uniform composition of following weight portion: vanillic aldehyde 1 part, 0.2 part, benzoic acid, phenylacetic acid 0.5 part, Peru's medicinal extract 1 part, tree moss concrete 5 parts, caryophyllus oil 0.5 part, anisic aldehyde 0.5 part, 0.5 part, pineapple aldehyde, benzyl carbinol 0.4 part, toluene ethyl ketone 0.2 part, ethyl phenylacetate 0.2 part, ethanol 25 parts and propane diols 65 parts.
As one of preferred version of the present invention, described flavouring essence for tobacco is mixed by the uniform composition of following weight portion: Megastigmatrienone 4 parts, ethyl maltol 3 parts, Ethyl vanillin 0.5 part, palmitic acid 0.5 part, dihydroactinidiolide 0.2 part, dimethyl succinate isovaleric acid 0.1 part, alpha, beta-lonone 0.5 part, phenmethylol 0.2 part, vanilla medicinal extract 2 parts, 4 parts of imperial saliva ethers and propane diols 85 parts.
Mouthfeel fragrance conditioning agent of the present invention is preferably ethyl acetate, ethyl lactate, ethyl propionate, ethyl butyrate, ethyl valerate, ethyl hexanoate, cognac oil, ethyl caprilate, 2-hydroxyl calculates ethyl ester, diethyl succinate, 2 Methylpropionic acid ethyl ester, certain herbaceous plants with big flowers acetoacetic ester, ethyl undecanoate, propyl acetate, normal propyl alcohol, 2-methylpropanol, isobutanol, n-butanol, isoamyl alcohol, acetaldehyde, acetal, hexanal, aldehyde C-9, certain herbaceous plants with big flowers aldehyde, acetic acid, propionic acid, 2 Methylpropionic acid, butyric acid, caproic acid, phenmethylol, 2 phenylethyl alcohol, ethyl benzoate, ethyl cinnamate, 2-ethyl phenylacetate, phenyl ethyl butyrate, one or more combination in 4-methyl guaiacol and 4 etc.
As one of preferred version of the present invention, described mouthfeel fragrance conditioning agent is mixed by the uniform composition of following weight portion: 50.16 parts, ethyl acetate, ethyl lactate 23.61 parts, ethyl propionate 0.08 part, ethyl hexanoate 0.13 part, ethyl caprilate 0.13 part, ethyl undecanoate 1.22 parts, 2 Methylpropionic acid ethyl ester 1.93 parts, propyl acetate 0.26 part, normal propyl alcohol 6.22 parts, 2-methylpropanol 2.69 parts, isoamyl alcohol 8.30 parts, 2.42 parts, acetaldehyde, acetal 0.12 part, hexanal 0.01 part, acetic acid 2.65 parts, 2 Methylpropionic acid 0.02 part, phenmethylol 0.03 part, ethyl benzoate 0.01 part and 2-ethyl phenylacetate 0.01 part.
As one of preferred version of the present invention, described mouthfeel fragrance conditioning agent is mixed by the uniform composition of following weight portion: 40.20 parts, ethyl acetate, ethyl lactate 24.90 parts, ethyl butyrate 0.04 part, ethyl hexanoate 0.02 part, ethyl caprilate 0.0 part, 2-hydroxy ethyl caproate 0.08 part, diethyl succinate 0.06 part, propyl acetate 0.49 part, normal propyl alcohol 9.07 parts, 2-methylpropanol 0.73 part, isoamyl alcohol 6.81 parts, n-butanol 0.08 part, 4.02 parts, acetaldehyde, acetal 3.60 parts, acetic acid 9.61 parts, propionic acid 0.15 part, benzaldehyde 0.10 part, ethyl cinnamate 0.01 part.
The preparation method of the second object of the present invention for providing a kind of delicate fragrance type to heat not burning tobacco goods.
Described method comprises following concrete steps:
(1) by consumption part, tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent, delicate fragrance type wine liquid and Alevaire are mixed, obtain mixture;
(2) with sprayer, described mixture is evenly sprayed on tobacco carrier, leaves standstill under constant temperature and humidity condition.
Described step (2) is preferably: be evenly sprayed on tobacco carrier with sprayer by described mixture, under temperature 21 ~ 23 DEG C, relative humidity 58 ~ 62% condition, leaves standstill 40 ~ 60h.Be more preferably and leave standstill balance under the condition of opposing seal.
