CN106691976A - Plant extract capable of controlling oil and shrinking pores and preparation method and application of plant extract - Google Patents
Plant extract capable of controlling oil and shrinking pores and preparation method and application of plant extract Download PDFInfo
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- CN106691976A CN106691976A CN201710124571.XA CN201710124571A CN106691976A CN 106691976 A CN106691976 A CN 106691976A CN 201710124571 A CN201710124571 A CN 201710124571A CN 106691976 A CN106691976 A CN 106691976A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention relates to a plant extract capable of controlling oil and shrinking pores and a preparation method and application of the plant extract. The plant extract uses a rice fermentation liquid, a calendula extracting solution, an aloe extracting solution and mauritia flexuosa fruit oil as raw materials, the weights of the raw materials are properly proportioned, the prepared plant extract has a better effect of inhibiting secretion of oil, the rate of change of the content of oil of the skin before and after use is up to 24.58%, meanwhile, the plant extract can also shrink the pores excellently, and improves the problems of rough skin and coarse pore, the skin is finer and more smooth, in addition, the plant extract is from the natural plants, has no side effects, can serve as a functional additive of a skin care product to control oil and shrink the pores, and has a broad application prospect.
Description
Technical field
The invention belongs to technical field of skin care, and in particular to a kind of oil-control simultaneously receives the plant extracts and its system in fine, soft fur hole
Preparation Method and application.
Background technology
The problems such as being radiated with age increase, excessive social pressures, environmental pollution, computer is increasingly severe, therewith to skin
Skin causes many harmful effects, and the people of combination is more and more, except some are born combination, also one
Groups of people are to become combination with pressure, also before be neutral skin or Oily, also can be with age, ring
Border etc. becomes combination.
Sebum be by skin inside sebocyte cell generation, be then secreted into the oil of skin surface.Combination or oil
Property skin formation precisely due to what skin oil and fat hypersecretion was caused, fat secretion is excessive, the grease support that pore can be stacked
Greatly.Pore is thick to be often as excessive hormone in vivo parasecretion, pressure and the reason such as environmental pollution, cleaning are not carried out
Cause.Additionally, with the increase at age, skin gradually follows the string, perifollicolar lacks supporting construction, is also easy to make hair
Hole seems than larger；The thick greatest problem for being to perplex oiliness and mixing skin of pore.Additionally, sunshine is strengthened, metabolism adds
The factor such as fast causes skin ingress of oil more vigorous, and pore may appear to thicker.
Excessive grease is deposited in pore, only can be more crowded bigger by pore.Grease is wrapped in skin can become hoary hair
Acne；Burst through meets air oxidation blackening, will form blackhead, and more serious even can deteriorate into acne.Acne
Formed, the grease that should be exactly ejected from pore originally, because the hyperkeratosis of hair aperture periphery blocks mixed product
Thing, so, when acne more product, the more, pore also can more be supportted bigger.
At present, in existing cosmetics, in order to control or adjusting sebum secretion, mainly using some Oil suction powders into
Point, such as silica, polymethyl methacrylate, nylon powder, boron nitride powder, talcum, titanium dioxide, zinc oxide, silicon
Body etc..These compositions are from synthetic ingredient or mineralogical composition, in addition to absorbing the ability of sebum, it is difficult to further
Effect.And the current cosmetics in order to modify enlarged pores, mainly use the silty particles such as filling silicide quickly handle
Pore is filled up, and described silty particle is generally also equipped with the optical effects such as soft focus, refraction, allows pore to seem less bright
It is aobvious, but can not fundamentally change the fact that pore is thick.In addition, also have to use chemicals composition to reach reduction skin
Fat generates and reduces the way of pore effect, for example with compositions such as 5 alpha reductase inhibitors to control fat secretion amount, but changes
The side effect for studying point is big, brings the other problemses of skin.
The content of the invention
In order to solve the above mentioned problem of prior art presence, carried the invention provides a kind of oil-control and the plant of receiving fine, soft fur hole
Take thing and its preparation method and application.The oil-control effect of the plant extracts is good, with the effect of fine, soft fur hole is received, has no side effect, can
As skin care item oil-control and the functional additive in fine, soft fur hole is received, be with a wide range of applications.
The technical solution adopted in the present invention is：
A kind of oil-control simultaneously receives the plant extracts in fine, soft fur hole, and raw material components include：
Rice zymotic fluid, 15-25 weight portions；
Pot marigold extract solution, 25-35 weight portions；
Aloe leaf extract, 15-25 weight portions；
The auspicious palmitic acid fruit oil of hair, 25-35 weight portions.
