CN110698662A - Preparation method of activating agent - Google Patents
Preparation method of activating agent Download PDFInfo
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- CN110698662A CN110698662A CN201910859169.5A CN201910859169A CN110698662A CN 110698662 A CN110698662 A CN 110698662A CN 201910859169 A CN201910859169 A CN 201910859169A CN 110698662 A CN110698662 A CN 110698662A
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- cardanol
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- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 230000003213 activating effect Effects 0.000 title claims description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims abstract description 48
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 21
- 238000006243 chemical reaction Methods 0.000 claims abstract description 20
- 238000003756 stirring Methods 0.000 claims abstract description 20
- JOLVYUIAMRUBRK-UHFFFAOYSA-N 11',12',14',15'-Tetradehydro(Z,Z-)-3-(8-Pentadecenyl)phenol Natural products OC1=CC=CC(CCCCCCCC=CCC=CCC=C)=C1 JOLVYUIAMRUBRK-UHFFFAOYSA-N 0.000 claims abstract description 16
- YLKVIMNNMLKUGJ-UHFFFAOYSA-N 3-Delta8-pentadecenylphenol Natural products CCCCCCC=CCCCCCCCC1=CC=CC(O)=C1 YLKVIMNNMLKUGJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- JOLVYUIAMRUBRK-UTOQUPLUSA-N Cardanol Chemical compound OC1=CC=CC(CCCCCCC\C=C/C\C=C/CC=C)=C1 JOLVYUIAMRUBRK-UTOQUPLUSA-N 0.000 claims abstract description 16
- FAYVLNWNMNHXGA-UHFFFAOYSA-N Cardanoldiene Natural products CCCC=CCC=CCCCCCCCC1=CC=CC(O)=C1 FAYVLNWNMNHXGA-UHFFFAOYSA-N 0.000 claims abstract description 16
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims abstract description 16
- PTFIPECGHSYQNR-UHFFFAOYSA-N cardanol Natural products CCCCCCCCCCCCCCCC1=CC=CC(O)=C1 PTFIPECGHSYQNR-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000004359 castor oil Substances 0.000 claims abstract description 16
- 235000019438 castor oil Nutrition 0.000 claims abstract description 16
- 239000002270 dispersing agent Substances 0.000 claims abstract description 16
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 16
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 239000012190 activator Substances 0.000 claims abstract description 13
- 238000001035 drying Methods 0.000 claims abstract description 10
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 238000010907 mechanical stirring Methods 0.000 claims abstract description 10
- 230000003472 neutralizing effect Effects 0.000 claims abstract description 10
- 238000005406 washing Methods 0.000 claims abstract description 10
- 239000013543 active substance Substances 0.000 claims description 27
- 239000006185 dispersion Substances 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 13
- 239000003153 chemical reaction reagent Substances 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 5
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 239000004576 sand Substances 0.000 claims description 5
- 238000007789 sealing Methods 0.000 claims description 5
- 239000000047 product Substances 0.000 claims 4
- 239000012467 final product Substances 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 abstract description 10
- 238000009775 high-speed stirring Methods 0.000 description 7
- 238000009472 formulation Methods 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 125000003277 amino group Chemical group 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 150000002430 hydrocarbons Chemical group 0.000 description 2
- 125000001165 hydrophobic group Chemical group 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 239000002280 amphoteric surfactant Substances 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Chemical group CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000002563 ionic surfactant Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
- C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of surfactants, and discloses a preparation method of an activator, which comprises the following steps: 1) dehydrating 5-10 parts of cardanol, 30-80 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.1-0.3 part of potassium hydroxide and 15-30 parts of castor oil, adding the raw materials under mechanical stirring at a high speed at the temperature of 140-270 ℃ and the pressure of 0.1-0.15 MPa, fully stirring for 5-15 min, and reacting at the temperature of 70-75 ℃ for 1 hour to obtain a reaction sample; 2) and then adding 30-80 parts of ethylene oxide into the reaction sample obtained in the step 1), then washing, neutralizing, drying and filtering to obtain a primary finished product, adding 0.1-1 part of dispersing agent, 0.1-1 part of emulsifying agent and 0.1-1 part of anti-settling agent, and stirring and mixing uniformly. The preparation method of the activator realizes the purposes of good dispersibility, good fluidity and good stability, further expands the application range of the activator and meets higher use requirements.
