CN108853605A - A kind of production application process adding the chitosan class water-soluble lubricating liquid in sheath - Google Patents

A kind of production application process adding the chitosan class water-soluble lubricating liquid in sheath Download PDF

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Publication number
CN108853605A
CN108853605A CN201810938414.7A CN201810938414A CN108853605A CN 108853605 A CN108853605 A CN 108853605A CN 201810938414 A CN201810938414 A CN 201810938414A CN 108853605 A CN108853605 A CN 108853605A
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China
Prior art keywords
sheath
pot
water
lubricating fluid
dissolution
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Pending
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CN201810938414.7A
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Chinese (zh)
Inventor
朱传锐
陈海超
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Guangdong Huitong Latex Products Group Co Ltd
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Guangdong Huitong Latex Products Group Co Ltd
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Priority to CN201810938414.7A priority Critical patent/CN108853605A/en
Publication of CN108853605A publication Critical patent/CN108853605A/en
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
    • A61L31/14—Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
    • A61L31/16—Biologically active materials, e.g. therapeutic substances
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
    • A61L31/04—Macromolecular materials
    • A61L31/042—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
    • A61L31/04—Macromolecular materials
    • A61L31/048—Macromolecular materials obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/20—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
    • A61L2300/216—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials with other specific functional groups, e.g. aldehydes, ketones, phenols, quaternary phosphonium groups
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/40—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
    • A61L2300/404—Biocides, antimicrobial agents, antiseptic agents
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2400/00—Materials characterised by their function or physical properties
    • A61L2400/10—Materials for lubricating medical devices

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Heart & Thoracic Surgery (AREA)
  • Surgery (AREA)
  • Vascular Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Molecular Biology (AREA)
  • Engineering & Computer Science (AREA)
  • Medicinal Chemistry (AREA)
  • Biomedical Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Preparation (AREA)
  • Orthopedics, Nursing, And Contraception (AREA)

Abstract

The present invention relates to a kind of production application process of chitosan class water-soluble lubricating liquid of addition in sheath, belong to condom manufacture technical field.The present invention is using propylene glycol, glycerine, butanediol as primary raw material, it is especially added with the moisturizer such as hyaluronic acid, amino acid humectant, chitosan derivatives, trehalose, pyrrolidone sodium carboxylate, carbamide, agitated uniform technique, make that entire moisturizing system is moist, thick and heavy, non-greasy, lubricating fluid is equably applied on sheath glue film again, or it is added dropwise on sheath, lubricate condom products more, with hemostasis, anti-inflammatory, wound healing, holding skin is promoted to moisten, it is smooth, prevent dry and obfuscation and other effects.

