RU2606669C2 - Method for producing alloy consisting of titanium, iron, chromium and zirconium, from aqueous suspension of particles of ores containing titanium, iron, chromium and zirconium compounds, and device therefor - Google Patents

Abstract

FIELD: metallurgy.

SUBSTANCE: invention relates to a method of preparing an alloy consisting of titanium, iron, chromium and zirconium, from an aqueous suspension of particles of ores containing compounds of said elements, and a device for its implementation. Method comprises placing a starting material in device, generating therein physical fields, recovery of metals with accumulation of end product and discharge thereof from device. Alloy is formed in form of ring columnar crystalline form in form of alloy consisting of above metals. Physical fields acting on used raw materials are rack magnetic fields. Reduction is carried out when supplying to material and its layers jets of compressed air with component-reducing agent, represented by carbon in form of a jet.

EFFECT: simple process and high operational reliability.

2 cl, 5 dwg, 2 ex

Description

The invention relates to those areas of non-ferrous metallurgy in which titanium-containing metal alloys are processed, as well as others, which are part of the final products synthesized using such technologies, elements that are present in the form of corresponding compounds in the raw materials used in their subsequent processing materials, as well as to devices providing the ability to implement the above methods.

At present, a technical solution is known, in the implementation of which a multicomponent titanium alloy containing in its composition, including the above elements, is zirconium (aluminum - 5-6.8%; zirconium - 5-7%, vanadium - 1- 2.5%; copper 0.01-0.12%; nickel 0.01-0.12% titanium, the rest up to 100%) is obtained by crystallization from a melt containing all previously noted components (a.s. 4788255 “Alloy based on titanium”, C22C 14/00, USSR; 05.23.92).

The introduction of 5-7% zirconium into the alloy allows a sufficiently high degree of efficiency to produce the necessary increase in the strength characteristics of the structural elements made using this material, which are part of the prefabricated assemblies, which, in turn, are used in the corresponding heavily loaded mechanisms of various aircraft.

However, based on all the information set forth in the description of this invention, the finished final product obtained in accordance with this known technology does not have sufficiently pronounced indices of intrinsic heat resistance. The need to use the melts of the latter metals in the preparation of this multicomponent alloy, among other things, inevitably leads to an increase in the costs of the “technological” electrical energy used in the manufacturing process.

All of the above has a negative impact on all technical and economic indicators characterizing the degree of effectiveness of this known process used in the processing of raw materials, in the case of using the previously mentioned technical solution - an analogue, directly in the conditions of existing industrial production.

In another, also known, method for producing a multicomponent alloy containing, among others, a zirconium element, in order to increase the technical parameters of the finished final product synthesized with its use, the following necessary additional technological methods are used.

The use of the latter, ultimately, allows one to increase the physicomechanical characteristics of the material produced using this well-known method — an alloy containing the entire set of the elements listed below.

So, the above-mentioned well-known multicomponent alloy contains in its composition: aluminum - 5.0-7.5%; zirconium - 3.0-5.0%; tungsten - 5.0-7.5%; hafnium - 0.005-0.2%, titanium - the rest, up to 100%. (See patent RU 2396366; “Heat-resistant titanium alloy”, C22C 14/00; published on 08/10/2010 - hereinafter this known technical solution will be considered as a prototype).

The aforementioned multicomponent material based on titanium, which includes the zirconium element, is synthesized in a vacuum arc furnace using the so-called double remelting method.

A well-known alloy made using the above technology, as evidenced by the information presented in the materials describing the invention, is characterized by a sufficiently high heat resistance. Products made from such a material quite successfully operate up to a temperature of 750 ° C under conditions of exposure to a sufficiently long load.

However, this previously noted, well-known method of manufacturing a multicomponent alloy based on titanium, zirconium, as well as other currently existing technical solutions - analogues, has all the same set of organically inherent, significant drawbacks, namely.

During this kind of processing carried out with its help, the raw material passes through at least two “remelting”.

And one and the other components of this well-known technology, its transitions are carried out using equipment that is quite complicated in design - a vacuum-arc furnace.

The presence of the fact of the above circumstances dramatically increases the additional costs used to meet the relevant production needs and the industrial needs that serve it, necessary for the implementation of all this, energy resources.

In view of the presence of such specific features of carrying out this known prototype method, that is, such as the need to perform the latter using high-temperature melts formed directly in them, as well as synthesized using their finished product and constituting this alloy of the starting metals used for the implementation of this method of processing raw materials, equipment, as well as auxiliary technological systems serving its functioning, are characterized by a high degree onstruktivnoy complexity and, consequently, its cost significantly.

The above-mentioned known prototype technology, among other things, has a “strikingly straightforward”, irrational organization of its own, used in the process of its implementation, and unique to it own technical structure.

So, for example, the implementation of the known processing process is carried out with the obligatory involvement of a significant number of metallurgical processes necessary for obtaining the known multicomponent titanium alloy. That is, during its implementation, the initial raw material charge is preliminarily formed, and then its subsequent “remelting” is carried out at least twice. After all this, obtained in the manner indicated above, the ingot is also subjected to additional heat treatment (annealing).

However, the use of the entire set of the abovementioned of these significant distinctive technical features, the presence of a negative effect on the course of this well-known processing process which interferes with the possibility of its widespread industrial use, does not ultimately achieve the set and necessary technical goal.

Namely, the use of the latter does not at all guarantee the receipt of a finished final product having sufficiently high intrinsic physical and mechanical characteristics.

That is, when using this well-known technical solution, the prototype, still it is not possible to obtain a heat-resistant titanium alloy, with layers forming its volume, which would be formed as a set of crystal lattices, the components of which would be corresponding synthesized from the feedstock and constituting the latter metals, and the finished product itself, produced from the raw material charge used, would be a columnar ring single crystal having a certain and predetermined e given set of geometric parameters of its own.

The aim of the invention is the formation when carrying out the proposed method for producing a multicomponent alloy based on titanium, iron, chromium and zirconium, a complex of necessary and optimal conditions, the very fact of the action of which would allow the synthesis of this material directly from the compounds of the above elements to its the line of components used in the implementation of the process of their recovery during the formation of this finished final product from the original ore raw materials, the simultaneous synthesis at the final stages of such a technology for processing the starting material, the crystalline structure, which is a columnar ring formation, which should also have high intrinsic physical and mechanical characteristics, as well as the latest “heat resistance” indicators, and besides all of the above earlier, also a decrease in the degree of structural complexity used in carrying out the proposed technology for the manufacture of multicomponent titanium alloy, this very used in the process of its implementation of the device.

Achieving the above goals is ensured by using the influence on the progress of the proposed method for processing the original raw material, the following set of significant distinctive technical features.

First of all, in the following, it would be necessary to also note that the proposed method includes, in the course of its implementation, the operation of loading a preformed and containing titanium, iron, chromium and zirconium compounds, the initial raw material mixture, in the internal volume its processing device. In the above device, after the loading operation of the feedstock is completed, physical fields are also generated that are superimposed on all zones in its cavity containing the processed raw material placed in them. Using these physical fields, the process of recovering the components of a multicomponent alloy of components from the ore material containing their initial compounds is carried out.

The use of the same processing physical fields, in the end, ensures the connection of the individual elements included in the composition of the raw material mixture used in the processing into an integral monolithic metal structure, i.e. into this finished product itself, presented as a multicomponent alloy.

Secondly, you should also pay close attention to the fact that in the process of implementing the proposed method, the mixing of the components of the initial volume of the raw material and its last layers during its processing is necessarily carried out. At the same time, the finished product is also accumulated in the device area located in the impact zone of the above-mentioned physical fields used in the processing of raw materials. Upon completion of the processing process, the finished monolithic formation is also unloaded from the cavity of the device used.

As the raw material containing titanium, iron, chromium, zirconium compounds when performing the proposed technology, water suspension obtained by introducing into a predetermined volume of water with subsequent distribution in it of a mixture consisting of particles of titanium, iron and zirconium ore is used. The dispersion of the solid components included in the composition of the latter is in the range of 0.001-0.008 mm, and their amount in the volume of this aqueous suspension corresponds to a value of 40-70%.

The initial ore rocks used to obtain the above raw material mixture form the latter when they contain 44-45% for zirconium, 14-15% for iron and titanium, respectively, the rest, up to 100%.

The alloy obtained at the end of the processing process itself is formed in the form of an annular columnar structural formation, consisting mainly of the above elements - titanium, iron, chromium and zirconium.

As the physical fields acting on the processed raw products, “rack and pinion, with teeth having the shape of rectangular trapeziums” are used, the intensity of which is 9 × 10 ⁴ ÷ 1.1 × 10 ⁵ A / m, and their vibration frequency corresponds to a value of 7-12 units within one hour, and the “processing” clusters formed by these physical fields, consisting of lines of force belonging to them, repeat the configuration as close as possible to the outline of the spatial formation obtained by rotating a rectangle elongated in length, making turns about its own longitudinal axis of symmetry.

At the same time, the process of forming the finished end product in the form of an annular columnar ring formation is carried out on a metal spacer rod, which acts as a “seed”, located directly in the center of the mobile working chamber used to place the feedstock. On its lateral outer surface at the very first stage of processing, an annular layer is first formed, which is represented by slag waste obtained during processing. Then, on this kind of “substrate”, the necessary finished product is synthesized.

As mentioned earlier, the formation of the latter is carried out in the form of an annular columnar structural formation, which includes the above components represented by its constituent elements, i.e. titanium, iron, chromium and zirconium.

When processing using the proposed method for its implementation, the raw materials used are preloaded into the working chamber, which is hermetically isolated from the rest of the device’s body volume.

The latter, when executed, also makes a reciprocating movement along the body cavity using the round-trip directions, and also makes angular rotations relative to its own longitudinal axis of symmetry.

The above-mentioned angular rotations that make up this camera elements are first performed in a circular trajectory, the outline of which coincides with the clockwise movement on the dial - on the very initial segment of the path of the movement performed by it, and in the opposite direction, i.e. counterclockwise, respectively, at the end of the processing cycle, the same, but already the opposite.

The very arrangement of the regions of formation of the "rack" magnetic fields was made using three, or a multiple of this number, a different number of spiral-shaped installation cylindrical lines. The latter “encircle” the outer surface of the device’s body, in the cavity of which the reciprocating movement of the working chamber is loaded with the mass of processed raw material loaded into it.

In addition to all of the above, when implementing the proposed technology, the zone of formation of technological “rack” magnetic fields that its working chamber periodically moves in the cavity of the device’s case periodically crosses, is removed from each other by the same mounting distance, and the number of areas in which the generation of the latter is carried out, is a value from nine to eighteen units per each spiral-shaped encircling device housing used for their placement Wa trajectory.

The process of restoration of elements included in a multicomponent alloy is carried out by supplying the components of the processed volume of raw materials to its layers of atmospheric air.

The carbon element present in the composition of the gases containing this component, which, in turn, form the jets themselves blown through the working chamber of the above product, is used as the element that provides this action.

The mixing of the volume of the raw material used to obtain the titanium alloy is carried out in the process of moving it in the internal volume of the movable working chamber, which performs a “screw” reciprocating movement in the direction from the rear housing of the device to its front part, and then vice versa. The above operation is performed by crushing and transferring from one region of the volume of the cavity of the working chamber to another constituent of the processed mass of its individual microports, which proceeds under the influence of blows created by the intersecting jets of compressed air supplied to the latter. The receipt of this product to the above zones is carried out under excess pressure, the value of which corresponds to a value of 0.4 ÷ 6.0.0 kgf / cm ² .

Themselves of this kind, "piercing" the material layers of the raw material jet stream flows are formed using specially provided for this action blowing elements - nozzles. The latter are also evenly fixed on three installation spiral lines, which are laid between the corresponding turns of the curves used to place the magnetic generators.

The blasting elements themselves, which ensure the supply of pressures consisting of the above product and directed directly to the volume of the feedstock of this kind of “crossing” flows, have both tangential and radial tilt angles of 30-45 ° with respect to the surface on which this processed material at a given time and is located.

The loading of the feedstock used for processing, as well as the unloading of the finished columnar ring single crystal at the end of the processing process, is carried out in a separate, removable cap - compartment attached to the fixed main body of the device, designed to perform the above technological transitions.

The device itself, designed to implement a method for producing an alloy based on titanium, iron, chromium and zirconium from an aqueous suspension, particles containing compounds of these ore elements, includes a body consisting of two parts. One of the parts of this case is removable and is made in the form of a cap removable cap that fits into the fixed main cylindrical shell-body. Docking is carried out using annular flat connecting flanges, and the length of the fixed element indicated above the assembly, is 80-85% of the total corresponding dimension of the latter. The rest of its length falls on this removable part itself - the cap. In addition, a movable working chamber is installed in the cavity of the fixed part of the device casing, kinematically connected by means of a running roller attached to the components of the last parts, with an external drive for transmitting movement, the presence of which ultimately allows its reciprocating movement along the internal cavity of this assembly the device’s body, in a round-trip direction, while simultaneously rotating its structural elements relative to its own longitudinal axis of sym etria.

The direction of such rotation changes to the opposite at the time when the mobile working chamber is returned from the final position it occupied by this node to its original initial position.

This working chamber itself is formed by the left and right “piston-like” restrictive cheeks fixed on the roller. Between the above details of the composite working chamber, a spacer rod is mounted - a seed used to deposit the finished product obtained in it on its lateral outer surface.

At the same time, the cheeks of the working chamber that are moved inside the cavity of the assembly housing of the device perform the functions of a double piston in it, and have sealing seals on their outer side surface.