Compared with prior art, the invention provides the preparation method that a kind of delicate fragrance type heats not burning tobacco goods and there is following benefit: (1) uses and heats the tobacco product that not burning tobacco goods can provide a kind of more less harmful; (2) by adding tobacco extract, under increase cryogenic conditions, this aromatic degree of tobacco of tobacco product, improves strength and the satisfaction of flue gas simultaneously; (3) by adding delicate fragrance type wine liquid, flue gas delicate fragrance is given prominence to, quiet and tastefully laid out exquisiteness, wine body enriches mellow, long times of aftertaste; (4) by improving the content of Alevaire, ensure that amount of smoke when consumer aspirates under cryogenic conditions greatly, a kind of impression more close with traditional cigarette is provided; (5) tobacco juice for electronic smoke that prior art provides is atomized not containing tar in the steam produced, and satisfaction is poor, and this perfume (or spice) of tobacco is weak.Comparatively speaking, delicate fragrance type of the present invention heats not burning tobacco goods and physical change and chemical reaction occurs in a heated condition simultaneously, not only can produce obvious haze effect, can there is thermal cracking chemical reaction in tobacco carrier material simultaneously in low-temperature heat process, produces tar, how extra this fragrant fragrance component of tobacco is provided, be aided with the atomization process of physics, make flue gas true to nature, this perfume of tobacco is remarkable, satisfaction is good, make it closer to traditional cigarette impression suck custom; Utilize molecular clock to carry out segmentation essence to extract to carry simultaneously, obtain that fragrance is pure, the fragrant significant essential oil of tobaccos of cigarette.Compared with electronic cigarette technology, the present invention shows clear superiority in simulation traditional cigarette.
Detailed description of the invention
Set forth the present invention further below in conjunction with specific embodiment, should be understood that these embodiments are only not used in for illustration of the present invention and limit the scope of the invention.
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
Embodiment 1
A kind of delicate fragrance type heats not burning tobacco goods, is prepared from: delicate fragrance type flue-cured tobacco extract 3kg, flavouring essence for tobacco 2kg, mouthfeel fragrance conditioning agent 1kg, Fenyang wine 3kg, glycerine 8kg, delicate fragrance type flue-cured tobacco reconstituted tobacoo 83kg by following raw material;
Described flue-cured tobacco extract is prepared from by following steps: the cured tobacco leaf of modulation is stored sth. in a cellar in wine cellar of learning from else's experience, 40 ~ 60 mesh sieves are crossed after pulverizer is pulverized, mix with ethanol with 1g/3ml, with frequency 40kHz ultrasonic extraction 4h under 50 DEG C of conditions, after standing sedimentation, use the filtering with microporous membrane in sand core funnel and 0.45 μm, aperture successively, reduced pressure concentration at 70 DEG C, with the charging rate of 5ml/min, under the condition of vacuum 18Pa, rotating speed 350r/min, heating-up temperature 80 DEG C, chilling temperature 10 DEG C, carry out molecular clock, obtain flue-cured tobacco essential oil, i.e. flue-cured tobacco extract;
Described flavouring essence for tobacco is mixed by the uniform composition of following percentage by weight: vanillic aldehyde 1%, benzoic acid 0.2%, phenylacetic acid 0.5%, Peru's medicinal extract 1.0%, tree moss concrete 5%, caryophyllus oil 0.5%, anisic aldehyde 0.5%, pineapple aldehyde 0.5%, benzyl carbinol 0.4%, toluene ethyl ketone 0.2%, ethyl phenylacetate 0.2%, ethanol 25% and propane diols 65%;
Described mouthfeel fragrance conditioning agent is mixed by the uniform composition of following percentage by weight: ethyl acetate 50.16%, ethyl lactate 23.61%, ethyl propionate 0.08%, ethyl hexanoate 0.13%, ethyl caprilate 0.13%, ethyl undecanoate 1.22%, 2 Methylpropionic acid ethyl ester 1.93%, propyl acetate 0.26%, normal propyl alcohol 6.22%, 2-methylpropanol 2.69%, isoamyl alcohol 8.30%, acetaldehyde 2.42%, acetal 0.12%, hexanal 0.01%, acetic acid 2.65%, 2 Methylpropionic acid 0.02%, phenmethylol 0.03%, ethyl benzoate 0.01% and 2-ethyl phenylacetate 0.01%.