Description

A kind of production and application adding the chitosan class water-soluble lubricating liquid in sheath Method
Technical field
The present invention relates to a kind of production application process of chitosan class water-soluble lubricating liquid of addition in sheath, belong to Condom manufacture technical field.
Background technique
Sheath is common family planning articles in people's daily life, sperm and ovum when being mainly used for separating human sexuality The combination of son, prevents from being pregnant.In the modern life, with the propagation and sprawling of the various venereal diseases such as AIDS, in sexual life, Nan Xingpei Wearing condom is a kind of most simple and effective means to venereal disease is prevented.
Chitosan class lubricating fluid can increase lubricant effect, promotes voluptus, makes sexual life more harmonious, promote between husband and wife Emotion；It is more reduced skin injury simultaneously, reduces the harmful microorganisms such as bacterium, virus to the erosion chance of human body；Effectively The breakage for reducing condom, reduces the probability of accidental pregnancy.It is therefore proposed that a kind of chitosan class of addition in sheath is water-soluble The production and application process of property lubricating fluid.
Summary of the invention
The object of the present invention is to provide a kind of production and applications of chitosan class water-soluble lubricating liquid of addition in sheath Process, production method gained lubricating fluid have enhancing lubrication, easy to clean, anti-inflammatory, detumescence, inhibit bacterial growth, analgesic And other effects.
For realize foregoing invention purpose, the technical solution adopted by the present invention is as follows：It is a kind of to add the shell in sheath The production and application process of glycans water-soluble lubricating liquid, includes the following steps：
(1) with tap water cleaning aqueous phase dissolved pot, oily phased soln pot, each filter screen and pipeline, emulsion pot, then to water phase Pot, oily phase pot are added half pot of purified water in emulsion pot, and three pots are both heated to 115 degrees Celsius using steam, keep 5min Afterwards, it is discharged by all pipelines and valve；
(2) dissolution of raw material is used in water phase pot:
1. the dissolution of solid bacteriostatic agent：Propylene glycol 25%, lactic acid 0.5%, ethyl-para-hydroxybenzoate 0.03%, purified water 3.35%；
Purified water is weighed according to the proportion, P-hydroxybenzoic acid sodium, lactic acid is then added, and steam is heated to 50 ± 3 DEG C, stirring Propylene glycol is added after dispersion, keep temperature and stirs 35min, keeps liquid uniform；
2. sodium hyaluronate pulvis dissolves：Hyaluronic acid 0.32%, amino acid humectant 3%, chitosan derivatives 3.5%, sea Algae sugar 1.5%, purified water 5.8%；
It weighs according to formula, adds materials according to following sequence into purified water：Chitosan derivatives, trehalose, amino Sour moisturizer, hyaluronic acid, are stirred when adding material, store material dissolution can and using stainless steel barrel with cover；
3. the dissolution of Sodium Polyacrylate pulvis：Carbamide 1%, Sodium Polyacrylate 0.5%, purified water 4%；
It weighs, stirs evenly according to the proportion, and stored using stainless steel barrel with cover；
(3) dissolution of raw material is pre-mixed method in water phase pot：
1. 2. 3. water-soluble material was impregnated by dissolution in 1 hour, sealed storage is not shone directly at shady and cool drying by sunlight The place penetrated；
Weigh in formula 2. 3., put into water phase pot, under room ambient conditions, stir 30min, add 1., stirring 40min；
(4) raw material premix used in oily phase pot close method：
Weigh glycerine 22%, the butanediol 15%, pyrrolidone sodium carboxylate 14.5%, lactic acid 0.5% in formula, investment In oily phase pot, air intake valve is opened, keeps temperature of charge at 70 DEG C, after stirring 30min with the speed of 30 turns/min, checks material Uniformity coefficient, when reaching requirement, cooling save；
(5) two pots of material mixing：By the material in water phase pot and oily phase pot, by pipeline, while being put into emulsion pot, add It is stirred while material, makes the mixing of material more evenly, obtain lubricant；
(6) the pre- dropwise addition of lubricating fluid：Sheath is after molding drying, in the state that do not batch, first changes electronics inspection Equipment and technique are tested, after electronic checkout terminates and before batching, lubricating fluid 1g described in a dropping step (1) makes sheath Appearance it is more moist bright, when use, more lubricates, and solves sheath lubricant permeability problems；