It should also be noted that focusing magnetic nozzles are passed through the walls of the fixed part of the housing, as well as blowing nozzles for forming compressed air jets entering the internal volume of this component of the assembly unit of the device, and in addition, accordingly, clusters of magnetic lines of force lines generated by the focusing nozzles having the configuration of radial "round" rays "logs" elongated along a straight line.

The arrangement of both those and other structural elements of this device is made on cylindrical spiral lines encircling its body.

The number of such kind of installation curves used to fix each such part is three, or any other number that is a multiple of this value, their units. The number of magnetic loops placed on each of these curved paths, which include focusing plates, is from nine to eighteen pieces.

Evenly arranged on spirals similar in shape and using the same number of spirals, located in turn between the turns used to arrange the magnetic contours of the curved installation lines, the blowing nozzles have both radial and tangential angles of 30-45 ° with respect to the surface of the housing on which they are mounted.

The working elements of the processing magnetic generators themselves are made in the form of plates of magnetically conductive material stacked together, with the formation of an F-shaped magnetic circuit during their installation.

In the volume of the individual components of this assembly, three electrical windings of the coil are placed, both in the left and right halves of the circuit.

The total number of such coil windings placed in each circuit is thus six. The electrical elements of the magnetic circuit noted above fulfill the function of solenoids in it.

Each such winding coil is connected to the corresponding "pseudophase" of an external source of electrical power supply. The input of sets of electric pulses generated by this external power source, each of which takes the form of a “gear trapezoidal rack”, is produced on separate solenoids with an angular displacement of the signal components that make up these packets with respect to the same ones, but supplied to adjacent windings - coils, as well as to generators, located on adjacent mounting spirals.

The value of the above angular displacement is a value of 120 °. In the lower horizontal transverse crossbar of each F-shaped magnetic generator, that is, in the recess in it, a shank of a cylindrical focusing nozzle is pressed in, the opposite end of which goes into the mounting hole made in the installation sleeve, passed through the walls of the fixed part of the housing. The aforementioned nozzle also has a cavity-indentation in the form of a depression with the configuration of a spatial rotation hyperboloid formed on its lower end part and focusing magnetic field lines in a cavity.

The “curvilinear recesses” on the inner side surface of its cavity, obtained in places of passage through the walls of the housing of the mounting sleeves with focusing magnetic nozzles, as well as blowing nozzles, are equipped with “smoothing” washers. The latter are made either of magnetic conductive powder pressed into the volume of these recesses - in the case of placement of magnetic focusing nozzles there, or in the form of split petal membranes of elastic rubber located near the outlet openings of the blowing nozzles.

In addition to all of the above, exhaust pipes are mounted in the left and right halves of the fixed casing for the discharge into the outside atmosphere of the excess gas accumulated in the working chamber, equipped with pressure reducing valves. The operation of these "bypass" elements is carried out in the case when the pressure value of the volatile compounds formed in the volume of the mobile working chamber exceeds its value specified by the processing technology.

Again, it should be noted that at the places of intersection of the body of these pipes with the side inner surface of the fixed housing, perforated plastic smoothing washers are mounted, which ensure the smooth flow of the sliding process in these areas of the working chamber of its right and left cheek pistons, as well as the output through the through holes in the above details through the perforations of the excess gas volumes filling it.

It is also necessary to point out that in the upper part of the removable cap of the device, there is a loading hopper, the internal volume of which through the through hatch in the installation area, made in the same part of the device’s body, communicates with the cavity located underneath the movable working chamber , occupying at the time of its filling, the initial "starting" position before the start of the processing cycle.

Based on all the above features of the proposed method, as well as taking into account the fact that there is an application of the entire set of the previously mentioned significant design features in the device used to implement this technology, we can ultimately conclude that the influence of the latter makes it possible to fundamentally change the process of formation of an annular columnar structural formation consisting of elements - titanium, iron, chromium, zirconium, obtained during Processing a feedstock containing ore compounds of these components listed above.

In connection with the fact that the above circumstances exist, the previously mentioned technology begins to acquire the following characteristic differences inherent only to it. First, the latter should definitely include the fact that the very initial stage of the implementation of the proposed method includes the stage of the so-called "ultrafine grinding" of pieces of initial ores containing compounds of titanium, iron, chromium and zirconium.

During its implementation, any known methods of crushing bulk material known in industrial production, for example, performed using conventional ball mills, are used. When applying the above device to achieve this goal, the pieces of the initial raw material used in the proposed technological process were ground using the latter to obtain ore particles from them having overall dimensions in the range from 0.001 to 0.008 mm.

The implementation of the above operation to "grind" large lumps of rock and further provides the possibility of forming from the thus obtained "powder", consisting of a mixture of small ore particles, containing, in turn, compounds of titanium, iron, chromium and zirconium, a kind "Dry residue", entirely synthesized from the above solid raw materials.

The multicomponent "dry residue" used in the processing process includes zirconium ore - 44-45%, iron ore - 14-15% and titanium rock - the rest, up to 100%.

The above ore components of such an initial mixture immediately before the crushing operation of the ore lumpy material used in its composition passes, respectively, through the preliminary dosage stage, at the end of which the further supply of the starting materials necessary for processing is guaranteed in a predetermined predetermined mutual ratio, ensuring the preservation of their technological percentage in the amount of cheese used in its implementation oh. This technological transition itself, that is, this preliminary dosage, is most often carried out by weighing the ore components included in the raw material mixture (i.e., titanium, iron and zirconium rocks, respectively).

From this kind of “powder” obtained by carrying out “ultrafine grinding”, consisting of small particles of zirconium, iron and titanium rock, the formation of the material used to process the raw materials into a multicomponent alloy is made, liquid, homogeneous, not stratified into separate components during a sufficiently long period of time, a mud-like mass - that is, the water suspension itself is made.

In order to synthesize the latter, it will only be necessary to add to the “powder” volume thus obtained, consisting of small particles of all the previously mentioned ore rocks, the required amount of water (30-60% of the total mass of this solid material). After performing such an action, the two-component substance thus obtained (a mixture of solid particles plus water) is thoroughly mixed.

To implement this technological transition, any industrial equipment designed for the implementation of the above goal can be used, for example, an ordinary paddle mechanical mixer. A homogeneous “mud-like” portion of the volume of the aqueous suspension formed at the end of its holding, consisting of these two components listed above, is then placed in the cavity of the loading hopper 2, which is part of the removable part of the housing used in the processing process of this device itself. From the cavity of the loading hopper 2, the water suspension through the through hole “B” (see FIG. 1) through the through-hole in the removable cap 4 enters the interior of the mobile working chamber located directly below the loading hopper and formed by restricting it to the right and left sides of the cheeks-pistons 3, which are part of such a node, as indicated above. Upon completion of the operation of the complete withdrawal of all previously filled the volume of the feed hopper 2 of the raw material mass 1 into the above cavity of the mobile working chamber, the following actions are performed.

Immediately and simultaneously connected to external power sources that generate and supply rack-shaped trapezoidal electric pulses, all of which are part of the F-shaped magnetic generators 11 of their winding-coil 13.

The roller 8 is set in motion, and makes the structural components making up the working chamber move in the direction from their initial starting "initial" position, to the very front "right" part of the fixed half of the device assembly 6. Simultaneously with the implementation of the above translational movement, carried out at a speed of 40-60 minutes, the details of the working chamber also perform additional angular rotations relative to its own longitudinal axis of symmetry (2-4 rpm). In addition, to the external supplying air under overpressure of the line (0.4-6 kgf / cm ² ); connected and placed on the spirals "D" passing between the respective turns of the installation curves "G" lines with the generators 11 fixed on them, blowing nozzles 10.

Thus, starting the treatment cycle, the working chamber with the processed raw material 1 caught between the “piston-shaped” cheeks 3 forming it, is pushed “to the right” from the cavity of the cap removable cap 4, and passes after this action, directly into the internal volume of the fixed body 6 ( see figure 1). As the depth of penetration of the mobile working chamber directly into the above-mentioned cavity of this collection unit increases, the material placed in the last raw material 1 undergoes a constantly increasing force effect, which is carried out from the side as the layers of the initial product “penetrating” into the mass “intersecting” among themselves exhausted from the nozzles 10 of compressed air, and generated by the focusing nozzles 14 of the magnetic "beam" cylindrical flows "K" (see figure 3). Due to the fact that all the above structural elements are placed on the spirals “G” and “D” encircling the outer side surface of the housing 6 (3 units + 3 units), the internal cavity with a “turtle” speed crawling along the body 6 devices of the working chamber with the raw material 1 placed there being processed into a multicomponent alloy, when performing its movement, inevitably falls into the zone of influence of all these power energy formations listed above.

The above-mentioned spatial technological systems, consisting of the individual individual “physical” elements forming the last, have the same, strictly preserved own configuration, oriented in a certain way relative to the trajectory line that the working chamber lays when performing its translational “screw” movement along the internal surface of the precast device enclosures. That is, taking into account the fact of the presence of the action of the above circumstances, we can confidently assume the following: after a certain fairly short period of time has elapsed, a whole set of factors begins to act in the space separating the left and right “piston-shaped” cheeks 3 of this assembly formed using all of the above and used as part of the design of the proposed device, power spiral formations.

Firstly, a mass of processed raw materials 1 covering the bottom at the moment the working chamber performs such a translational movement from the initially occupied last position to the front “right” end of the housing 6, a series of “crossing air strikes” directed at different spatial angles falls.

Such a nature of the flow of action from the side of the air flows formed by the jet nozzles 10 is explained, first of all, by the selected scheme for their installation on the housing 6 (that is, by their placement along the spiral line “D” encircling the device’s body and at “oblique” angles with respect to the surface housing on which they are fixed).

Experiencing itself, as it were, constantly increasing “pressure” from the latter, a compact “heap” of raw materials resting in the very bottom of the working chamber, in the literal sense of the word, is “scattered” into separate, small, previously micro-volumes of it. These new “microscopic” raw material fragments obtained from the source material are picked up by a peculiar vortex “tornado” “E” formed between the corresponding surfaces of the right and left cheeks 3, and after that they begin to circulate forcibly given by its action in the circuits creating such a spiral flow and generated using nozzles 10, constituting this newly obtained gas formation, and entering directly into it, its individual jets.

It should also be remembered that due to the ongoing and continuously carried out application of the above “series”, consisting of such “air attacks” generated in the processing zone, torn from the place of its “initial basing”, and spaced over all of the working chambers to its individual regions, the “smallest” portions of the starting material 1 will inevitably transform into aerosol bubbles formed from small air gas formations, as well as the films of the liquid that covers them from the outside, and also sticks x directly on its surface of microscopic particles of ore rock.

As already noted above, almost the entire volume of this type of aerosol foam obtained in the manner indicated above continues to flow continuously between the cheeks 3 bounding the cavity of the mobile working chamber, and directed along the “E” vortex flow, a kind of “orienting” spiral, as if forced circulation.

The previously noted nature of the transfer of the constituents of this “aerosol” cloud of layers is protected throughout the entire period of time during which the working chamber is moved in the device casing 6 in a round-trip direction.

In the process of performing this previously noted forced and artificially provided circulation of the “foam mass” already obtained in the cavity of the mobile working chamber from “aerosol bubbles”, ore microparticles placed on them necessarily “run” against the body cavity 6 piercing “through and through”, and, therefore, the regions constituting the separation space between the cheeks 3 of the mobile working chamber, rectilinear cylindrical and radially directed, rotating clusters “K”, to the magnetic fields created in the device.

The fact of the constant effect of this circumstance during the processing of raw materials, again again leads to the inevitable emergence of a number of new physical factors that influence and transform the structure of the ore components of the initial product.

In fact, each separately taken kind of “technological” aerosol bubble, in the process of making its own complex spatial movement along a curved three-coordinate trajectory, as it were, “tears” through the “picket fence” facing it, which again consists of separate generatrices arranged in a spatial spiral its "logs" - that is, clusters located radially in the cavity of the device, and stretched directly in its constituent zones, moreover, having the configuration n rectilinear cylindrical, rotating around its axis of symmetry of the structural formations formed by magnetic lines of force.

Among other things, the “height” of these movements placed directly on the path of such an “aerosol foam” and, as it were, a kind of obstacle to it, are three at once built along the trajectory of the “stockade” it carries out (magnetic generators 11 are mounted on three encircling buildings 6 set spirals “G”), moreover, and continuously changes its own value.

That is, each “power” log included in this kind of “fence” alternately increases its length, then again resets this parameter to almost zero, and with all this, it also rotates around its own longitudinal axis.

The aforementioned phenomenon occurs due to the fact that the sets of electric pulses sent to the generating magnetic fields solenoids 13 are in the form of a bar with trapezoidal teeth (see Fig. 5 - pseudophases a, b, c), and are fed with an angular offset relative to each other.

In addition, the individual logs erected on the path of the movement of individual aerosol bubbles of this kind of “fence” also have mounting displacements relative to the same exact “stockade” used in neighboring, located next to it (pulses applied to solenoids 13 more and shifted into each pseudophase a, b, c sent to the solenoids by an angle of 120 ° - see Fig. 5).

The straightness of the outlines formed by the focusing nozzles 14 clusters (cylindrical logs) generated by the contours of 11 magnetic lines is ensured by the use of the so-called last concentrating recesses "M" made in the form of a recess in the form of a spatial rotation hyperboloid (see figure 3).

Based on the foregoing, we can come to the final conclusion that a “three-way” technological complex consisting of the above-mentioned magnetic barriers, some elements of which also change their height periodically, erected through the erected directly on the trajectory of their movement , and rotate around its axis, the microscopic particles of the processed raw materials inevitably pass through the “continuous downpour" applied directly along them using the entire possible set of spatial directions their influence, as well as continuously changing their own value, generated by the components of these "palisade" logs, powerful force blows.