Description
Technical Field
The invention relates to the technical field of surfactants, in particular to a preparation method of an activator.
Background
Surfactant (surfactant) is a substance which is added in a small amount and can obviously change the interface state of a solution system, has fixed hydrophilic and lipophilic groups, can be directionally arranged on the surface of the solution, and has an amphiphilic molecular structure: one end is a hydrophilic group, and the other end is a hydrophobic group; the hydrophilic group is often a polar group, such as carboxylic acid, sulfonic acid, sulfuric acid, amino group or amino group and salts thereof, hydroxyl group, amide group, ether bond and the like may also be used as the polar hydrophilic group; the hydrophobic group is usually a nonpolar hydrocarbon chain, such as a hydrocarbon chain with more than 8 carbon atoms, and the surfactant is classified into an ionic surfactant (including a cationic surfactant and an anionic surfactant), a nonionic surfactant, an amphoteric surfactant, a compound surfactant, other surfactants and the like.
The existing surfactant preparation method is simple, various in structure type and good in surface performance, but the existing surfactant preparation method is not good enough in dispersibility, flowability and stability in the actual using process, and a large promotion space is provided.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a preparation method of an activator, which has the advantages of good dispersibility, good fluidity and good stability, and solves the problems that the existing preparation method of the surfactant has poor dispersibility, fluidity and stability, and has a great promotion space, and the application range of the activator cannot be further expanded due to the factors of poor oil repellency and interface bonding force of particles, so that the higher requirement is difficult to meet.
(II) technical scheme
In order to realize the purposes of good dispersibility, good fluidity and good stability, the invention provides the following technical scheme: a method for preparing an activator, comprising the steps of:
1) dehydrating 5-10 parts of cardanol, 30-80 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.1-0.3 part of potassium hydroxide and 15-30 parts of castor oil, adding the raw materials under mechanical stirring at a high speed at the temperature of 140-270 ℃ and the pressure of 0.1-0.15 MPa, fully stirring for 5-15 min, and reacting at the temperature of 70-75 ℃ for 1 hour to obtain a reaction sample;
2) then adding 30-80 parts of ethylene oxide into the reaction sample obtained in the step 1), then washing, neutralizing, drying and filtering to obtain a primary finished product, adding 0.1-1 part of dispersing agent, 0.1-1 part of emulsifying agent and 0.1-1 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use;
3) and (3) putting the mixture into a dispersion machine, uniformly mixing and dispersing the mixture by using the dispersion machine to finally form an active agent finished product with good dispersibility, good fluidity and good stability, cooling the active agent finished product, then putting the active agent finished product into a storage tank, and sealing and packaging the storage tank by using a capping machine.
Preferably, the activator finished product can be divided into HY 001, HY 002 and HY 003 according to different proportions.
Preferably, the disperser may be replaced with one of a ball mill, a sand mill and a homogenizer.
Preferably, HY 001 comprises the following raw materials in parts by weight: 10 parts of cardanol, 30 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 15 parts of castor oil, 0.3 part of potassium hydroxide, 80 parts of ethylene oxide, 0.1 part of a dispersing agent, 0.1 part of an emulsifying agent and 0.1 part of an anti-settling agent.
Preferably, HY 002 comprises the following raw materials in parts by weight: 7.5 parts of cardanol, 55 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 22.5 parts of castor oil, 0.2 part of potassium hydroxide, 55 parts of ethylene oxide, 0.55 part of a dispersing agent, 0.55 part of an emulsifying agent and 0.55 part of an anti-settling agent.