Described delicate fragrance type heats not burning tobacco goods and is prepared from by following steps: flue-cured tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent, Fenyang wine and glycerine are mixed according to consumption, obtain mixture; With laryngeal spray, described mixture is evenly sprayed on flue-cured tobacco reconstituted tobacoo, in the climatic chamber of temperature 21 ~ 23 DEG C, relative humidity 58 ~ 62%, leaves standstill balance 48h, to obtain final product.
Embodiment 2
A kind of delicate fragrance type heats not burning tobacco goods, is prepared from: burley tobaccos extract 5.5kg, flavouring essence for tobacco 3.5kg, mouthfeel fragrance conditioning agent 2kg, Baofeng wine 1kg, glycerine 12kg, burley tobaccos reconstituted tobacoo 76kg by following raw material;
Described burley tobaccos extract is prepared from by following steps: the burley tobaccos tobacco leaf of modulation is stored sth. in a cellar in wine cellar of learning from else's experience, 40 ~ 60 mesh sieves are crossed after pulverizer is pulverized, mix with ethanol with 1g/3ml, with frequency 30kHz ultrasonic extraction 4h under 45 DEG C of conditions, after standing sedimentation, use the filtering with microporous membrane in sand core funnel and 0.45 μm, aperture successively, reduced pressure concentration at 70 DEG C, with the charging rate of 8ml/min, at vacuum 20Pa, rotating speed 400r/min, heating-up temperature 80 DEG C, molecular clock is carried out under the condition that chilling temperature is 10 DEG C, obtain burley tobaccos essential oil, i.e. burley tobaccos extract,
Described flavouring essence for tobacco is with embodiment 1;
Described mouthfeel fragrance conditioning agent is with embodiment 1.
Described delicate fragrance type heats the preparation process of not burning tobacco goods with embodiment 1.
Embodiment 3
A kind of delicate fragrance type heats not burning tobacco goods, is prepared from: Turkish tobaccos extract 1kg, flavouring essence for tobacco 2kg, mouthfeel fragrance conditioning agent 0.5kg, Jinmen Chinese sorghum 4kg, glycerine 5.5kg, Turkish tobaccos expanded cut tobacco 87kg by following raw material;
The preparation method of described Turkish tobaccos extract is with embodiment 1;
Described flavouring essence for tobacco is mixed by the uniform composition of following percentage by weight: Megastigmatrienone 4%, ethyl maltol 3%, Ethyl vanillin 0.5%, palmitic acid 0.5%, dihydroactinidiolide 0.2%, dimethyl succinate isovaleric acid 0.1%, alpha, beta-lonone 0.5%, phenmethylol 0.2%, vanilla medicinal extract 2%, 4% imperial saliva ether and propane diols 85%;
Described mouthfeel fragrance conditioning agent is mixed by the uniform composition of following percentage by weight: ethyl acetate 40.20%, ethyl lactate 24.90%, ethyl butyrate 0.04%, ethyl hexanoate 0.02%, ethyl caprilate 0.03%, 2-hydroxy ethyl caproate 0.08%, diethyl succinate 0.06%, propyl acetate 0.49%, normal propyl alcohol 9.07%, 2-methylpropanol 0.73%, isoamyl alcohol 6.81%, n-butanol 0.08%, acetaldehyde 4.02%, acetal 3.60%, acetic acid 9.61%, propionic acid 0.15%, benzaldehyde 0.10%, ethyl cinnamate 0.01%.
Described delicate fragrance type heats the preparation process of not burning tobacco goods with embodiment 1.
Embodiment 4
A kind of delicate fragrance type heats not burning tobacco goods, is prepared from: Turkish tobaccos extract 3kg, flavouring essence for tobacco 5kg, mouthfeel fragrance conditioning agent 2kg, Erguotou wine 6kg, glycerine 2kg, Turkish tobaccos expanded cut tobacco 82kg by following raw material;
The preparation process method of described Turkish tobaccos extract is with embodiment 1;
Described flavouring essence for tobacco is with embodiment 3;
Described mouthfeel fragrance conditioning agent is with embodiment 3;
Described delicate fragrance type heats the preparation process of not burning tobacco goods with embodiment 1.