Under the influence of the latter, aerosol bubbles, microscopic solid particles of the initial ore rock, molecules of their initial compounds, containing the metals forming the produced single crystal, are broken up into separate “fragmentary” components that are “attached” to the film coating. At the same time, all types of valence bonds forming them earlier, both ionic and covalent, are broken.

The individual atoms that were previously made up of these molecules, under the influence of the powerful external continuously performed external energy action indicated above, rearrange the original initial structure - the electrons they have move from lower orbits relative to their core to higher ones, their spin moments change. As a result of all this, in the final final variant of carrying out such structural adjustment, the atoms - “fragments” located directly in the processing zone and obtained in the above manner are converted into positively or negatively charged particles — that is, into ions. But this kind of technological complex, as if formed from a “vibrating peak” of a kind of “jack hammers” (this tool is the power flows generated by the magnetic circuits 11 and sent through the nozzles 14), “breaks”, and also turns into a set of “activated of fragments ”not only compounds contained in solid raw metal particles of metals, but also“ breaks ”the gas molecules located in the same zone containing the reducing element, that is, carbon. The latter, as already noted earlier, is part of the gases necessarily present in the atmospheric air and its constituent gases (CO ₂ ; CH ₄ ).

The appearance of a carbon ion synthesized in the above manner, that is, a substance with the pronounced properties of a reducing component, in the immediate vicinity of activated by using powerful magnetic fluxes and previously obtained “fragmentation” fragments containing charged metal particles, and provides a “strong” connection of the released upon the destruction of the initial molecules-compounds of oxygen atoms, which subsequently instantly form strong valence bonds with the above element, restore elem, and ultimately, the last removed from the field of processing, becoming a new volatile gas connection.

The volumes of gas thus formed leave the cavity of the working chamber at times when it moves through the installation zones of the exhaust pipes 18 (Fig. 1) equipped with pressure reducing valves 19. When the latter are actuated, they are configured for a specific and predetermined technological overpressure accumulated in the cavity portions of already unnecessary volatile compounds are sent through the upper end of the exhaust pipe 18 directly to the surrounding device, the external atmosphere.

These newly-formed alloy components themselves are formed directly from the constituent ore and reduced from the compounds present there and necessary elements for this, and create in the processing area at the very initial stage of its implementation, still microscopic crystallization centers, mainly consisting of the finished product thus obtained.

Under the influence of the vortex stream continuously circulating in the cavity of the working chamber and the artificially formed vortex there, such “microcrystals” at this, so to speak, “starting” processing stage, move in it so far only in the direction from its left cheek 3 to the right one, and then vice versa, as if carrying out a kind of process of “free swimming” in its rotating spiral jets.

It is necessary to pay additional attention also to the fact that when conducting a more detailed consideration of the features of the technology for the formation of these, as if without any noticeable "difficulties" "floating" in this "tornado" and its constituent air layers, metal " nuclei "of the future single-crystal annular columnar formation, the inevitability of the fact of the action of another, but very significant circumstance, facilitating, so to speak, the process of their" unobstructed "appearance on the" white light ".

Separate aerosol foam bubbles carried there by a spiral hurricane created there, containing microparticles used in ore processing, moving in the volume of a mobile working chamber using a complex set of curved spatial paths, repeatedly change their positioning relative to their own three-axis symmetry axes. At the same time, such “foamy” bubbles also constantly shift “here and there”, “here and there”, in different directions from the direction of the alloy components specially carried out in the zone of restoration and continuously created in this device itself, which is necessary to perform the above operation , technological force action, formed in the same processing area, where all these bubbles at a given time themselves are located.

Figuratively speaking, each separate raw material particle of this kind, at the moment of applying a “powerful” power processing blow, substitutes either one “side” or the other under it, and continuously rotating at the same time, provides an occasion for it to all its own volume components and forming it microlayers of the starting material.

Due to the action of the above-mentioned factor, the processing magnetic fluxes generated in the device acquire the most optimal conditions for free access to all structural formations of these solid microparticles, and thereby guarantee the achievement of the highest possible conversion rate of the initial compounds included in the latter , into the desired finished product.

The previously noted free air “planning” of newly emerged nuclei from a multicomponent alloy in vortex-like jet streams continues until the mass of the latter becomes so significant that the force of gravity acting on them does not start significantly exceed the aerodynamic lifting created by the vortex formation.

This kind of "growth" of small grains of the alloy into larger "larger granules" becomes possible due to the presence of the influence of two immediately, ensuring the inevitable implementation in practice of this factor, simultaneously operating processes.

In accordance with the first of the above, a grain of a multicomponent alloy “flying” in the thickness of an aerosol cloud will inevitably fasten other, smaller solid “ore” particles surrounding it on all its sides, appropriately placed at this moment in time, to the smallest adjacent aerosol bubbles. The latter, encountering a solid “enormous” crystalline grain flying at them “directly into the forehead” at high speed, simply collapse, throwing ore microparticles previously attached to the surface of this air bubble and transferred to it before it. As a result of the fulfillment of a number of such numerous collisions, the outer surface of the crystalline nucleus “hovering” in the air flow acquires a kind of “coat” consisting of microporosity scattered around it by other and neighboring aerosol bubbles, and, as a result of the above action, “sticks” "Directly to him, ore rock. Due to the fact that the process of its movement continues to take place in swirling air streams covering the “embryo” from all sides, the latter crosses repeatedly and periodically with its whole body created by installation spirals radially located along the installation spirals used in the device and piercing by its clusters of magnetic lines of force of the physical fields generated there, a kind of processing and hanging in the volume of the working chamber itself, a “cylindrical vibrating fringe”.

The aforementioned processes of conversion contained in the layers of ore rock contained in the adhering to the crystalline nucleus body, consisting of the compounds that make up the alloy of components, continue to be carried out there in accordance with the technological scheme already discussed above. As a result, the "enveloping" body of the "coat" transferred by the vortex flows of the "grain" of the previously obtained alloy "coat" ultimately turns into a full-fledged metal coating uniformly distributed over the entire outer surface of the latter. Located directly under the very base of this metal film formed from a raw "fur coat", and the "surface" layers of the crystalline nucleus adjacent to it, in this case, they act as a seed substrate, on which the process of its growth is carried out. As a result, the alloy crystal “flying” through the cavity of the mobile working chamber, as a result of all this, significantly increases its initial overall dimensions, and, consequently, its volume and its own mass.

Simultaneously with the above-mentioned scheme for growing larger metal crystals from any “germ” fines formed earlier in the processing zone, there is another, second mechanism for synthesizing similar large-sized structural formations. The latter is carried out as follows. When performing complex spatial displacements in the space bounded by the cavity of the mobile working chamber with small, newly crystallized metal grains of metal, inevitably situations arise when these microscopic crystalline "grains" directly collide with each other. Since in the zone of such kind of “mutual runs”, as a rule, clusters of magnetic lines of force are assembled in a “tight” cylindrical beam, that is, there is always a kind of “processing fringe” created by the magnetic circuits 11 and focusing nozzles 14, then the small metal nuclei that "came across" each other, as a result of this, are glued together under the influence of the above-mentioned power "tools", forming as a result a new composite structure. It is quite clear that it has large linear dimensions, relative to those that had the original, constituting its individual formations.

In practice, the above mechanisms for the formation of large-sized granule-like structures from any metallic fines that appeared in the processing area of the raw material flow together and at the same time, which ensures the transformation of small crystalline grains directly in it into a kind of large-sized structures from those obtained in the processing zone lumpy finished product.

Since the above “combined” formations are no longer able, due to a serious increase in their own weight, to continue the process of their “swimming” in the jets of the whirling air flow created in the cavity of the mobile working chamber, the latter fall vertically downward under the influence of gravitational forces, and reach the most extreme lower horizontal level of their possible subsequent placement in the device casing. On the outer lateral surface of the rod - the seed 7, installed directly along the longitudinal axis of symmetry of the device, at this point in time the ring layer "G" has time to form (see Fig. 2), consisting of the metal formed from the direct reduction from its ore compounds “Sticky” slag waste. The latter, as a rule, consist of 80-85% of the volume of slag included in the above “tailings” obtained and accumulated in this zone, i.e. the so-called ferrotitanoaluminosilicates and ferrozirconoaluminosilicates.

This intermediate layer “Zh” enveloping the outer surface of the core - seed 7 appears there, primarily due to the fact that in the central zone of the working chamber, aerodynamic forces practically do not act on the particles placed in it, created mainly by “peripheral” jets sweeping through it swirl air flow "E". That is, this core - seed 7 is placed, as it were, in the very "eye of the storm", where the "calm" reigns always. Possessing good “adhesive” ability, small particles of slag waste synthesized in the working chamber under the influence of air flows created in its cavity and directed from its periphery to the center of the air (from the high pressure zone in the region of maximum vacuum) almost always carry out its own radially directional movement, which, ultimately, collects them together and causes them to “stick together” in the encircling rod - the seed 7, the annular layer “G” (see figure 2). The latter has a rather "loose" structure, and subsequently easily disconnects into its component parts when the finished product is removed from the device body, which has the shape of an annular columnar single crystal "And" (see figure 2).

Similar processes take place when receiving in the device the most multicomponent finished product. That is, part of the strongly “sprawled” crystalline nuclei from the synthesized alloy falls vertically downward, falling directly onto the outer surface of the chamber located in the center of the chamber and already formed there earlier, from the slag waste from the slag waste, and it gets stuck on its plane in contact with them while creating, as it were, “secondary zones” of the course of further crystallization of the constituents of the already obtained multicomponent metal alloy. The particles of the synthesized finished final product, which have again moved there, begin to use these pieces of alloy previously found in the above region as a supporting substrate — a base that allows their further growth to occur and, ultimately, the formation of all these separate “grains” due to “fusion” »As if into an integral monolith, formed in this way, in the form of a columnar ring single crystal, consisting mainly of elements synthesized in the device - Ti; Fe; Cr; Zr.

A somewhat different picture is observed in the case when the alloy grains, which have increased their own initial mass, fly by the target due to the action of some complex of negative factors — that is, they fall down, bypassing the central core — the seed 7, and eventually fail in the lowest region of the fixed body 6.

Once on its very “bottom”, they can either fall directly onto the petals of the split smoothing washer 17 (see FIG. 4), which covers the nozzle outlet 10, or onto the surface of a kind of gap separating such distributed over the lateral outer surface of the assembly 6 included in its composition blowing elements 10.

In the first version, a “blasting” stream of compressed air under a sufficiently high pressure, bending the radial petals of the smoothing washer 17 to the side (see Fig. 4), immediately throws a “grain” of metal into this zone at an inclined angle towards that plane, on which it lay, as well as up.

As a result of the implementation of the above own displacement, the direction of which is determined by the available tangential and radial angles of inclination of the blowing nozzles 10 installed on the sheathing spiral “D”, and a metal particle falling under the impact of an air stream will either be thrown into the central region of the working chamber and then, as a result this, again, will be glued to the growing single crystal “I”, or will come into direct contact with the surface of the moving working chamber bounding the cavity with one the first of its sides, the piston cheek 3. With this collision, the metal “grain of the alloy” bounces, and again, either “bounces” from the plane of this element of the device and moves to the “core” of the working chamber filled with an expanding metal single crystal “And ", Or again falls into the lower region of the housing 6. In this case, the cycle of movement of a metal particle is repeated in exactly the same way. The “metal grains” that fell on the “isthmus of the isthmus” between the nozzles 10 installed in the device’s case sooner or later are pushed out from their original location by the surface of the continuously and progressively moving cheek-piston 3 of the working chamber, which, moreover, also “scrolls” around its own longitudinal axis of symmetry.

Thus, this part of metal particles accumulated on the "bottom" of the housing 6 is "retracted" to parts of its surface through which jets of compressed air entering the volume of the working chamber are passed.

Finding himself in these areas of the surface of the housing 6, and this accumulation of “grains” of the alloy obtained in the working chamber, will go through the entire previously disassembled cycle consisting of “rebounds” and “rebounds”, which ultimately, due to the action of ordinary laws of statistical probability, will force the latter to take the required final position, fixed right in the thickness of the grown single crystal “I”.

The above-mentioned processes of formation of an annular columnar single crystal “And” on a seed rod 7 (see FIG. 1) continue throughout the entire period of time during which the working chamber is moved, in the “back and forth” direction, which corresponding dimension is due to with the above and is 15-20% of the value of this parameter, which determines the total length of the device used for its movement. Based on the need to create the most optimal conditions for completing the processing process, the choice of the value of the speed of its longitudinal feed (40-60 mm / min) was made. The working chamber makes angular rotations of the latter around its own longitudinal axis of symmetry at an insignificant speed - only 2-4 rpm.

When reversing to the other side (the reverse segment of the path of its movement carried out by the working chamber), the seed-seed rod 7, as it were, “wraps” metal layers formed around it onto its outer side surface, thereby increasing the uniformity of the distribution of their own thicknesses obtained in these zones along the entire length of the body of the single crystal “I” itself forming in the working chamber.

So, having reached its extreme final front “right” position, and having received the appropriate commands from the external power supply and control unit used as part of the device, the working camera begins to move in the opposite direction, that is, it begins to move already to the very rear left side of the device 6, until until she again takes the same initial position in the cavity of the removable cap 4, in which she was at the very initial stage of the processing process. During the implementation of the aforementioned part of the cycle of this kind of "reverse movement" of this working unit of the device, which is performed at the same speed as the direct one, the processes of "final completion" of the formation of the obtained columnar ring single crystal consisting of a multicomponent alloy continue to be carried out in it. That is, in fact, a “finishing” refinement of its configuration and composition to the final standards required by the processing technology is carried out.