Preferably, HY 003 comprises the following raw materials in parts by weight: 10 parts of cardanol, 80 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 30 parts of castor oil, 0.3 part of potassium hydroxide, 80 parts of ethylene oxide, 1 part of a dispersing agent, 1 part of an emulsifying agent and 1 part of an anti-settling agent.
(III) advantageous effects
Compared with the prior art, the invention provides a preparation method of the activating agent, which has the following beneficial effects:
the preparation method of the activator comprises the steps of dehydrating 5-10 parts of cardanol, 30-80 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.1-0.3 part of potassium hydroxide and 15-30 parts of castor oil, feeding the raw materials at the temperature of 140-270 ℃ and the pressure of 0.1-0.15 MPa under the condition of mechanical stirring and high-speed stirring, fully stirring for 5-15 min, and reacting at the temperature of 70-75 ℃ for 1 hour to obtain a reaction sample; then adding 30-80 parts of ethylene oxide into a reaction sample, then washing, neutralizing, drying and filtering to obtain a primary finished product, adding 0.1-1 part of dispersing agent, 0.1-1 part of emulsifying agent and 0.1-1 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use; the active agent is placed into a dispersion machine, and is uniformly mixed and dispersed by the dispersion machine, and finally, an active agent finished product with good dispersibility, good fluidity and good stability is formed, so that the aims of good dispersibility, good fluidity and good stability are fulfilled, the application range of the active agent is further expanded, and higher use requirements are met.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
a method for preparing an activator, comprising the steps of:
1) dehydrating 5 parts of cardanol, 30 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.1 part of potassium hydroxide and 15 parts of castor oil, adding the raw materials under mechanical stirring and high speed stirring at the temperature of 140 ℃ and the pressure of 0.1MPa, fully stirring for 5min, and reacting at the temperature of 70 ℃ for 1 hour to obtain a reaction sample;
2) then adding 30 parts of ethylene oxide into the reaction sample obtained in the step 1), then washing, neutralizing, drying and filtering to obtain a primary finished product, adding 0.1 part of dispersing agent, 0.1 part of emulsifying agent and 0.1 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use;
3) and (3) putting the mixture into a dispersion machine, uniformly mixing and dispersing the mixture by using the dispersion machine to finally form an active agent finished product with good dispersibility, good fluidity and good stability, cooling the active agent finished product, then putting the active agent finished product into a storage tank, and sealing and packaging the storage tank by using a capping machine.
Preferably, the formulation shown in the first embodiment is HY 001.
Preferably, the disperser may be replaced with one of a ball mill, a sand mill and a homogenizer.
Dehydrating 5 parts of cardanol, 30 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.1 part of potassium hydroxide and 15 parts of castor oil, adding the raw materials under mechanical stirring and high-speed stirring at the temperature of 140 ℃ and the pressure of 0.1MPa, fully stirring for 5min, and reacting at the temperature of 70 ℃ for 1 hour to obtain a reaction sample; then adding 30 parts of ethylene oxide into a reaction sample, then washing, neutralizing, drying and filtering to obtain a primary finished product, adding 0.1 part of dispersing agent, 0.1 part of emulsifying agent and 0.1 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use; the active agent is placed into a dispersion machine, and is uniformly mixed and dispersed by the dispersion machine, and finally, an active agent finished product with good dispersibility, good fluidity and good stability is formed, so that the aims of good dispersibility, good fluidity and good stability are fulfilled, the application range of the active agent is further expanded, and higher use requirements are met.
Example two:
a method for preparing an activator, comprising the steps of:
1) dehydrating 7.5 parts of cardanol, 55 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.2 part of potassium hydroxide and 22.5 parts of castor oil, adding the raw materials under mechanical stirring and high speed stirring at the temperature of 205 ℃ and the pressure of 0.125MPa, fully stirring for 10min, and reacting at the temperature of 72.5 ℃ for 1 hour to obtain a reaction sample;
2) adding 55 parts of ethylene oxide into the reaction sample obtained in the step 1), washing, neutralizing, drying and filtering to obtain a primary finished product, adding 0.55 part of dispersing agent, 0.55 part of emulsifying agent and 0.55 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use;
3) and (3) putting the mixture into a dispersion machine, uniformly mixing and dispersing the mixture by using the dispersion machine to finally form an active agent finished product with good dispersibility, good fluidity and good stability, cooling the active agent finished product, then putting the active agent finished product into a storage tank, and sealing and packaging the storage tank by using a capping machine.