Embodiment 5
Compared with embodiment 1, difference is only, replaces glycerine as Alevaire with polyethylene glycol.
Comparative example 1
Compared with embodiment 1, difference is only, is prepared from: flavouring essence for tobacco 2kg, mouthfeel fragrance conditioning agent 1kg, Fenyang wine 3kg, glycerine 8kg, flue-cured tobacco reconstituted tobacoo 86kg by following raw material.
Comparative example 2
Compared with embodiment 1, difference is only, is prepared from: the flue-cured tobacco extract 3kg that embodiment 1 provides, flavouring essence for tobacco 2kg, mouthfeel fragrance conditioning agent 1kg, glycerine 8kg, flue-cured tobacco reconstituted tobacoo 86kg by following raw material.
Comparative example 3
Compared with embodiment 1, difference is only, is prepared from: the flue-cured tobacco extract 3kg that embodiment 1 provides, mouthfeel fragrance conditioning agent 1kg, Fenyang wine 3kg, flue-cured tobacco reconstituted tobacoo 93kg by following raw material.
Comparative example 4
Compared with embodiment 1, difference is only, described tobacco product is prepared from by following raw material: delicate fragrance type flue-cured tobacco extract 1kg, flavouring essence for tobacco 0.5kg, mouthfeel fragrance conditioning agent 0.5kg, Fenyang wine 0.5kg, glycerine 8kg, delicate fragrance type flue-cured tobacco reconstituted tobacoo 100kg;
The composition of described flavouring essence for tobacco and mouthfeel fragrance conditioning agent is with embodiment 1.
Comparative example 5
Compared with embodiment 1, difference is only, described tobacco product is prepared from by following raw material: delicate fragrance type flue-cured tobacco extract 6kg, flavouring essence for tobacco 5kg, mouthfeel fragrance conditioning agent 3kg, Fenyang wine 6kg, glycerine 8kg, delicate fragrance type flue-cured tobacco reconstituted tobacoo 60kg;
The composition of described flavouring essence for tobacco and mouthfeel fragrance conditioning agent is with embodiment 1.
Comparative example 6
A kind of delicate fragrance type tobacco juice for electronic smoke, is prepared from by following raw material: delicate fragrance type flue-cured tobacco extract 3kg, flavouring essence for tobacco 2kg, mouthfeel fragrance conditioning agent 1kg, Fenyang wine 3kg, glycerine 8kg;
Described delicate fragrance type tobacco juice for electronic smoke is prepared from by following steps: mixed by each raw material by consumption, and in stirred at ambient temperature 30min, each component is fully mixed, to obtain final product.
Experimental example
The delicate fragrance type that each embodiment and comparative example provide is heated not burning tobacco goods to add heating to and do not burn in low temperature cigarette device and carry out sensory effects evaluation respectively.
In the present invention, burning tobacco goods sensory effects evaluation method is not as described below in electrical heating, comprises the following steps:
(1) be provided with 7 indexs, comprise excitant, strength, harmony, fragrance, assorted gas, pleasant impression and the amount of being fuming, and give different points according to the Different Effects degree of indices to electrical heating not burning tobacco goods aesthetic quality; Each index specifically refers to:
Excitant: the discomfort that flue gas comprises oral cavity to sense organ, throat and nasal cavity produce is subject to;
Strength: the physiological strength of flue gas, becomes positive correlation with the content of nicotine;
Harmony: tobacco product is filled a prescription, and flue gas mixes each component in combustion process, harmony is consistent heating not;
Fragrance: the fragrant breath that flue gas has, comprises aroma quality and perfume quantity double meaning; Wherein aroma quality refers to the quality of fragrance and fine and smooth degree, and perfume quantity refers to a plentiful and saturating degree of fragrance;
Assorted gas: breath beastly in flue gas;
Pleasant impression: after flue gas spues, the taste perception that flue gas particle left behind, comprises clean degree and level of comfort;
The amount of being fuming: the number of exhaust gas volumn;
(2) member of smoking of 9 people is set, adopts the overall method of smokeing panel test that circulates: when smokeing panel test, flue gas direct oral cavity sucks, throat swallows, nasal cavity is breathed out, and experienced, catches the overall process of smoke transportation; Aesthetic quality's overall merit adopts hundred-mark system point system, every evaluation index by five points, very, 15 or four ten point system scorings, and the score value summation of 7 sensory quality assessment indexs is a percentage; Described hundred-mark system point system, by the different score values of different sensory quality assessment index, embodies the different weights of different sensory quality assessment index, can reflect that every sensory quality assessment index is to the influence degree heating not burning tobacco product property comprehensively; Described aesthetic quality's score value is higher, and described heating not burning tobacco product property is better, and specifically, described evaluation index score value is as shown in table 1;