Having moved to the leftmost position, and having again taken its initial position, upon completion of the above steps, the working chamber of the device thereby completes the entire cycle of the process of processing the feedstock into the desired finished product. Accordingly, at this stage, the shutdowns are made: the drive, providing for the reciprocating and rotational movement of the working chamber, the solenoids 13 of the magnetic generators 11 are de-energized, and the nozzles 10 are disconnected from the external supply line of compressed air. At the same time, from the back of the housing 6 due to the release of the flanges 9 pressed against each other, a removable cap 4 is detached.

After all this, the piston-like cheek 3 is unscrewed, the nut 9, and the cheek 3, are removed from the corresponding end of the roller 8 to the supporting shoulders of the seed rod 7 (see FIG. 1). The single crystal obtained from the processing from the multicomponent alloy “I”, due to the presence of an intermediate loose layer of slag waste “Ж”, easily collides with the outer surface of the seed rod 7 and is sent for its intended use. The processing cycle can be considered complete.

The processes of direct reduction themselves of the constituents of a multicomponent alloy of elements from their ore compounds, at the time they are exposed to by artificially created powerful magnetic fluxes, are carried out in accordance with the following schemes for transforming the initial components.

CO ₂ → C ⁺⁴ + 2O ^-2 ; H ₂ O → 2H ⁺ + O ^-2 ;

CH ₄ → C ⁺⁴ + 4H ⁺ + 8e;

TiO ₂ → Ti + ⁴ + 2O ^-2 ;

TiO ₂ + 2O ^-2 + C + ⁴ → TiO ₃ + CO;

TiO ₃ → Ti ⁺⁶ + 3O ^-2 ;

Fe ₃ O ₄ → Fe ₂ O ₃ + FeO;

Fe ₂ O ₃ + 3C + ⁴ → 2Fe + ² + CO + 8e;

FeO → Fe + ² + O ^-2 ;

CO + CO → 2C ⁺⁴ + 2O ^-2 + 4e;

Cr ₂ O ₃ → 2Cr ⁺³ + 3O ^-2 ;

ZrO ₂ + 2O ^-2 + C + ⁴ → ZrO ₃ + CO;

ZrO ₃ → Zr ⁺⁶ + 3O ^-2 ;

Fe ₂ O ₃ + ZrO ₂ + Al ₂ O ₃ + SiO ₂ → Fe ₂ O ₃ × ZrO ₂ × Al ₂ O ₃ × SiO ₂ ;

Fe ₂ O ₃ + TiO ₂ + Al ₂ O ₃ + SiO ₂ → Fe ₂ O ₃ × TiO ₂ × Al ₂ O ₃ × SiO ₂ ;

H ⁺ + H ⁺ + 2e → H ₂ ;

2H ⁺ + O ^-2 → H ₂ O;

C ⁺⁴ + 2O ^-2 → CO ₂ ;

Ti ^{+ 6} + 6e → Ti ⁰ ;

Zr ⁺⁶ + 6e → Zr ⁰ ;

Fe + ² + 2e → Fe ⁰ ;

Fe ⁺³ + 3e → Fe ⁰ ;

Cr ⁺⁶ + 6e → Cr ⁰ ; Ti ⁰ + Fe ⁰ + Cr ⁰ + Zr ⁰ → Ti × Fe × Cr × Zr;

where e is an electron; or a single charge with a negative value of the intrinsic valency obtained in the process of ionizing the atoms that make up the raw materials and form them.

Thus, by considering the synthesis performed in accordance with the above schemes for the synthesis of the constituent metals of the alloy and from their compounds, we can conclude that directly and inverse molecular transformations of the raw materials therein continuously occur directly in the processing zone during the implementation of the proposed method components with a shift of the chemical equilibrium developing in it towards the formation of a columnar single-crystal alloy structure in this region, consisting of titanium, iron, chromium and zirconium, as well as exhaust into the ambient atmosphere outside the intended device allocated during the execution of these complex reactions microvolumes above volatile gaseous products (CO _2; H ₂ O; H _2).

Thus, their previous analysis allows us to state that the carbon element C ⁺ obtained from carbon-containing molecules that make up the atmosphere and include this component (CO ₂ ; CH ₄ ) of gases during the implementation of “magnetic shocks” applied to them ⁴ in the end and takes away the corresponding titanium compounds; iron, chromium and zirconium released during the decay of these components atomic oxygen, tightly attached to the latter. In addition to direct ones, as was previously reported, reverse reactions also occur in the treatment zone, during which volatile gases are formed that have a minimum of their internal energy (H ₂ O; CO under the conditions of this powerful and continuously performed “field” energy effect) ₂ ; H ₂ , etc.).

Due to the influence of the entire complex of conditions indicated above, the multicomponent alloy thus obtained is a stable, in relation to the influence of all these external, artificially created force factors, annular columnar single crystal having the same predefined spatial configuration, the components of which do not pass into connection with other active components located next to it under the conditions of this intensively conducted external energy impact.

The characteristic features of crystallization of the individual metal components included in it should include, first of all, the fact that the formation of these, which forms the last and the above structural elements, is clearly set by such a basic parameter of the technological process of processing as the magnitude of the tension formed in the zone the conversion of the starting metallic and non-metallic compounds into the final product, the “rack-shaped trapezoidal” magnetic fields generated there. That is, the very possibility of obtaining it is determined, first of all, by the urgent need for strict observance, established by the technology for processing the feedstock, of the lower limit of the range of possible changes in the value of this parameter (the tension in the processing zone should always be ≥9 × 10 ⁴ A / m, and the oscillation frequency during the synthesis of an alloy of processing physical fields can correspond only to a value of 7-12 units per hour.

In general, it should be considered that the previously mentioned specific features inherent in the processing technology performed in the aforementioned manner as if allow simulating the conditions of the so-called "melting zone". That is, the process of growing a multicomponent crystal in a working chamber constantly moving in the cavity of the working chamber with its angular rotations around its own longitudinal axis of symmetry, the supply of “rack” pulses having angular displacements relative to each other and in adjacent pseudophase packets supplying them composed of them, ultimately, and provides the formation obtained in the device of the crystalline structure in the form of a columnar annular monolithic formation, consisting of an exception It is only from one of its constituent metal elements (Ti; Fe; Cr; Zr).

Other pollutants, which are also present in the composition of the initial raw material mixture of impurities, will necessarily and inevitably be converted to new crystalline formations, which subsequently synthesize finely divided loose slag waste that appears at the end of the processing process. The latter are grains of yellow-brown color with a violet tint, with overall dimensions from 0.1 to 0.3 mm. The composition of these for the most part is represented by ferrotitanoaluminosilicates, and very reminiscent of the latter ferrozirconoaluminosilicates (80-85% of the total total slag obtained during the processing process). The above set of substances can be used after grinding and mixing with water to form products consisting of insulating, refractory ceramics.

In the role of the feedstock for the implementation of the proposed method can be various concentrates of ore rocks, the composition of which, as one of the constituents of the last components, includes compounds of titanium, iron, chromium and zirconium. Their processing can be carried out without involving any additional operations for their preliminary post-treatment.

The processing of the raw feed slurry, carried out in accordance with the proposed technology, is carried out at a tension of “rack fields with trapezoidal teeth”, measured directly in the cavity of the working chamber used, amounting to 9 × 10 ⁴ ÷ 1.1 × 10 ⁵ A / m. The oscillation frequency of these force formations used for processing the initial ore materials is in the range from 7 to 12 units, passed through the solenoids of the processing magnetic circuits of the “rack” pulses for one hour.

When performing the proposed method for processing raw materials, i.e. upon receipt of alloys from titanium, iron, chromium and zirconium from the initial ore material, a technological magnetic system mounted on three encircling the outer side surface of the device body was used, in turn consisting of F-shaped magnetic circuits, in the lower part of which there were passed through the walls this assembly unit of the device focusing nozzles, located, in turn, in the mounting sleeves. The number of such magnetic generators fixed on each installation spiral passing through the device casing was from nine to eighteen units.

The F-shaped magnetic contours that process the raw materials are mounted on the surface of the device’s body in such a way that the focusing nozzle in them, located in the mounting cavity of the mounting sleeve, passes through the case walls in a radial direction relative to the longitudinal axis of symmetry of this assembly (i.e., at an angle 90 ° to the installation spiral line).

The angles at which the blasting nozzles 0 were fixed were equal to 30-45 ° (both tangential and radial) relative to the surface of the housing on which they were mounted. The installation of these nozzles 10 was carried out in exactly the same way as the processing magnetic circuits 11, that is, also using three mounting spirals. In the feed hopper 2, which is a part of the removable sleeve cap 4, which is directly included in the removable cap 4, 60 liters of the initial raw material mass were charged before starting the process of producing metal zirconium. The latter consisted of two-component (dry residue plus water) mud-like water suspension obtained by mixing small, consistency of powder, particles of titanium, iron and zirconium ore in a given volume of water. The solid components used in the composition of this initial raw material product, forming the so-called “dry residue” in it, were obtained from the nearest processing plants where concentrates were made from quarry ore rocks being developed nearby, in order to further use the resulting product to satisfy the relevant the needs of existing metallurgical production.

Before starting the preparation of the raw water suspension, an operation was carried out to break up the pieces of ore concentrates of the pieces that are described above into fine particles, carried out using a conventional ball mill. Before crushing pieces of rock, dosing of the ore concentrates used in the "dry residue" of the used raw material mixture was carried out, ensuring the formation of the latter with the specified technology by the content of its initial components (compounds Ti; Fe; Cr; Zr).

Obtained during the "ultrafine grinding" particles of the feedstock had overall dimensions in the range from 0.001 to 0.008 mm. The processing time of the above volume of raw materials using this kind of "three-helix" magnetic system containing F-shaped processing magnetic circuits with radial focusing nozzles, and using the previously indicated range of magnetic field strengths, averaged 35-45 minutes. The yield of the finished metal single crystal, calculated on the use of 60 liters of raw aqueous suspension for its production, reached a value of 18 kg to 21 kg (30% -35%) of the total volume used in processing it). These indicators come close enough to the theoretically possible limit that determines the total amount of metal multicomponent alloy produced from the initial mass of the raw material at the percentage of titanium, iron, chromium and zirconium compounds used in the processing process and including this component used ore rocks.

The proposed method for producing the above alloy is performed at room temperature (17-27 ° C), and the processing of the feedstock is carried out under the action of compressed air jets supplied to the zones of structural transformations under an overpressure of 0.4 ÷ 6.0 kgf / cm ² .

The technological modes assigned for the processing of initial raw materials are the intensity of the rack magnetic fields, the frequency of oscillations that create these fields of current pulses, the processing time, the amount of excess pressure in the volumes of compressed air supplied to the raw material (etc., etc.) .d.), assigned on the basis of considerations of the formation of the most optimal conditions for accelerated flow specified by the technology for producing a multicomponent alloy structural transformations included in the ore with metal unions into this necessary finished product itself.

The percentage in the mixture of "dry residue formed from solid particles used to obtain the metal of the original ore rocks in the composition of the aqueous suspension used in the processing is determined based on the presence of the following factors.

When the concentration of this component component in the latter is less than 40%, the raw material used automatically turns into “poor”, which negatively affects the performance indicators of the process of processing raw materials, since the yield of the required finished product is significantly reduced. With an increase in its content above a value of 70%, the processed raw material sharply reduces the indicators determining the degree of its plasticity. This, in the end, significantly complicates the process of moving it from the volume of the loading hopper into the cavity of the mobile working chamber, as well as the subsequent transfer of the microportions of this material that make up the mass of raw materials through the zones for generating processing magnetic fields located in it.

The particle sizes used to obtain an aqueous suspension of ore rocks, the dimensions of which are determined by a value of 0.001 ÷ 0.008 mm, are determined on the basis of the need to form with their use a “stable” plastic mud-like raw material mass.

The latter should not be stratified into its individual components for the time period necessary for the complete completion of the processing process.

To perform the process of producing an alloy based on titanium, iron, chromium and zirconium, carried out using the proposed method, a mixture was used consisting of ore concentrates containing both titanium and iron, chromium and zirconium compounds (respectively, “ilmenite”, magnetic “iron ore” "And" zirconite ").

Ore rocks used as the main initial components to obtain the necessary raw material contained in their composition:

I. Titanium concentrate "ilmenite":

1. TiO ₂ - 49%;

2. Fe ₂ O ₃ - 22%;

3. FeO - 19%;

4. Cr ₂ O ₃ - 3.6%;

5. Al ₂ O ₃ - 2%;

6. CaO - 0.2%;

7. MgO - 0.07%;

8. SiO ₂ - the rest, up to 100%;

II. Magnetite Concentrate:

1. Fe ₃ O ₄ - 75%;

2. Fe ₂ CO ₃ (spar iron ore) - 12.6%;

3. FeO ₃ - 6.5%;

4. Cr ₂ O ₃ - 3.2%;

5. Al ₂ O ₃ - 1.1%;

6. CaO - 0.3%;

7. MgO - 0.06%;

8. SiO ₂ - the rest, up to 100%;

III. Zirconium concentrate

1. ZrO ₂ - 66%;

2. Hf - 1.8%;

3. SiO ₂ - 30.1%;

4. Al ₂ O ₃ - 0.52%;

5. Fe ₂ O ₃ - 0.44%;

6. TiO ₂ - 0.62%;

7. U ₂ O ₃ - 0.022%;

8. P ₂ O ₅ - 0.091%;

9. Other elements - impurities present in the earth's crust, the rest is up to 100%.

Before grinding all three of the above rocks, they were pre-dosed, ensuring the content of the latter in the so-called "dry residue" used in the preparation of a viscous aqueous suspension in the following amounts:

- titanium ore - 44-45%;

- iron ore - 14-15%;

- zirconium rock - the rest, up to 100%.