Preferably, the formulation shown in the second embodiment is HY 002.
Preferably, the disperser may be replaced with one of a ball mill, a sand mill and a homogenizer.
Dehydrating 7.5 parts of cardanol, 55 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.2 part of potassium hydroxide and 22.5 parts of castor oil, adding the raw materials under mechanical stirring and high speed stirring at the temperature of 205 ℃ and the pressure of 0.125MPa, fully stirring for 10min, and reacting at the temperature of 72.5 ℃ for 1 hour to obtain a reaction sample; adding 55 parts of ethylene oxide into a reaction sample, washing, neutralizing, drying and filtering to obtain a primary finished product, adding 0.55 part of dispersing agent, 0.55 part of emulsifying agent and 0.55 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use; the active agent is placed into a dispersion machine, and is uniformly mixed and dispersed by the dispersion machine, and finally, an active agent finished product with good dispersibility, good fluidity and good stability is formed, so that the aims of good dispersibility, good fluidity and good stability are fulfilled, the application range of the active agent is further expanded, and higher use requirements are met.
Example three:
a method for preparing an activator, comprising the steps of:
1) dehydrating 10 parts of cardanol, 80 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.3 part of potassium hydroxide and 30 parts of castor oil, adding the raw materials under mechanical stirring and high speed stirring at the temperature of 270 ℃ and the pressure of 0.15MPa, fully stirring for 15min, and reacting at the temperature of 75 ℃ for 1 hour to obtain a reaction sample;
2) adding 80 parts of ethylene oxide into the reaction sample obtained in the step 1), washing, neutralizing, drying and filtering to obtain a primary finished product, adding 1 part of dispersing agent, 1 part of emulsifying agent and 1 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use;
3) and (3) putting the mixture into a dispersion machine, uniformly mixing and dispersing the mixture by using the dispersion machine to finally form an active agent finished product with good dispersibility, good fluidity and good stability, cooling the active agent finished product, then putting the active agent finished product into a storage tank, and sealing and packaging the storage tank by using a capping machine.
Preferably, the formulation shown in the third embodiment is HY 003.
Preferably, the disperser may be replaced with one of a ball mill, a sand mill and a homogenizer.
The invention has the beneficial effects that: dehydrating 10 parts of cardanol, 80 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.3 part of potassium hydroxide and 30 parts of castor oil, adding the raw materials under mechanical stirring and high-speed stirring at the temperature of 270 ℃ and the pressure of 0.15MPa, fully stirring for 15min, and reacting at the temperature of 75 ℃ for 1 hour to obtain a reaction sample; then adding 80 parts of ethylene oxide into a reaction sample, then washing, neutralizing, drying and filtering to obtain a primary finished product, adding 1 part of dispersing agent, 1 part of emulsifying agent and 1 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use; the active agent is placed into a dispersion machine, and is uniformly mixed and dispersed by the dispersion machine, and finally, an active agent finished product with good dispersibility, good fluidity and good stability is formed, so that the aims of good dispersibility, good fluidity and good stability are fulfilled, the application range of the active agent is further expanded, and higher use requirements are met.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. A method for preparing an activator, comprising the steps of:
1) dehydrating 5-10 parts of cardanol, 30-80 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 0.1-0.3 part of potassium hydroxide and 15-30 parts of castor oil, adding the raw materials under mechanical stirring at a high speed at the temperature of 140-270 ℃ and the pressure of 0.1-0.15 MPa, fully stirring for 5-15 min, and reacting at the temperature of 70-75 ℃ for 1 hour to obtain a reaction sample;
2) then adding 30-80 parts of ethylene oxide into the reaction sample obtained in the step 1), then washing, neutralizing, drying and filtering to obtain a primary finished product, adding 0.1-1 part of dispersing agent, 0.1-1 part of emulsifying agent and 0.1-1 part of anti-settling agent, stirring and mixing uniformly for 40 minutes to obtain a mixed reagent, and keeping for later use;
3) and (3) putting the mixture into a dispersion machine, uniformly mixing and dispersing the mixture by using the dispersion machine to finally form an active agent finished product with good dispersibility, good fluidity and good stability, cooling the active agent finished product, then putting the active agent finished product into a storage tank, and sealing and packaging the storage tank by using a capping machine.