Table 1: the score value of sensory quality assessment index
(3) evaluation method: according to the evaluation index in table 1 and score value, member of smoking tackles each evaluation index and carries out sensory quality assessment, and records its evaluation result, and the minimum score unit of score value is 0.5;
(4) result statistics: remove minimum point and a best result in the sensory quality assessment result of all members of smoking, calculate the arithmetic mean of instantaneous value of remaining effective single item evaluation index score value, result retains two-decimal, the sensory quality assessment comprehensive grading of last not burning tobacco goods is the arithmetic mean of instantaneous value sums calculating the scoring of each single index, obtain total score, result retains a decimal.
By each embodiment and each comparative example gained not burning tobacco goods be added on and do not carry out sensory quality assessment in burning tobacco goods smoking set.Concrete evaluation result is in table 2, and in table 2, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided.
Table 2: sensory effects evaluation result
The sensory effects evaluation result of table 2 shows: it is less to throat irritation that a kind of delicate fragrance type provided by the invention heats the flue gas that not burning tobacco goods produce under low-temperature heat condition, fragrance is remarkable, this perfume of tobacco and the harmony of delicate fragrance type aroma, just, pure and sweet soft, sweet profit is tasty and refreshing for delicate fragrance alcohol simultaneously, unique style, satisfaction is good, and pleasant impression is purer comfortable, the amount of being fuming abundance.
Meanwhile, compared with tobacco juice for electronic smoke, heat the not overall fragrance of burning tobacco goods more horn of plenty coordination, strength foot, assorted gas celebrating, good after-taste, better simulates traditional cigarette effect.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (10)
1. a delicate fragrance type heats not burning tobacco goods, it is characterized in that, be prepared from by the raw material comprising following weight portion: tobacco extract 1 ~ 6 part, flavouring essence for tobacco 0.5 ~ 5 part, mouthfeel fragrance conditioning agent 0.5 ~ 3 part, delicate fragrance type wine liquid 0.5 ~ 6 part, Alevaire 0.5 ~ 15 part, 75 ~ 95 parts, tobacco carrier.
2. tobacco product according to claim 1, it is characterized in that, described tobacco product is prepared from by the raw material comprising following weight portion: tobacco extract 1 ~ 5.5 part, flavouring essence for tobacco 1 ~ 5 part, mouthfeel fragrance conditioning agent 0.5 ~ 2 part, delicate fragrance type wine liquid 1 ~ 6 part, Alevaire 2 ~ 12 parts, 76 ~ 87 parts, tobacco carrier.
3. tobacco product according to claim 1 and 2, is characterized in that, described tobacco extract is the extract of tobacco material; Be preferably one or more the extract in flue-cured tobacco, air-curing of tobacco leaves or suncured tabacco; The more preferably extract of delicate fragrance type flue-cured tobacco, burley tobaccos or Turkish tobaccos.
4. tobacco product according to claim 3, is characterized in that, described tobacco extract is extracted by the method comprised the following steps and forms: get tobacco material, grinding and sieving, adds solvent and mixes, ultrasonic extraction, after sedimentation, filtration, reduced pressure concentration, molecular clock, to obtain final product;
Preferably extracted by the method comprised the following steps and form: get tobacco material, 40 ~ 100 mesh sieves are crossed after pulverizer is pulverized, mix with ethanol with 1g/2 ~ 5ml, with frequency 30 ~ 50kHz ultrasonic extraction 2 ~ 5h under 30 ~ 60 DEG C of conditions, after standing sedimentation, the filtering with microporous membrane of 0.5 μm is not more than successively with sand core funnel and aperture, reduced pressure concentration at 50 ~ 90 DEG C, with the charging rate of 2 ~ 10ml/min, at vacuum 15 ~ 20Pa, rotating speed 300 ~ 400r/min, heating-up temperature 60 ~ 80 DEG C, molecular clock is carried out under the condition that chilling temperature is 10 ~ 20 DEG C, obtain.