The rice zymotic fluid is adopted and prepared with the following method：
(A1) rice is taken, after soaking, is cooked, obtain shortening rice；
(A2) to aspergillus oryzae is inoculated with shortening rice described in step (A1), the inoculation quality of the aspergillus oryzae accounts for described ripe
The 1-3% of rice milling meal quality, afterwards temperature be 30-33 DEG C, humidity be 55-65% under conditions of carry out cultivation 48-32h, pass through
Centrifugation, filtering, obtain final product the rice zymotic fluid.
The pot marigold extract solution is adopted and prepared with the following method：
(B1) pot marigold is taken, through drying, is crushed, obtain pot marigold fine powder；
(B2) to ethanol is added for the first time in the pot marigold fine powder in step (B1), refluxing extraction 1- is carried out at 35-85 DEG C
2h, centrifugation, filtering, obtains the first filtrate and the first filter residue；Ethanol is added to second in first filter residue and at 35-85 DEG C
Refluxing extraction 1-2h is carried out, centrifugation, filtering obtain the second filtrate and the second filter residue；To being added for the third time in second filter residue
Ethanol simultaneously carries out refluxing extraction 1-2h at 35-85 DEG C, centrifugation, filtering, obtains the 3rd filtrate and the 3rd filter residue；By the described first filter
Liquid, the second filtrate, the 3rd filtrate merge, and concentration carries out micro porous filtration after removing ethanol, obtains final product the pot marigold extract solution.
In step (B1), the drying temperature is 45-55 DEG C, and the particle diameter of the pot marigold fine powder is 35-45 mesh.
In step (B2), the volumetric concentration of three addition ethanol is 65-35%；
The pot marigold fine powder is 1 with the mass volume ratio of addition ethanol for the first time:15-1:20g/ml, first filter
Slag is 1 with the mass volume ratio of second addition ethanol:15-1:20g/ml, second filter residue and third time addition ethanol
Mass volume ratio is 1:15-1:20g/ml；
The concentration is concentrated under reduced pressure, and the temperature of the concentration is 35-45 DEG C, carries out the filter sizes of the micro porous filtration
It is 0.4-0.5 μm.
The aloe leaf extract is prepared using following method：
(C1) Chinese aloe leaf is taken, slurry is broken into after peeling, obtain aloe slurries；
(C2) to ethanol is added in the aloe slurries in step (C1), after immersion 20-40min, it is centrifuged, filters, consolidate
Shape thing；To distilled water is added in the solid content for the first time, after immersion 20-40min, insulation is carried out at 90-100 DEG C and extracts 1-
2h, centrifugation, filtering, obtains the first filtrate and the first filter residue；Distilled water is added to second in first filter residue and in 90-
100 DEG C carry out insulation and extract 1-2h, and centrifugation, filtering obtain the second filtrate and the second filter residue；By first filtrate and the second filter
Liquid merges, and concentration carries out micro porous filtration after removing distilled water, obtains final product the aloe leaf extract.
In step (C2), the ethanol is 1.5 with the mass ratio of the aloe slurries:1-2.5:1, the volume of the ethanol
Concentration is 30-90%；
The solid content is 1 with the mass ratio of addition distilled water for the first time:8-1:12；First filter residue with add for the second time
Plus the mass ratio of distilled water is 1:8-1:12.
The concentration is concentrated for water-bath, and the temperature of the concentration is 85-95 DEG C, carries out the filter sizes of the micro porous filtration
It is 0.4-0.5 μm.
Described oil-control and the preparation method of the plant extracts for receiving fine, soft fur hole, concretely comprise the following steps：
After taking the rice zymotic fluid, pot marigold extract solution and aloe leaf extract respectively and being mixed, add hair auspicious
Palmitic acid fruit oil, is sufficiently mixed uniformly, obtains final product the plant extracts.
Application of the plant extracts in the skin care item for preparing oil-control and receiving fine, soft fur hole.
Beneficial effects of the present invention are：
Oil-control of the present invention simultaneously receives the plant extracts in fine, soft fur hole, is extracted by using rice zymotic fluid, pot marigold
Liquid, aloe leaf extract and Mao Rui palmitic acids fruit oil are for raw material and carry out being adapted to weight proportion, and the plant extracts for preparing has
Effect of preferable oil-control secretion, is up to 24.58%, together using the rate of change (i.e. inhibiting rate) of front and rear skin oil and fat content
When can also preferably receive fine, soft fur hole, improve the thick problem of pachylosis, pore, make skin finer and smoother, additionally, the plant carries
Take thing and come from natural plants, have no side effect, as skin care item oil-control and the functional additive in fine, soft fur hole can be received, with extensive
Application prospect.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing
The accompanying drawing to be used needed for having technology description is briefly described, it should be apparent that, drawings in the following description are only this
Some embodiments of invention, for those of ordinary skill in the art, on the premise of not paying creative work, can be with
Other accompanying drawings are obtained according to these accompanying drawings.