(7) the inner packing addition of lubricating fluid：Naked sheath after being batched by electronic checkout, when into inner packing, Automatic dripping 0.10-0.80g lubricating fluid is needed, the permeability of this lubricating fluid is strong, and extensibility is good, can moisten entire sheath quickly Glue film；
Above-mentioned lubricating fluid is transparent, viscosity between 100~500CPS, lubricating fluid of the pH value between 5.5-8.
The beneficial effects of the invention are as follows：The rational proportion of the lubricant of the invention keeps entire moisturizing system moist, thick and heavy, no Greasy, lubricating fluid is equably applied on sheath glue film, or is added dropwise on sheath, lubricates condom products more, With hemostasis, anti-inflammatory, wound healing, holding skin is promoted to moisten, it is smooth, prevent dry and obfuscation and other effects.
Specific embodiment
The present invention is described in further details below by example, these embodiments are merely to illustrate the present invention, not It limits the scope of the invention.
Embodiment 1
Chitosan class water-soluble lubricating liquid of the production addition in sheath：
(1) first with tap water cleaning aqueous phase dissolved pot, oily phased soln pot, each filter screen and pipeline, emulsion pot, then to water phase Pot, oily phase pot are added half pot of purified water in emulsion pot, and three pots are both heated to 115 degrees Celsius using steam, keep 5min And agitating paddle is opened simultaneously, for the pasteurised completely inside equipment, the valve for flowing to emulsion pot is opened after the completion, makes all valves Door, pipeline, filter are by disinfection treatment；
(2) dissolution of raw material is used in water phase pot:
1. the dissolution of solid bacteriostatic agent：Propylene glycol 25%, lactic acid 0.5%, ethyl-para-hydroxybenzoate 0.03%, purified water 3.35%；
Purified water is weighed according to the proportion, P-hydroxybenzoic acid sodium, lactic acid is then added, and steam is heated to 50 ± 3 DEG C, stirring Propylene glycol is added after dispersion, keep temperature and stirs 35min, keeps liquid uniform；
2. sodium hyaluronate pulvis dissolves：Hyaluronic acid 0.32%, amino acid humectant 3%, chitosan derivatives 3.5%, sea Algae sugar 1.5%, purified water 5.8%；
It weighs according to formula, adds materials according to following sequence into purified water：Chitosan derivatives, trehalose, amino Sour moisturizer, hyaluronic acid, are stirred when adding material, store material dissolution can and using stainless steel barrel with cover；
3. the dissolution of Sodium Polyacrylate pulvis：Carbamide 1%, Sodium Polyacrylate 0.5%, purified water 4%；
It weighs, stirs evenly according to the proportion, and stored using stainless steel barrel with cover；
(3) dissolution of raw material is pre-mixed method in water phase pot：
2. 3. by dissolving within 1 hour or more the water-soluble material of immersion 1., need sealed storage at shady and cool drying, not by The place of sunlight direct irradiation；
Weigh in formula 2. 3., investment water phase pot 1. in, under room ambient conditions, stir 50min, aqueous phase dissolved mixing is not required to It heats；
(4) raw material premix used in oily phase pot close method：
Weigh glycerine 22%, the butanediol 15%, pyrrolidone sodium carboxylate 14.5%, lactic acid 0.5% in formula, investment In oily phase pot, air intake valve is opened, keeps temperature of charge at 70 DEG C, after stirring 30min with the speed of 30 turns/min, checks material Uniformity coefficient, when reaching requirement, cooling save；
(5) two pots of material mixing：By the material in water phase pot and oily phase pot, by pipeline, while being put into emulsion pot, add It is stirred while material, after stirring 30min with the speed of 30 turns/min, makes the mixing of material more evenly, obtain lubricant；
(6) the pre- dropwise addition of lubricating fluid：Sheath is after molding drying, in the state that do not batch, first changes electronics inspection Equipment and technique are tested, after electronic checkout terminates and before batching, lubricating fluid 1g described in a dropping step (1) makes sheath Appearance it is more moist bright, when use, more lubricates, and solves sheath lubricant permeability problems；
(7) the inner packing addition of lubricating fluid：Naked sheath after being batched by electronic checkout, when into inner packing, Automatic dripping 0.10-0.80g lubricating fluid is needed, the permeability of this lubricating fluid is strong, and extensibility is good, can moisten entire sheath quickly Glue film；The lubricating fluid is transparent, viscosity between 100~500CPS, lubricating fluid of the pH value between 5.5-8.