5. the tobacco product according to Claims 1 to 4 any one, is characterized in that, described Alevaire is selected from the ester derivative of polyalcohol or polyalcohol; Be preferably glycerine.
6. the tobacco product according to Claims 1 to 5 any one, is characterized in that, described tobacco carrier is pipe tobacco, cut tobacco, stem or reconstituted tobacoo;
Be preferably the pipe tobacco of tissue looseness, expansive cut tobacco, expanded cut stem or reconstituted tobacoo.
7. tobacco product according to claim 6, is characterized in that, described tobacco carrier to be selected from flue-cured tobacco, burley tobaccos, Turkish tobaccos or Sun cured tobacco any one or a few mixing; Be preferably flue-cured tobacco, burley tobaccos or Turkish tobaccos.
8. tobacco product according to claim 1, it is characterized in that, described flavouring essence for tobacco is selected from vanillic aldehyde, benzoic acid, phenylacetic acid, Peru's medicinal extract, tree moss concrete, caryophyllus oil, anisic aldehyde, pineapple ketone, phenmethylol, benzyl carbinol, toluene ethyl ketone, ethyl phenylacetate, small bell plum medicinal extract, phenylacetaldehyde, acetophenone, angelica lactone, method Buddhist nun ketone, dodecoic acid, isovaleric acid, benzyl butyrate, octanol, Tetramethylpyrazine, citric acid, ethyl maltol, sclareol, Clary sage lactone, dragon saliva ether, davana oil, petit grain oil, valerian oil, vetiver oil, labdanum concrete, storax medicinal extract, angelica grosseserrata root tincture, tart fruit liquid extract, tamarind medicinal extract, yellow chamomile medicinal extract, vanilla medicinal extract, fig medicinal extract, cider, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone, palmitic acid, one or more in geranyl acetone, the solvent of described flavouring essence for tobacco be selected from propane diols, ethanol, water one or more,
Described delicate fragrance type wine liquid be selected from Fenyang wine, Erguotou wine, Baofeng wine, Green Bamboo Leaf Liquor, Yutang wine brewed in spring, six bent cordiales, the Lushui River wine, Jinmen Chinese sorghum, cattle pen mountain, Xing Jingfang, Yanggao wine, eight or eight tunnels one or more;
Described mouthfeel fragrance conditioning agent is selected from ethyl acetate, ethyl lactate, ethyl propionate, ethyl butyrate, ethyl valerate, ethyl hexanoate, cognac oil, ethyl caprilate, 2-hydroxyl calculates ethyl ester, diethyl succinate, 2 Methylpropionic acid ethyl ester, certain herbaceous plants with big flowers acetoacetic ester, ethyl undecanoate, propyl acetate, normal propyl alcohol, 2-methylpropanol, isobutanol, n-butanol, isoamyl alcohol, acetaldehyde, acetal, hexanal, aldehyde C-9, certain herbaceous plants with big flowers aldehyde, acetic acid, propionic acid, 2 Methylpropionic acid, butyric acid, caproic acid, phenmethylol, 2 phenylethyl alcohol, ethyl benzoate, ethyl cinnamate, 2-ethyl phenylacetate, phenyl ethyl butyrate, one or more in 4-methyl guaiacol and 4.
9. according to claim 1 ~ 8 any one, delicate fragrance type heats the preparation method of not burning tobacco goods, it is characterized in that, comprises the following steps:
(1) by consumption part, tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent, delicate fragrance type wine liquid and Alevaire are mixed, obtain mixture;
(2) with sprayer, described mixture is evenly sprayed on tobacco carrier, leaves standstill under constant temperature and humidity condition.
10. preparation method according to claim 9, it is characterized in that, described step (2) is specially: be evenly sprayed on tobacco material by described mixture with sprayer, under temperature 21 ~ 23 DEG C, relative humidity 58 ~ 62% condition, leave standstill 40 ~ 60h.
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