When carrying out all the experiments listed below to obtain alloys based on titanium, iron, chromium, zirconium using the proposed method to achieve this goal, we used the same type of raw material containing the above components, including titanium, iron, chromium, zirconium compounds having the same, previously noted composition.

Before the preparation of the aqueous suspension loaded into the processing device, pieces of the initial ore component used in it were crushed using a ball mill to obtain from these bulk materials that were previously included in these large-sized particle formations, the dispersion of which corresponded to a value of 0.001-0.008 mm.

The finished end product formed at the end of the processing process was a columnar ring single crystal consisting of the corresponding elements indicated above, and tails, fine-grained slag waste, were formed from the impurities that are part of the ore used. Milled into small particles, that is, to a “powder” state, containing titanium, iron, chromium and zirconium compounds, the initial ore rocks were then poured with a predetermined treatment technology with a volume of water, and mixed in it until all of the above raw materials were homogeneous viscous plastic mud-like suspension.

After the manufacture of the latter, the mass of the dirt-like substance formed during this operation was loaded directly into the loading hopper of the device used to obtain the multicomponent alloy.

Further, the process of implementing the proposed method is illustrated using a number of examples below.

Example 1. In the feed hopper 2, having a volume of 60 l, was placed an aqueous suspension containing a raw material mixture, which included titanium, iron and zirconium ore. The ratio of all these components of the aqueous suspension and the previously listed components of the so-called “dry residue” used in it corresponded to the previously indicated. The content of this “dry residue” in the volume of the aqueous suspension used during the treatment was 40% (24 kg). The remaining mass of the load was represented by water - 60% (36 liters).

After completion of the loading operation of the source material being processed 1 and the completion of the operation for releasing the inner cavity of the hopper 2 from it, from where the mud-like water suspension through gravity hatch “B” by gravity entered directly directly into the space of the mobile working chamber, the following were simultaneously turned on:

- an external drive of the device, providing reciprocating movement of the roller 8, as well as kinematically connected with it by the working chamber itself, while simultaneously performing angular rotations around its own longitudinal axis of symmetry;

- all winding coils 13 included in the magnetic circuits 11 were connected to the electronic unit present in the circuit of an external source of electrical supply, the presence of which provided a supply to the above-mentioned elements of the pulse packets, each of which had the form of a “rail with trapezoidal teeth” ";

- through all the blowing nozzles 10 located on the housing 6 of the device began to be supplied with streams of compressed air.

Its receipt to the above-mentioned blowing elements 10 from an external supply line in this example was carried out under an overpressure of 0.4 kgf / cm ² . The tension generated in the cavity of the working chamber and having the form of a kind of spiral-shaped “cylindrical” “fringe” of “rack-shaped” magnetic fields corresponded to a value of 9 × 10 ⁴ A / m.

The frequency of arrival of pulses having the configuration of a "rectangular trapezoid" on the winding coils of 13 generators 11 was 12 units for one hour.

The mobile working chamber moved from the loading zone to the front “right” end of the device body 6, and then back to its original “left” position at a speed of 40 mm / min. Moreover, she made revolutions around her own longitudinal axis of symmetry. The number of the latter was 4 rpm. When making the transition from “direct displacement” of the working chamber to “reverse”, the direction of rotation of the structural components making it was reversed, which changed to the opposite.

The time of the entire processing cycle of the starting raw material 1 in the total result was 45 minutes (0.75 hours).

The raw material mass 1 moving, as it were, "back and forth" together with the movable working chamber under the influence of the magnetic radiation generated in the device, generated by the generators 11 and the focusing nozzles 14, was transformed into a columnar ring single crystal "I" upon completion of the processing process. The latter was deposited directly on the slag waste layer “Ж”, covering the lateral surface of the spacer rod-seed 7, and consisted entirely of the previously mentioned Ti elements; Fe; Cr; Zr.

The color tone of the obtained single crystal was dark gray. The mass of the finished product thus obtained was consistent with a value of 11.2 kg. The weight of the processing of fine-grained slag waste was 7.6 kg. The rest of the mass of the original raw material was spent on the formation of volatile gas compounds that were ejected from the cavity of the device into the outside atmosphere.

Example 2. The processing of the mass of the feedstock was carried out in accordance with the same scheme as was indicated in example 1.

The initial raw material mixture contained a “dry residue”, the amount of which, relative to the total volume of water suspension used, was 70% (42 kg). The remaining volume of the initial product was water - 30% or 18 liters. The air supply to the processed raw materials was carried out under excess pressure equal to 6.0 kgf / cm ² . The working chamber was moved with the source material loaded into it at a speed of 60 mm / min, and the angular rotation of the structural elements included in it was carried out at a value of this parameter corresponding to 2 rpm.

The tension generated in the volume of the working chamber and forming there a spiral-shaped cylindrical magnetic fringe - the “palisade” of physical fields corresponded to 1.1 × 10 ⁵ A / m. The number of 11 magnetic impulses passed through the coil windings of 11 magnetic generators was equal to the value of 7 units passed through the magnetic signal generators for one hour.

The processing time under these conditions corresponded to a period of 30 minutes (0.5 hours). The weight of the columnar ring single crystal obtained at the end of this process, consisting of the metals listed above, was 22.2 kg.

The color cast of the multicomponent single crystal obtained in the device can be characterized as light gray.

Example 3. The processing obtained from the particles of the original ore rocks of the raw material suspension was carried out in accordance with the same scheme as was already indicated in examples 1,2.

The content of the so-called "dry residue" in the composition used in the processing of the aqueous suspension formed from particles of the initial raw materials included in its mass was 60% of its total amount or 36 kg. The remaining volume of the raw suspension was water - 40% (24 liters).

The supply of compressed air through the blowing nozzle 10 was carried out under an overpressure of 4 kgf / cm ² .

The longitudinal movement of the working chamber along the housing of the device was carried out at a feed rate of 50 mm / min. The angular rotation speed of its constituent elements was equal to a value of 2.8 rpm.

The intensity of the processing magnetic fields generated in the volume of the working chamber was 1.0 × 10 ⁵ A / m. The number of 13 "trapezoidal rack pulses" suppressed to the coil windings supplied from an external power source to the coil windings of the magnetic generators was 10 units supplied to these signal elements for one hour.

As a result of the processing process of the used feedstock, carried out for 36 minutes (0.6 hours), a columnar ring single crystal was formed on the seed rod 7, including Ti; Fe; Cr; Zr. The weight of the obtained crystal was 19.4 kg.

The remaining mass of raw materials used to produce the finished product was spent on the formation of finely dispersed slag waste 9.4 kg, as well as volatile gas compounds sent to the external atmosphere.

From all the examples presented above it is clearly seen that the formation of an alloy based on titanium, iron, chromium and zirconium, synthesized in the form of a columnar ring formation, and also having good indices of its refractoriness obtained during the process of its manufacture, can be carried out using widely used and long used to meet the relevant needs of the current metallurgical production of ore concentrates, without any additional ny operations for their post-treatment or appropriate revision.

This ring-shaped single crystal obtained in the device used, as it were, consists of granules adhering to each other, which are like rectangular plates with overall dimensions of 40 ÷ 60 mm × 20 ÷ 30 mm × 8-12 mm;

The thickness of the formed manufactured columnar annular wall formation usually ranges from 5-8%.

The aforementioned crystalline formation is easily “broken” into separate, previously “pieces” of its “plate,” when even minor mechanical forces are applied to it.

Obtained during the implementation of the proposed processing method, among others, included in the multicomponent alloy of the components involved in the formation of the body of the annular columnar crystalline formation made in the device in this way, the chromium element, as obviously follows from the analysis of the formulation of the used initial ore rocks, is present in the volume of the latter as a contaminant contaminant that accidentally fell into their total mass. If it is not present in the composition of the ore materials due to the fact that certain features of the formation of quarry deposits are found, of which the latter are mined, a small amount of rock may be included in the composition of this raw material mixture, which includes compounds containing this element.

In the above cases, such a technological method was not used, since in the recipe of the used ore rocks the previously mentioned “desired” element was as if initially “automatically” turned on.

Obtained in accordance with the previously indicated technological scheme (examples 1; 2; 3) of the processing of the initial ore raw materials, a multicomponent alloy comprising titanium elements; iron; chromium; Zirconium has the following set of its own technical characteristics:

1. Formed in the form of an annular columnar formation, a multicomponent alloy contains its constituent elements in the following percentage ratio:

Ti - 41.8 ÷ 42%; Fe - 17.9 ÷ 18%; Cr - 1.1-1.2%; Zr - the rest, up to 100%.

2. The specific volume of the fabricated alloy is 6.8 g / cm ³ ;

3. The melting point Tm - 8290 ° C;

4. The specific volume resistance is 36.2 H⋅Ohm⋅m;

5. External surface hardness HRC - 62-64 units.

6. Tensile strength σp - 0.4 GPa;

7. Shear modulus - 28 GPa;

8. Young's modulus - 92 GPa;

9. A sample made of the above multicomponent alloy made in the above manner does not react with a 30% aqueous solution of concentrated "strong" inorganic acids (H ₂ SO ₄ ; HNO ₃ ; HCl) while holding this previously made crystalline formation for at least 120 hours . The exact same picture is observed when a sample containing the above alloy is immersed in an aqueous solution of KOH or NaOH with a content of the above components of 300 g / liter (the duration of the tests is the same 120 hours). At room temperature, an article made from a titanium, iron, chromium, zirconium-containing alloy does not react with a 50% aqueous solution of concentrated hydrofluoric acid (HF). Its interaction with hydrofluoric acid begins to occur at a heating temperature of his body exceeding a value of 350 ° C.

The samples made of the multicomponent alloy made earlier by the method are well processed using standard metal-cutting and press-forging equipment.

In the future, in the materials presented below, structural principles are set forth in accordance with which the device itself used to carry out this method is implemented.

The presence of the latter, in turn, ensures that in the process of applying this unit, the necessary positive effect is obtained.

The drawings show a device for implementing the proposed method for producing a multicomponent alloy based on titanium, iron, chromium and zirconium.

Figure 1 is a longitudinal section - a diagram of the device with the main installed on its body, providing the processing of raw materials functional, serving the above process, nodes.

Figure 2 is a cross-sectional view of the device housing along AA, passing directly through its working chamber with a columnar ring single crystal of a multicomponent alloy forming in it.

Figure 3 - image of the node 1 (see figure 2), which on an enlarged scale shows the installation of the F-shaped power magnetic circuit 11 on the housing 6 used in the processing of the device.

Figure 4 - node II (see figure 2), with the image fixed on the housing 6 of the device blowing nozzle 10, which feeds into the cavity of the last jets of compressed air.

Figure 5 - shows a diagram of the supply of "rack-shaped trapezoidal" current pulses sent to each of the windings - coils 13 that are part of the magnetic circuit 11, which perform the functions of solenoids in these magnetic generators.

On all these figures, in turn, are indicated:

Pos.1 - the initial raw material substance, with the use of which the necessary final product is obtained - a multicomponent alloy.

Pos.2 - loading hopper, into the cavity of which the processed feedstock, containing in its composition particles of the ore used, is placed before the start of the processing process.

Pos.3 - the right and left “cheeks” of the movable piston, forming the cavity of the working chamber, in the volume of which the metal constituting the alloy of metals from the initial ore compounds is restored.

Pos.4 - a removable cap, in the cavity of which the working chamber is loaded with the processed raw material, as well as after its dismantling, and the finished products are unloaded after the processing process is completed.

Pos.5 - a set of flat annular connecting flanges with quick-detachable threaded fasteners, with the help of which the removable cap 4 is docked with the device body 6, as well as its dismantling after the end of the processing of the original raw material.

Pos.6 - the device case is its fixed part, on the outer surface of which all power units serving the processing process are fixed, and screw reciprocating movement of the movable working chamber is carried out in its cavity. The volume of the internal space in the latter is formed between the right and left piston-shaped cheeks 3.

Pos.7 - an expansion rod - a seed on which the products of processing of the feedstock obtained in the volume of the movable working chamber are deposited, and also with the help of which the left and right cheeks 3 included in the translational moving in the cavity of the casing 6 of the aforementioned assembly are rigidly fixed node.

Pos.8 - a running roller attached to the left cheek of the working chamber, using which the latter can reciprocate in the cavity of the housing 6, and also perform angular rotations around its own longitudinal axis of symmetry.

Pos. 9 - a fixing nut mounted on a threaded shank — a bolt located at the very end of the rod — the seed 7, when unscrewed which creates conditions for free removal of the right piston-shaped cheek 3 of the working chamber, and thereby provides free access to the final products obtained in it carrying out processing.

Pos.10 - blowing nozzle mounted on the outer surface of the housing 6, and passing through its walls, and installed there in compliance with the specified technological parameters of the angles of its inclination - tangential β ° and radial α °, the value of which corresponds to a value of 30-45 °.

Pos.11 - F-shaped power magnetic circuits, providing when connected to an external source of supply "rack-shaped trapezoidal" pulses, the formation in their working elements 12 of the magnetic flux, incoming, in turn, to the body of the focusing nozzle 14.

Pos.12 - working elements made in the form of plates, with the mutual docking of which the body of the F-shaped magnetic generator 11 is formed.

Pos.13 - winding coils mounted directly in the body volume of the working elements 12, and performing the functions there creating individual magnetic fields of solenoids.

Pos.14 - pressed directly into the mounting technological hole in the body of the magnetic circuit 11, the focusing nozzle, with the help of which cylindrical clusters of magnetic lines of force - "K" rays "elongated" in length directed directly into the internal volume of the housing 6 are formed.