Claims (2)

1. a kind of production application process of chitosan class water-soluble lubricating liquid of addition in sheath, it is characterised in that：Including Following steps：
(1) with tap water cleaning aqueous phase dissolved pot, oily phased soln pot, each filter screen and pipeline, emulsion pot, then to water phase pot, oil Half pot of purified water is added in phase pot, emulsion pot, and three pots are both heated to 115 degrees Celsius using steam, after keeping 5min, leads to Cross all pipelines and valve discharge；
(2) dissolution of raw material is used in water phase pot:
1. the dissolution of solid bacteriostatic agent：Propylene glycol 25%, lactic acid 0.5%, ethyl-para-hydroxybenzoate 0.03%, purified water 3.35%；
Purified water is weighed according to the proportion, P-hydroxybenzoic acid sodium, lactic acid is then added, and steam is heated to 50 ± 3 DEG C, is dispersed with stirring After add propylene glycol, keep temperature simultaneously to stir 35min, keep liquid uniform；
2. sodium hyaluronate pulvis dissolves：Hyaluronic acid 0.32%, amino acid humectant 3%, chitosan derivatives 3.5%, trehalose 1.5%, purified water 5.8%；
It weighs according to formula, adds materials according to following sequence into purified water：Chitosan derivatives, trehalose, amino acid are protected Humectant, hyaluronic acid, are stirred when adding material, store material dissolution can and using stainless steel barrel with cover；
3. the dissolution of Sodium Polyacrylate pulvis：Carbamide 1%, Sodium Polyacrylate 0.5%, purified water 4%；
It weighs, stirs evenly according to the proportion, and stored using stainless steel barrel with cover；
(3) dissolution of raw material is pre-mixed method in water phase pot：
1. 2. 3. water-soluble material was impregnated by dissolution in 1 hour, sealed storage is at shady and cool drying, not by sunlight direct irradiation Place；
Weigh in formula 2. 3., put into water phase pot, under room ambient conditions, stir 30min, add 1., stir 40min；
(4) raw material premix used in oily phase pot close method：
Glycerine 22%, the butanediol 15%, pyrrolidone sodium carboxylate 14.5%, lactic acid 0.5% in formula are weighed, oily phase is put into In pot, air intake valve is opened, keeps temperature of charge at 70 DEG C, after stirring 30min with the speed of 30 turns/min, checks the equal of material Even degree, when reaching requirement, cooling is saved；
(5) two pots of material mixing：By the material in water phase pot and oily phase pot, by pipeline, while being put into emulsion pot, charging It is stirred simultaneously, makes the mixing of material more evenly, obtain lubricant；
(6) the pre- dropwise addition of lubricating fluid：Sheath is after molding drying, in the state that do not batch, first changes electronic checkout and sets Standby and technique, after electronic checkout terminates and before batching, lubricating fluid 1g described in a dropping step (1) makes the outer of sheath See more moist bright, when use more lubricates, and solves sheath lubricant permeability problems；
(7) the inner packing addition of lubricating fluid：Naked sheath after batching by electronic checkout needs when into inner packing Automatic dripping 0.10-0.80g lubricating fluid, the permeability of this lubricating fluid is strong, and extensibility is good, can moisten entire sheath glue quickly Film.
2. a kind of production and application side of chitosan class water-soluble lubricating liquid of the addition according to claim 1 in sheath Method, it is characterised in that：The lubricating fluid is transparent, viscosity between 100~500CPS, profit of the pH value between 5.5-8 Synovia.
CN201810938414.7A 2018-08-17 2018-08-17 A kind of production application process adding the chitosan class water-soluble lubricating liquid in sheath Pending CN108853605A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810938414.7A CN108853605A (en) 2018-08-17 2018-08-17 A kind of production application process adding the chitosan class water-soluble lubricating liquid in sheath

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810938414.7A CN108853605A (en) 2018-08-17 2018-08-17 A kind of production application process adding the chitosan class water-soluble lubricating liquid in sheath

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CN108853605A true CN108853605A (en) 2018-11-23

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117258052A (en) * 2023-11-22 2023-12-22 广州双一乳胶制品有限公司 Application of beta-1, 3-glucan in preparation of aqueous lubricant for condom

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1559625A (en) * 2004-02-16 2005-01-05 华南理工大学 Biological nursing liquid used for candom sarface and its preparation method
CN101172065A (en) * 2006-11-02 2008-05-07 上海金名流医疗器械有限公司 Oil filling technique in production process of condom
CN101773513A (en) * 2009-01-14 2010-07-14 邢建慧 Water soluble body lubricant with natural antibacterial components and with pH value consistence with pH value of vagina
CN102512338A (en) * 2012-01-13 2012-06-27 北京国联诚辉医药技术有限公司 Water-soluble human body lubricant and preparation method thereof
CN102989045A (en) * 2012-11-12 2013-03-27 梁忠品 Biocompatible water-soluble composition and use thereof
CN103405594A (en) * 2013-05-30 2013-11-27 石杰克 Water-soluble personal lubricant, preparation method thereof, and condom employing lubricant

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1559625A (en) * 2004-02-16 2005-01-05 华南理工大学 Biological nursing liquid used for candom sarface and its preparation method
CN101172065A (en) * 2006-11-02 2008-05-07 上海金名流医疗器械有限公司 Oil filling technique in production process of condom
CN101773513A (en) * 2009-01-14 2010-07-14 邢建慧 Water soluble body lubricant with natural antibacterial components and with pH value consistence with pH value of vagina
CN102512338A (en) * 2012-01-13 2012-06-27 北京国联诚辉医药技术有限公司 Water-soluble human body lubricant and preparation method thereof
CN102989045A (en) * 2012-11-12 2013-03-27 梁忠品 Biocompatible water-soluble composition and use thereof
CN103405594A (en) * 2013-05-30 2013-11-27 石杰克 Water-soluble personal lubricant, preparation method thereof, and condom employing lubricant

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117258052A (en) * 2023-11-22 2023-12-22 广州双一乳胶制品有限公司 Application of beta-1, 3-glucan in preparation of aqueous lubricant for condom
CN117258052B (en) * 2023-11-22 2024-03-01 广州双一乳胶制品有限公司 Application of beta-1, 3-glucan in preparation of aqueous lubricant for condom

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Application publication date: 20181123

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