2. The method as claimed in claim 1, wherein the final product is classified into HY 001, HY 002 and HY 003 according to different ratios.
3. The method of claim 1, wherein the dispersing machine is replaced by one of a ball mill, a sand mill and a homogenizer.
4. The preparation method of the activating agent as claimed in claim 2, wherein HY 001 comprises the following raw materials in parts by weight: 10 parts of cardanol, 30 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 15 parts of castor oil, 0.3 part of potassium hydroxide, 80 parts of ethylene oxide, 0.1 part of a dispersing agent, 0.1 part of an emulsifying agent and 0.1 part of an anti-settling agent.
5. The preparation method of the activating agent as claimed in claim 2, wherein HY 002 comprises the following raw materials in parts by weight: 7.5 parts of cardanol, 55 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 22.5 parts of castor oil, 0.2 part of potassium hydroxide, 55 parts of ethylene oxide, 0.55 part of a dispersing agent, 0.55 part of an emulsifying agent and 0.55 part of an anti-settling agent.
6. The preparation method of the activating agent as claimed in claim 2, wherein HY 003 comprises the following raw materials in parts by weight: 10 parts of cardanol, 80 parts of 2, 4, 7, 9-tetramethyl-4, 7-diol-5-decyne, 30 parts of castor oil, 0.3 part of potassium hydroxide, 80 parts of ethylene oxide, 1 part of a dispersing agent, 1 part of an emulsifying agent and 1 part of an anti-settling agent.
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|---|---|---|---|
| CN201910859169.5A CN110698662A (en) | 2019-09-11 | 2019-09-11 | Preparation method of activating agent |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910859169.5A CN110698662A (en) | 2019-09-11 | 2019-09-11 | Preparation method of activating agent |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103554476A (en) * | 2013-10-31 | 2014-02-05 | 淄博德信联邦化学工业有限公司 | Method for preparing surfactant |
| CN105013391A (en) * | 2015-08-05 | 2015-11-04 | 吴俊宏 | Preparation method of surface active agent |
| US20160257848A1 (en) * | 2013-11-27 | 2016-09-08 | Dow Global Technologies Llc | Cardanol Modified Epoxy Polyol |
| US20160264714A1 (en) * | 2013-11-27 | 2016-09-15 | Dow Global Technologies Llc | Cardanol modified epoxy polyol |
-
2019
- 2019-09-11 CN CN201910859169.5A patent/CN110698662A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103554476A (en) * | 2013-10-31 | 2014-02-05 | 淄博德信联邦化学工业有限公司 | Method for preparing surfactant |
| US20160257848A1 (en) * | 2013-11-27 | 2016-09-08 | Dow Global Technologies Llc | Cardanol Modified Epoxy Polyol |
| US20160264714A1 (en) * | 2013-11-27 | 2016-09-15 | Dow Global Technologies Llc | Cardanol modified epoxy polyol |
| CN105013391A (en) * | 2015-08-05 | 2015-11-04 | 吴俊宏 | Preparation method of surface active agent |
Non-Patent Citations (1)
| Title |
|---|
| 孙阿惠;丁雷涛;郝磊磊;刘军海;: "聚氧乙烯型表面活性剂的研究进展" * |
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