Pos.15 - installation of a hollow sleeve, rigidly fixed directly to the outer surface of the housing 6, the inner cavity of which is in communication with the volume of the latter, and in its upper part there is a threaded thread. With the help of its manufacturer, the connection of the inner surface of the installation sleeve with the external end threaded part of the focusing cylindrical nozzle 14 intended for installation in the same area.

Pos.16 - curvilinear insert washer, which ensures filling of the volume obtained when installing the F-shaped magnetic contour 11 of the recess directly adjacent to the inner side surface of the cavity of the housing 6, and eliminating the appearance of protruding sharp edges on the edges of this cavity (that is, it “smooths” »It during the fixing of the above washer" flush "with the plane of the inner cavity of this housing 6). The curved washer 16 is made of pressed directly into the last mass of small crumbs of magnetically conductive metal (for example, including cobalt sawdust or cast iron shavings).

Pos.17 - almost the same as in the previous case, the “smoothing” washer, the installation of which is also carried out in a curved recess formed during installation of the body of the blowing nozzle 10 passing through the walls of the body 6. The material for the manufacture of this kind of “leveling” element any sufficiently “slippery” plastic can serve - for example, elastic sheet rubber. This washer also has split “petals” diverging from its central opening to the periphery, which bend downward from its own core — the base, at the moment of passage of compressed air sent there through the cavity of the blowing nozzle 10.

Pos.18 - a pipe for the withdrawal from the internal cavity of the working chamber of the device of the portions of volatile gas compounds newly arising there during the recovery of metals and nonmetals, as well as excess volumes of compressed air received therein.

Pos.19 - pressure reducing valves, the opening of which is carried out at times when the overpressure in the working chamber begins to exceed the limits specified by the processing technology.

Pos.20 - the front end wall overlapping the cavity of the fixed part of the precast housing 6, with a hole made in the center for the passage of the moving roller body 8 moving in it.

In turn, in the presented images of figures 1-5, the letters indicate:

"A", "b", "c" - figure 5, individual pseudophases involved in the process of electric power supply and addressed to the winding coils 13 of the magnetic circuits 11, and, in turn, consisting of arranged in a certain order and sets of “rack-shaped trapezoidal” current pulses forming them.

In - hole-hatch connecting the cavity of the loading hopper 2 with the internal volume of the working chamber formed by the left and right "cheeks" 3.

G - installation cylindrical spiral lines laid on the outer side surface of the housing 6, on which are located processing magnetic circuits 11.

D - the same kind of spiral curves used to fix the blowing nozzles 10, supplying a stream of compressed air to the raw material.

E - formed in the inner surface of the housing 6, as well as in the volume of the mobile working chamber, a vortex-shaped jet air gas stable formation - "tornado".

And - obtained on the outer surface of the rod 7 columnar annular single crystal, consisting of a multicomponent alloy.

G - a loose layer formed on the plane of the same rod 7, obtained from fine-grained slag waste formed during ore processing.

K — clusters of force lines generated by magnetic circuits 11 formed in the form of straight cylindrical cylindrical formations, which, in turn, belong to force-processing physical fields created using focusing nozzles 14.

M is the cavity — cavity made at the lower end of the nozzle 14, with a configuration that maximally matches the outlines of the spatial rotation hyperboloid, and is designed to generate clusters of magnetic field lines, the shape of which almost completely duplicates that which is obtained by rotating around its own longitudinal axis of symmetry elongated in the length of the rectangle, spatial formation (i.e. imitates the shape of a figure made in the form of a segment of a round volume cylinder).

α ° - radial tilt angles (30-45 °), with the use of which the blasting nozzles 10 are fixed on the surface of the housing 6.

β ° - respectively, the tangential angles (30-45 °) of the same elements, determined relative to the lateral outer surface of the same assembly unit 6 of the device on which they are placed.

t ₁ t ₂ - segments along the abscissa axis (see figure 5), specifying the relative angular displacement of the components of the "pseudophase"a;b; in their individual impulses.

Based on the foregoing, it is imperative to carry out the necessary additional clarifications regarding the design features of the performance of the apparatus proposed for processing raw materials.

As can be clearly seen from the drawings presented in the application, the production of ring columnar "I" single crystals consisting exclusively of the previously listed elements - titanium, iron, chromium and zirconium, flows directly into the cavity of the mobile working chamber formed by the right and left cheeks belonging to it 3.

Its total length is 1/5 relative to the size of the same dimension, which determines the value of the corresponding similar parameter of the entire proposed design. The piston-shaped cheeks 3 are fixed in this node indicated above by “stringing” them onto the roller. In the process of their installation in the “regular” permanent position, the previously noted structural elements are passed along the lateral outer surface of this part, and reach the persistent end shoulders of the rod — the seed 7. When they reach the end position indicated here, they are finally fixed in it with threaded nuts 9 (see figure 1). The twisting of these fasteners 9 is carried out according to the thread made on the corresponding parts of the surface of the roller 8 (not shown). In addition, plastic sealing elements are installed on the outer side surface of the piston-shaped cheeks 3, forming a working chamber with an annular columnar crystalline formation grown in its volume, to insulate its volume from its external environment (not shown in the seal drawing). Upon completion of the processing process, the working chamber enters, ultimately, again in the cavity of the removable cap 4, occupying a fixed extreme position there.

The removable cap 4 after the placement of the aforementioned working chamber in it and the complete stop of the movement drives used in the device, as well as all the systems serving its operation, is disconnected from the fixed part of the housing 6. This kind of assembly is disassembled by releasing the coupling ring flat flanges 5 carried out by loosening and moving to the starting position used in the structure of the quick-release fastener assembly (not shown in the drawing). After removing the cap 4, the nut 9 was released, with the help of which the right cheek was fixed 3. The latter, in turn, is removed from the corresponding end of the roller 8 without completing any of the above transitions, thereby opening up free access to the annular columnar single crystal “And” located on the rod — the seed 7. This metal formation can then, without particularly noticeable efforts, be moved to the right, and then completely removed from the apparatus used to obtain it.

The roller 8, providing a “helical” movement of the working chamber during processing of the initial raw material mixture, is connected to the corresponding external drive, the presence of which allows the necessary changes in its angular positioning, as well as the translational movement of the constituent components of the latter along the cavity of the housing 6, to round-trip direction. That is, first to the front "right" end of the housing 6, and then from it to the very rear "left" part of this device.

For the installation of the processing magnetic circuits 11, a set of curved lines is used, consisting of three installation spirals “G”. Blowing nozzles 10, in a similar manner, are also fixed on the corresponding three curved paths "D", laid between the turns that make up the installation lines "G".

To prevent premature failure of the plastic sealing seals mounted on the outer side surface of the left and right cheeks 3, at the joints of the power units 10 and 11 used in the device, with the walls of the housing 6, the following technique is additionally applied.

In the zone of formation of the curvilinear cavity, resulting from the intersection of the above elements 10 and 11 of this design, with the lateral inner surface of the cavity of the fixed part of the housing 6, additional “smoothing” washers 16 and 17 are placed.

Their facing the volume of the cavity of the housing 6, the surface has a shape that completely copies the configuration of the curved cylindrical inner side surface of this assembly. That is, in the places of their own installation, with their mass, they “hermetically” overlap the mounting holes obtained during their passage, located on the corresponding surface of the body cavity, and some kind of cutting “edges” formed there, and at the same time form a “patch” there providing “perfect” coincidence and “alignment” between adjacent “adjacent” planes (as if connecting them “flush”).

In this case, the washer 16 is made of a finely dispersed metal powder pressed into the aforementioned curvilinear recess, having a low value of its specific magnetic resistance (for example, the latter is made from small cobalt particles).

The “smoothing” washer 17, in order to ensure the passage of 10 jets of compressed air formed in the nozzles, is made in the form of elastic rubber petals extending from the “central point”, which open at the moment of supply of the above product and close back under the influence of “pressing” they have a lateral outer surface that runs along the cavity of the body and has "sealing" cheek seals 3. The most successful material for the manufacture of the above structural element will be an elastic ezina.

In the same way, the docking areas are formed, the exhaust gases of the nozzles 18 with the internal cavity of the housing 6. In the area of the appearance of exactly the same curved recesses during installation of the latter, smoothing plastic washers are again placed, but in this particular embodiment they will be provided with through holes perforations large enough to allow the passage of microvolumes of volatile gas compounds, but at the same time too “small” to allow passage of solid particles through them ore rocks being abatable in the working chamber (the above unit is not shown in the drawing).

The installation of blowing nozzles 10 is carried out, as already noted, on three spiral cylindrical lines "D" with the formation of tangential β ° and radial α ° angles of inclination to the outer surface of the housing 6 at the points of their fastening. The value of the above angles is 30-45 ° .

The installation of magnetic F-shaped circuits 11 is carried out in exactly the same way using three cylindrical spiral lines “G” laid on the outer surface of the housing 6. The number of power nodes located on each of these three curved trajectories “G” is from nine to eighteen units.

Fastening of the F-shaped generators is carried out using the installation sleeves 15, the mounting internal cavity of which in the upper part is threaded (not shown in the drawing). The bushings 15 pass through the walls of the housing 6, forming an angle equal to 90 ° relative to its outer "convex" surface.

The assembly 11 itself, consisting of an F-shaped magnetic circuit, and a focusing nozzle 14 pressed into its lower part, also has a fixing mounting thread made on the outer side surface of the above element 14. At the time of the final fixing of the latter on the body 6, it is screwed into the sleeve 15, occupying the desired end position required by the device design (mating threads are not shown in the drawing).

The cavity recess “M” located in the lower part of the focusing nozzle 14, at its end, ensures the formation of a physical field with its magnetic, “radial-ray” lines “K”, which are very elongated and create a kind of “processing spiral cylindrical fringe. "

Each of the winding coils included in the F-shaped contour is connected to its “pseudophase” (or “a”; or “b”; or “c” - see Fig. 5) of an external power source that supplies it through the corresponding , the electronic circuit contained in it, sets of packets of “rack-shaped trapezoidal” pulses, electric current.

Each component constituting the last individual impulse has corresponding displacements - segments t ₁ ; t ₂ , marked in figure 5, relative to the same generated in adjacent "pseudophases" (in the drawing, the external power source is not shown).

Installation of the device case with the assembly units located on it on the most used technological base was carried out using a system consisting of ordinary mounting racks (these elements are not shown in the drawing).

To fix in the position specified by the processing technology, as well as to perform subsequent disconnection of the cap 4, a quick-release fastener system is used (not shown in the drawing).

The central hole in the front end cap-plug 20, through which the drive roller 8 passes, has seals installed on its inner side surface (not shown). Their presence provides isolation of the internal cavity of the fixed part of the prefabricated housing 6 from the external atmosphere, and at the same time, does not prevent the execution of the corresponding translations, both translational and rotational, used as part of the device a kind of "traction" element, that is, the above-mentioned roller 8.

The work of the proposed device when performing the processing of the source ore ore proceeds as follows.

After completion of the operation to fill with the raw material 1 the cavity of the loading hopper 2, mounted in the upper part of the removable cap cap 4, and also at the end of the process of emptying through the through hatch "B" (see figure 1), which is provided by spontaneous by leakage of a viscous aqueous suspension placed in it, the latter, subsequently, goes directly from there directly into the volume of the mobile working chamber, formed between the components of its right and left cheeks 3. After all The transitions listed above include:

- an external drive to move the roller 8 (in the drawing, an external drive is not shown). Simultaneously with the beginning of the implementation of the structural elements that make up the mobile working chamber, translational and rotational movements, all electrical windings-coils 13, which are the main component of the F-shaped magnetic circuits 11, located in turn on three encircling belts, are connected to an external power source the outer surface of the body 6 cylindrical spirals "G". Blowing nozzles 10 in the same way mounted on the surface of the fixed part of the assembly 6, similar to the above, and also using the same number of units used, curved lines "D", at the same time, are connected to the external supplying compressed air under excess pressure, the supply line (not shown in the drawing).

Thus, having a rigid kinematic connection with the roller 8, the working chamber with the processed raw material 1 placed in its cavity is pushed out of the internal volume of the removable cap cap 4, leaving the loading area, and begins to perform the process of translational and rotational movement in the inner cavity of the fixed part of the housing 6, in which it is, in the end, and "pushed". The outline of the path of movement of the processed raw material 1, which is picked up by the piston-shaped cheeks 3, located in the cavity of the aforementioned structural unit, moving from the feed loading zone to the front end of the housing 6, completely duplicates this configuration, which is formed during this kind of movement along the inner the surface of the housing 6, a spatial curved path.

The latter, due to the presence of the elements that make up the working chamber, the fact that they immediately act on two types of motion, both translational and rotational, ultimately, is a segment of a multi-turn helical spiral that is very elongated in length. Since the working chamber thus moved to a new position inevitably opens up access to its internal volume by jets of compressed air formed by blowing nozzles 10 mounted on the outer surface of the housing 6, which have both radial α ° and tangential angles of inclination β °, then located at the very bottom of the working chamber, the "bulk mass" of raw material 1 collapses a whole hail of a kind of "air strikes" generated in the area of the latter "crossing" at spatial angles s this product.

The presence of this kind of “behavior” features in the processing zone of the above-mentioned gas “flows” created in the cavity of the working chamber is provided by the obligatory influence on the above process of the specific design factors noted above used in the power elements used in the device (that is, the installation of blowing nozzles 10 along the encircling the outer surface of the fixed part of the housing 6 of the spiral lines "D", the presence of radial α ° and tangential β ° inclination angles - see figure 1, figure 2, figure 4).

Under the influence of continuously carried out and the above-mentioned intense force, the volume of this "bulk mass" of processed raw materials 1 is divided into small, previously constituting it "microportions", which are "pulled" in all directions by a vortex stream formed by the same air jets " E ”(tornado). When exposed to the raging currents in the body of the “E” vortex, these individual microvolumes, firstly, are transformed into small bubbles of gas-liquid aerosols, and, secondly, they are spread throughout the cavity of the mobile working chamber, uniformly filling almost all its parts, with the exception of the central zone, where a kind of small discharge is created (“eye of the storm”).

The whole mass of the raw material 1, completely transformed into the aerosol cloud in the aforementioned manner in the above manner, subsequently continues to perform complex curvilinear helical movement over all the inner zones of the device body 6, carrying it out together and simultaneously with the latter used and hermetically isolated from other volumes surrounding it space, the cavity of the mobile working chamber of this unit. Synchronously with all this, it is revealed that there is one more effect on the used processed raw material, which is necessary to obtain the finished final product specified by the processing technology and also artificially created in this device that specifically affects the applied raw material, an external force factor.

The thing is that when you turn on all the windings-coils 13 that are part of the magnetic generators 11, which are available in the device, into the external electric network, since they perform the functions of solenoids directly in the volume of the working elements 12 themselves, in which, in fact, the assembly of these structural elements of the machining F-shaped contours was carried out, individual magnetic fields are created almost instantly.

Due to the fact that the body of each generator 11 has a configuration of halves folded on top of each other - the eyes of the letter F, these newly arising fields merge into a single total circuit used for the processing process. Thus, the total flow circulating in a closed F-shaped loop of the body of the processing circuit is generated immediately by six windings. Each winding coil 13 is connected to its own, supplying "trapezoidal rack and pinion" impulse packets only for it, by a circuit-circuit of an external power source (not shown in the drawing).

Due to all this, the total field obtained in each magnetic generator 11 will have all the same characteristic features that are inherent to the same individual physical fields that form the latter (changes in the main parameters of such force formation are carried out in accordance with a schedule recording the behavior features of the “trapezoidal” functions, and also the fact that this total formation formed in this way necessarily has an angular displacement of its magnetic clusters power lines relative to neighboring lines, etc.).

Due to the fact that the upper tail of the focusing nozzle 14 is pressed into the lower crossbar of each F-shaped contour 11 (see Fig. 3), at the lower end of which a collecting cluster of magnetic field lines is made into a single cylindrical segment “K” focusing cavity, having the form of a spatial rotation hyperboloid, the total magnetic flux sent to it and received from six windings-coils 13 generates a technological processing physical field in the body of this nozzle 14, the outlines of clusters of field lines in said torus and possess in Figure 2; figure 3 "special" configuration.

Since the uniform arrangement of all magnetic generators 11 was made immediately on three spirals “G” encircling the body of the body 6, and the number of such processing loops on each curve of the installation line “G” is a number equal to nine to eighteen units, the presence of all of these above factors, ultimately, inevitably leads to the fact that in the cavity of the housing 6 of the device as if formed consisting of radially directed from the surface of the installation zone-base, directly directly to the center of the housing Cylindrical rotating magnetic clusters "K", a kind of technological processing system (see FIG. 2). The latter is a kind of spatial power cylindrical "fringe" consisting of individual logs collected in a "stockade". The number of such processing located in the internal volume of the housing 6 and consisting of cylindrical magnetic structures assembled into a spiral - spatial structures, respectively, in the embodiment of the device shown in FIG. 1, FIG. 2, FIG. 3 is, in total, at least three units.

It should also be noted that the technological processing systems included in the above, used to perform the recovery of metals and non-metals from their ore compounds, magnetic clusters “K”, consisting of a kind of cylindrical force formations - “logs”, periodically change their own geometric parameters (the electrical pulses supplied to power the windings-coils 13 are in the form of a "trapezoidal rail", and are shifted relative to each other by a certain, predetermined offset angle - see figure 5).

That is, their individual elements that make up such "barriers - fringe" - "logs" then "stretch" in height, then vice versa, sharply "shorten". Moreover, each “forming” the “three-way” “barrier” mentioned above, a separate picket fence, in the process of changing the height of its constituent elements, performs this periodically “renewed” kind of vibrational cycle with a shift in time of its conduct relative to the same as he, but neighboring, carried out in the adjacent located similar to this, installation spirals "G" (see the procedure for supplying "trapezoidal" pulses - figure 5). The action of the above circumstance is ensured by the fact that the pulses used in the feeding pseudophases "a", "b", "c" are offset relative to the same adjacent ones by angles of about 120 ° —the segments t ₁ ; t ₂ in figure 5.

As a result of the joint action of all the specific features listed above, the formation of power structural formations carrying out processing of raw materials carried away by vortex flows belonging to the jet air stream “E” (see FIG. 1), the “smallest” air-liquid aerosol bubbles formed in the working cavity cameras "raw cloud", move along with it along the fixed part of the housing 6. Moreover, the above components of such a "foam formation" as if forcibly "about askivayutsya "through quite often placed on the path of their movement obstruction log" ranks "- magnetic fences (manufacturing cylindrical" fringe ").

On small particles of the processed ore compounds, which are fastened onto a “film liquid base” of such “foam bubbles” formed in the cavity of the working chamber and moving in it, when the latter carry out this kind of “punching” through the spiral-shaped “magnetic fence” indicated above, it is as if applied entire series of multidirectional and intensively performed power energy strikes.

Since the movement of these microscopic ore components proceeds along rather complex spatial curved "twisted" trajectories, the rock layers that make up their body are always in the most optimal position for their further structural transformation, when access to the last microvolumes of raw materials for penetrating these particles " of magnetic rays - logs ”, it turns out to be practically unshielded in almost nothing. That is, the micro-volumes of compounds that make up small particles of “ore” rock are “pierced” by processing rotating cylindrical magnetic fluxes “K” using the entire range of directions of their possible spatial effects.

All of the above, facilitates the restoration of metal constituting an annular columnar crystal from small particles of ore compounds “glued” to the above “film” base, and also provides an increase in the percentage of the latter, the main constituent elements of it, Ti; Fe; Cr; Zr, and also also allows you to get a fairly high degree of completeness of the above recovery process. That is, ultimately, the application of the above techniques and guarantees the flow into the body of the crystalline formation synthesized during processing and the components of the volume of the multicomponent alloy obtained in it, necessary for its formation of the “main” elements included in it.

So, when carrying out the transfer of small particles of initial ore rocks carried away by “flying through” aerosol foam bubbles through an artificially created and having a proprietary technology configuration of their own magnetic spatial structure, small crystalline “nuclei” inevitably form in the jets of the “E” tornado, consisting of the above Ti metals; Fe; Cr; Zr.

The appearance, so to speak, of the "white light" of the microscopic "grains" noted above, entirely consisting of these elements, is ensured, first of all, by the obligatory presence in the surroundings of the "small" ore particles of the ions of the element that fill it in the air passing through the cavity of the working chamber - reducing agent, that is, a kind of "champion" in the framework of this specialization: carbon C ⁺⁴ . The latter is generated from molecules containing the aforementioned component of gases, always present in the composition of ordinary atmospheric air, which is supplied to the treatment zone under slight excess pressure.

The presence of the very fact of the occurrence of this, which is necessary for the bonding of the “liberated” during decomposition of the metal-containing atomic oxygen compound, the reducing ion, is again ensured by the “crushing” impact action exerted by those entering the vortex formation directly on the “span” path "E" of gas flows concentrated in a narrow section of power accumulations, consisting of logs collected in separate barriers, i.e. a kind of "beams" formed from magnetic lines belonging to the processing physical fields.

Like ore microscopic particles, upon encountering this spiral-shaped force palisade, carbon-containing gas molecules are separated into separate fragments, while ensuring the delivery of the “reducing” ion necessary for conducting the release of the “base” metals from their ore compounds (the latter is generated by decay into individual constituent gases CO ₂ ; CH ₄ ). The very subsequent movement of such layers, again emerging in the bulk of the “aerosol cloud”, in the spiral vortex flow “E”, crystalline nuclei, due to the continuous “proliferation” of these metal “grains” occurring in the same processing zone, continues to until their mass becomes so large that these "jet currents" will no longer have great potential to continue to support such, constantly increasing their overall dimensions of the "grain", by weight. Because of this, the latter stop their free “hovering” in the layers making up the “E” vortex flow, and then they move already under the influence of gravitational forces from the highest level occupied by the latter, which belongs to the aerosol cloud located in this region, as close to its lower parts. The process of increasing the initial dimensions obtained during the formation of crystals of a multicomponent alloy proceeds under the influence of two immediately accompanying this technology to synthesize the above finished finished product from the original ore compounds, which actively influence the course of its implementation, significant factors.

First, during the movement of aerosol bubbles directly in the thickness of the “tornado” formed in the cavity of the working chamber, these components of the “aerosol foam” inevitably collide with “flying” through these same regions of the above “vortex”, which reappeared in them and still very small crystalline "nuclei".

In the process of such a mutual “collision”, aerosol bubbles “flying” onto such solid “grains” of the alloy inevitably collapse, and the microscopic ore particles placed on their liquid film shell are “thrown” directly onto the outer surface of the “crashed” into this bubble is a metallic crystalline.

As a result of all this, the latter is covered, as it were, with a “raw fur coat” consisting of such small ore components “thrown” directly onto his body. Since the process of magnetic irradiation of all moving in the jet vortex formation “E” and the suspended microscopic ore component particles present in it does not stop there, this kind of specifically obtained “raw material shell” will almost inevitably be converted into a full metal coating in the future. The latter grows on the outer layers of such an alloy crystal, using it as a kind of substrate - the basis for carrying out its subsequent formation. That is, in this case, the “embryo", acquiring this kind of additional metal layer that is built up directly on its body, will inevitably increase its original overall dimensions.

Secondly, during the “flight” between the restrictive cheeks 3 of the working chamber, which carry out its small crystalline “grains” of the multicomponent alloy, also have a high degree of probability of a “point” getting into the “final” situation, in the event of which they inevitably come into close mutual contact (that is, their “head-on” collision occurs).

At the moment of implementation of the above mutual close contact, their subsequent “magnetic bonding” is inevitable, and, as an indispensable consequence of the fact that this circumstance exists, is the formation of a larger, composite structure from these tiny metal fragments.

It is understandable that both of the above factors for the enlargement of "nuclei of a multicomponent alloy" work in parallel and simultaneously. That is, as the length of the path along which the working chamber moves from its original initial position toward the front end of the housing 6 increases, sooner or later, all small “fragments” consisting of new crystalline nuclei synthesized directly in the cavity of the latter will thus , without fail, converted into large monolithic granules.

The latter, as already noted, upon completion of the process of their own enlargement, strive to move from the upper level of their “initial” location to the lowest zone of the device used for processing.

Performing the aforementioned vertical movement, some part of the thus formed sufficiently massive metal “flakes” can “accidentally” meet the surface of the seed rod 7 of the loose layer “F” that had previously settled on the lateral outer surface of the rod and formed from the finely dispersed “ sticky "slag waste. Due to the fact of the effect of such a “random hit”, these “overgrown” granules, with a rather high degree of probability, may simply be “tightly” “glued” into the enveloping seed-seed 7 loose non-metallic formation “G” (see Fig. 2), which has quite pronounced indicators of its own adhesion.

Due to the incessant influence of the technological factors listed above, these “adhering” particles of the multicomponent alloy will steadily continue the process of formation of more and more new body constituents of the structural formation of metal layers obtained there, based on the use of this “growth” aerosol foam volumes surrounding the latter on all sides.

The very process of deposition on the outer side surface of the seed rod 7 of the aforementioned intermediate slag layer "Ж", which is formed at the "start" stage of the implementation of the proposed processing technology, proceeds as follows.

Due to the fact that various kinds of compounds — impurities from other elements present therein — contaminants, which were obtained in the same way that were simultaneously released during the reduction of metals that contain the last ore particles and also directly enter their composition, are obtained in exactly the same way Since crystals are also transformed, ultimately, into grains of non-metallic slag waste, due to the presence of this circumstance, the following character will be observed in the cavity of the used mobile working chamber oh picture.

Consisting of particles of non-metallic waste sticking together, enlarged lumps of slag associates, making a “flight” in the thickness of the same “tornado” of “E” streams, and moving into them under the influence of the same force factors noted earlier, from the peripheral regions of the vortex “ E ”, to its core - the center, that is, such“ tail ”structural formations, ultimately, without fail, will end up as if moved directly into the zone of“ constantly maintained calm calm ”.

Due to the fact that the above-mentioned small slag “associates” adhere well to any surface that comes into close contact with them, they will thus form a loose intermediate non-metallic “sticky” layer “G” on the peripheral lateral parts of the body of the seed rod 7 , on which subsequently, "capture" and "fixation" of the "overgrown" granules of a multicomponent alloy obtained in the vortex flows moving downward are carried out. In addition, and enlarged “flakes” of the same alloy that have flown past the outer surface of the seed rod 7, again, maybe a little earlier, maybe a little later they will be, as it were, obviously known, thrown back onto the plane of the expanding ring single-crystal structure “ And "(see figure 2).

The fact of the obligatory onset of this event is determined, first of all, by the presence of the influence of the next action, which determines the inevitability of the moment of its practical implementation, an essential technical circumstance.

Flying past the rod-seed 7, enlarged in the jets of the vortex, “grains” of alloy, ultimately fall either directly onto the split lobe membrane — washer 17 directly over the nozzle 10 inlet (see FIG. 4), or are located on the “intermediate” section - the “isthmus” adjacent to this zone itself, the surface of the bottom 6. Both those and other “pieces” of the alloy will be moved by the cheek surface 3 moving and periodically making angular rotations, from the original location of its intermediate “bazaar” ’”, directly to the central outlet of the jet of compressed air, an outlet made in the center of the above structural element 17.

Since the pressure created in the cavity of the working chamber by blowing nozzles 10 of the air flows is quite large (overpressure corresponds to 0.4-0.6 kgf / cm ² ), metal fragments from this alloy that have fallen into their last jets literally words are simply “kicked out” of the zone of their location, and are thrown up and to the side at oblique angles α ° and β °.

Having encountered any obstacle on the trajectory of this kind of “approach”, for example, the surface of the moving cheek - piston 3, these pieces of metal alloy bounce off it and change, as a result, the direction of their movement. In this case, there again appears a rather high probability that these “thrown up” metal “fragments” will be thrown directly onto the outer surface of the annular columnar formation “I” grown on the seed rod 7. Indeed, in this central zone of the working chamber, unlike all the others located on its periphery, "calm calm" always reigns, because the so-called "eye of the storm" is located in this area. If, even after this single “jump” is completed, a piece of metal flies past the surface of the “I” single crystal grown in the device, the previously indicated cycle of repeated “tosses” and “flights” will continue until this event nevertheless turns into "Practically realized."

Ultimately, the granules of this metal that “got” onto the surface of the “I” single crystal during the execution of a series of such “bounces” and “rebounds” “stick” to its body, and continue together with the constituents of this crystalline structure and previously settled on it body base layers to carry out a joint process of its further growth.

An increase in the uniformity of the distribution of thickness of the components of the annular columnar formation of “I” along its entire length of the walls, as well as an increase in the level of cleanliness of its outer surface during its formation, is ensured by the constant execution of a series of turns carried out with a small angular velocity (2-4 r / minute), around its longitudinal axis of symmetry.

To eliminate the possibility of the occurrence of “random” “gross” errors obtained by this formation in a circular shape, on the second, “reverse” segment of the path of its movement along the surface of the cavity of the housing 6, the direction of rotation of this crystalline structure “I” is reversed (it is reversed) .

All the above events, performed in the cavity of the mobile working chamber, occur and proceed in its volume throughout the entire cycle of its movement inside the case used for processing, this device itself. When this assembly unit reaches the extreme front “right” position; (a straight segment of the path of its movement has been completely traveled), the travel limit switch (not shown in the drawing) is triggered, and the translational movement of the working chamber begins with the transfer of its constituent structural elements, bringing them closer to the rear “left” part of the device body 6.

The direction of the angular displacement of the components of this chamber around its own longitudinal axis of symmetry, at this point in time, as already indicated, also changes to the opposite.

Thus, during the second, “final” stage of the cycle of its reverse movement, in the volume of the working chamber, the last stages of the process of forming the body of the “And” columnar ring single crystal synthesized on the seed rod 7 are completely completed, which ensures that the last specified processing technology produces high-quality “conditions” . That is, as if the “finishing" "refinement" of this already almost completely finished final product is carried out, until the required technical parameters are specified and specified by the technical conditions. Ultimately, moving in the opposite direction, the working chamber again returns to its original initial position it occupied, that is, it again falls into the cavity of the removable cap 4, in which its volume was previously loaded with the processed raw material 1.

In the process of passing through the working chamber of the corresponding areas of the housing 6, periodic “bleeding” of the volumes of newly obtained volatile gas compounds obtained from the particles of the original ore from the particles of the original ore from the particles of the original ore and the excessively received portions of compressed air supplied thereto was periodically “bleached” in the internal cavity. To carry out this operation, we used outlet pipes 18 fixed on the device casing 6, the cavity of which was connected to the volume of the working chamber at the moments of operation of the pressure reducing valves 19. The latter were opened if the overpressure in the cavity of the mobile working chamber exceeded the value specified by the processing technology .

The opening of the pressure reducing valves 19, in the end, provided the emission of gas volumes unnecessary for the process of forming the “I” single crystal directly into the outside atmosphere surrounding the device.

Since on the lateral outer surface of the right and left piston-shaped cheeks 3 that are part of the mobile working chamber, it is planned to install elastic “slippery” seals to seal its volume, then to prevent their premature failure (seals are not shown in the drawing), during manufacture the proposed device used the following design methods.

Formed in the places of installation communicating with the internal volume of the housing 6 and used in the device structural elements 10; fourteen; 18 curvilinear recesses, obtained as if by themselves when mutually crossing contacting each other mating curved surfaces of the bodies of revolution, are filled with smoothing washers (see figure 3 - position 16; figure 4 - position 17). The latter are made in the form of petal membranes with a “hole” in the center, installed in the area where the lower outlet openings of the blowing nozzles 10, and also the outlet pipes 18 are located, and elastic rubber is used as the material for the manufacture.

When carrying out the installation of the focusing nozzles 14 in the cavity of the mounting sleeves 15 (see Fig. 3), the above “curved” recesses on the inner surface of the housing 6 are filled “tightly” pressed into these cavities obtained on its inner surface — the cavity, with the powder consisting from small particles of cobalt or cast iron (washer pos.17 - figure 3).

And in this and in another case, the use of the above structural elements eliminates the possibility of forming sharp cutting edges on the nodes of its intersection with the surface of nodes 10, 14, 18 on the inner side surface of the housing 6. It turns out, as it were, “by itself”, that all the mating zones of the latter with the housing 6 are, as it were, “flush” with neighboring sections of its inner surface, and have absolutely smooth planes at the points of the possible passage of the cheeks 3 located on the outer outer surface - the pistons 3 and belonging them sealing seals.

The installation of the F-shaped magnetic generators 11 with the nozzles 14 located in their lower part on the surface of the housing 6 is carried out using rigidly fixed guide hollow sleeves 15, and through the use of fastening threads made on the mating surfaces of the above parts (see Fig. 3). To increase the accuracy of the mutual fixation of the structural components that are assembled into a single unit, 2 lock nuts can be threaded onto the mounting thread located on the outer surface of the focusing nozzle 14 (the above-mentioned performance features of these parts are not reflected in the drawing).

So, after a movable working chamber with a columnar ring single crystal obtained in its internal volume, consisting entirely of a set of elements included in the last and listed above, fully occupies its original initial position in the volume of a removable cap 4, and the fact of the occurrence of this event an appropriate signal will be received from the sensor used to fix its end position (for example, from the limit switch), all systems that service the installation are disconnected from external power sources (motion drive; electrical circuits of magnetic generators, supplying compressed air jets to nozzles).

Subsequently, from the housing 6, by disconnecting from each other the annular flat docking flanges, carried out using quick-release fasteners (not shown in the drawing), the cap cap 4 is removed. Then the locking nut 9 is unscrewed, fixing on the threaded neck of the roller 8 a piston-like left cheek 3, and the latter is “pulled out” from its former position, previously occupied in the above node. This opens up free access to the formed annular columnar crystalline formation "And" (see figure 2), and the latter without any special difficulties is removed from the cavity of this device.

Comfortable conditions for dismantling such a metal structure previously obtained in the device are ensured, first of all, by the fact that between the inner side surface of the hole formed at its center and the seed rod 7 there is an intermediate loose layer “G” (see figure 2), which consists entirely from slag waste accumulated in this area.

After removing the “I” crystal from the device, partially filling the central landing hole in it, finely dispersed grains consisting of “slags” are easily shaken from there when even a slight mechanical effect is applied to them.

The processing cycle on this can be considered completely completed. It is also necessary to dwell on the fact that the power supply windings can be connected — coils 13 of electric pulse generators 11, the corresponding power supplies (not shown in the drawings) are equipped with the necessary electronic circuits, with the help of which these signals are formed in the form of a “rail with trapezoidal teeth ", And are assembled into a kind of typesetting packets (as if in a" pseudophase "), the components of which the elements have corresponding angular displacements relative to similar neighboring ones (see Fig. 5), as well as the last incl. chayut in its composition and additional circuit, providing the possibility of adjusting the voltage and frequency fluctuations in the processing zone, "rack" of magnetic fields (i.e., the magnitude of current, voltage, frequency supplied electric signals).

As already noted earlier, due to the above changes in the main technological parameters of the processing of the used raw material mixture, consisting of the initial ore rocks, in the end, the opportunity arises to obtain a finished final product that has predetermined technical specifications for the drawing, its own qualitative technical indicators and positive properties.

The technical and economic indicators characterizing the degree of efficiency of the processing performed with its use, recorded during the use to achieve the above goals when applying this type of design of the proposed device, made it possible to determine the following.

With a device length of 1.5 meters and its width, taking into account the dimensions of the systems serving its operation of 1.2 m, as well as the case diameter of 0.44 m, and in the case of its operation in 3 shift modes, it is obtained 0.7 ÷ 0.8 tons of a multicomponent alloy, including titanium, iron, chromium and zirconium, within one day. The energy consumption per tonne obtained in accordance with the proposed technology of this multicomponent alloy is 2.7-3.2 thousand kW / h.

Given all of the above, we can come to the following conclusion. Using the proposed method for producing a multicomponent alloy, as well as the device used to implement this technology, provides a significant reduction in the cost of electric energy required for processing the feedstock into a finished final product. That is, the application of the proposed technical solutions creates the conditions for reducing its consumption by 8-15 times with respect to its quantity, which is necessary to obtain a similar product, but carried out using melts consisting of the elements formed above the alloy formed with the involvement of sufficiently complex technical systems created from various sorts and purposes of smelting and chemical units to achieve this goal.

In addition, if the processing process is carried out in accordance with the proposed method, the latter proceeds during only one technological transition, and no harmful substances are released into the environment noted above, inevitably accompanying the methods performed in accordance with the “classical” scheme obtaining the same final product.

It should also be noted that the multicomponent alloy itself, which is completely ready for the subsequent application, is formed in the form of an annular columnar cylindrical formation that has a practically unchanged intrinsic configuration and includes all the elements necessary for its construction that strictly preserve its own constancy, " automatically ”received in the body of the latter, its percentage concentration.

The crystalline formations synthesized in accordance with the proposed technological scheme on the basis of titanium, iron, chromium and zirconium have a whole set of rather high physical and mechanical characteristics, as well as the corresponding latest chemical resistance and refractoriness.

Ring cylindrical crystals made using the proposed technology can be used to meet the corresponding needs of existing industrial production, without carrying out any operations for their “final” refinement.

The introduction of the proposed processing process, as well as the device used during its implementation in production, does not require significant investment, and is not associated with the need to use significant labor and financial costs, as well as long periods of time necessary for the preparation of production.

The choice of materials and components included in the composition of the proposed device was made taking into account the possibility of using them as the latter similar, widespread and used in equipment designed to perform technologies similar to the above. This proposed device itself is characterized by a high degree of simplicity of its design and, as a result of this, has fairly good indicators of its own operational reliability.

Claims (2)

1. A method of producing an alloy consisting of titanium, iron, chromium and zirconium from an aqueous suspension of ore particles containing titanium, iron, chromium and zirconium compounds, including the generation of magnetic fields superimposed on portions of the processed raw material, the recovery of metals from ores with continuous mixing the raw material mass, followed by accumulation and formation of the product in the form of an annular columnar crystalline formation from an alloy consisting of titanium, iron, chromium and zirconium, and its discharge, while bottom of the raw material mass use an aqueous suspension containing particles of ore material in the form of a mixture of titanium, iron, zirconium ore with a dispersion in the range of 0.001 ÷ 0.008 mm and in the amount of 40-70% of the volume of the aqueous suspension, and the original ore material contains 44-45% zirconium ore, 14-15% of iron ore and titanium ore - the rest is up to 100%, while magnetic fields with a trapezoidal tooth magnetic field with a strength of 9 × 10 ⁴ ÷ 1.1 × 10 ⁵ A / m and pulse oscillation frequency are used as magnetic fields that form clusters in the form of power lines having a configuration as close as possible to the shape of the spatial formation obtained by rotating a elongated rectangle that rotates about its own longitudinal axis of symmetry, while the process of restoration and formation of the said annular columnar crystalline formation is carried out on a metal rod located in a sealed mobile working chamber installed in the case and making reciprocating movements, while perfect and a body of angular rotations relative to its own longitudinal axis of symmetry, with the supply to the layers of the raw material mass of gas jets consisting of compressed atmospheric air and carbon as a reducing agent present in the composition of the compressed gases, and mixing of the initial raw material by transferring it to the internal volume of the sealed working chamber , crushing and subsequent extrusion of individual microporities of the feedstock under the influence of shocks created by intersecting jets of compressed air entering under excess chnym pressure of 0.4 ÷ 6.0 kgf / cm ^2. 2. A device for producing an alloy consisting of titanium, iron, chromium and zirconium from an aqueous suspension of ore particles containing compounds of titanium, iron, chromium and zirconium, the method according to claim 1, containing a housing consisting of two parts, one of which is removable and made in the form of a cap removable cap connected using annular flat flanges with its fixed base in the form of a cylindrical shell with the formation of a prefabricated unit, while the length of the fixed base of the prefabricated unit is 80-85% of its entire length in the body cavity A sealed movable working chamber is installed, which is arranged for reciprocating movement, and the housing is rotatable relative to its own longitudinal axis of symmetry, the working chamber being provided with left and right cheeks in the form of pistons mounted on the roller and mounted between them core, focusing magnetic nozzles are generated through the walls of the fixed base of the assembly, generating clusters of magnetic field lines, mounting sleeves and blow-off nozzles intended for the entry of compressed atmospheric air jets into the body cavity and having both radial and tangential angles of inclination of 30-45 ° with respect to the surface of the body, with outlet pipes for outputting to the left and right halves of the fixed base of the assembly the external atmosphere of the excess gas accumulated in the working chamber, and in the upper part of the removable cap there is a feed hopper of raw materials, the volume of which is communicated through spine located beneath the working chamber.

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