Fig. 1 is comparison diagrams of the different time measurement sample liquid A and sample liquid E to skin pore tightening effect.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below
Detailed description.Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are resulting on the premise of creative work is not made to be owned
Other embodiment, belongs to the scope that the present invention is protected.
1mg is represented with 1 weight portion in example below.
Embodiment 1
The present embodiment provides a kind of oil-control and receives the plant extracts in fine, soft fur hole, and raw material components include：
Rice zymotic fluid, 15 weight portions；
Pot marigold extract solution, 35 weight portions；
Aloe leaf extract, 15 weight portions；
The auspicious palmitic acid fruit of hair is oily (offer of Shanghai Lu Ya Bioisystech Co., Ltd), 35 weight portions.
Further, the oil-control and receive fine, soft fur hole plant extracts preparation method, comprise the following steps that：
(1) rice zymotic fluid is prepared
(A1) rice is taken, after adding 1 times of quality water to carry out immersion 12h, is cooked, obtain shortening rice；
(A2) to inoculation aspergillus oryzae (Japanese brewery industry Co., Ltd. provides), institute in shortening rice described in step (A1)
The inoculation quality for stating aspergillus oryzae accounts for the 1% of the shortening rice quality, afterwards temperature be 30 DEG C, humidity be 55% under conditions of
Cultivation 48h is carried out, through centrifugation, filtering, the rice zymotic fluid is obtained final product；
(2) pot marigold extract solution is prepared
(B1) pot marigold is taken, through 45 DEG C of dryings, is crushed, obtain the pot marigold fine powder that particle diameter is 35 mesh；
(B2) it is 65% ethanol to volumetric concentration is added in the pot marigold fine powder in step (B1) for the first time, and controls described
Pot marigold fine powder is 1 with the mass volume ratio of addition ethanol for the first time:15g/ml, carries out refluxing extraction 2h at 35 DEG C afterwards, from
The heart, filtering, obtain the first filtrate and the first filter residue；
It is 65% ethanol to add volumetric concentration to second in first filter residue, and controls first filter residue and second
The mass volume ratio of secondary addition ethanol is 1:15g/ml, carries out refluxing extraction 2h at 35 DEG C afterwards, and centrifugation, filtering obtain second
Filtrate and the second filter residue；
To adding volumetric concentration in second filter residue for the third time for 65% ethanol, and control second filter residue and the 3rd
The mass volume ratio of secondary addition ethanol is 1:15g/ml, carries out refluxing extraction 2h at 35 DEG C afterwards, and centrifugation, filtering obtain the 3rd
Filtrate and the 3rd filter residue；
First filtrate, the second filtrate, the 3rd filtrate are merged, 35 DEG C carry out removing ethanol concentrated under reduced pressure, adopt afterwards
Micro porous filtration is carried out with the filter membrane that aperture is 0.4 μm, the pot marigold extract solution is obtained final product；
(3) aloe leaf extract is prepared
(C1) Chinese aloe leaf is taken, ultraviolet-sterilization after peeling, and slurry is broken into, obtain aloe slurries；
(C2) it is 30% ethanol to volumetric concentration is added in the aloe slurries in step (C1), and controls the ethanol and institute
The mass ratio for stating aloe slurries is 1.5:1, after immersion 20min, centrifugation, filtering obtain solid content；
To distilled water is added in the solid content for the first time and control the solid content with addition distilled water mass ratio be
1:8, after immersion 20min, insulation is carried out at 90 DEG C and extracts 2h, centrifugation, filtering obtain the first filtrate and the first filter residue；
Distilled water is added to second in first filter residue and control first filter residue with second addition distilled water
Mass ratio be 1:8, insulation is carried out at 90 DEG C afterwards and extracts 2h, centrifugation, filtering obtain the second filtrate and the second filter residue；
First filtrate is merged with the second filtrate, concentration is carried out under 85 DEG C of water bath conditions and is removed distilled water, Zhi Houyong
Aperture carries out micro porous filtration for 0.4 μm of filter membrane, obtains final product the aloe leaf extract；
(4) after taking the rice zymotic fluid, pot marigold extract solution and aloe leaf extract respectively and being mixed, hair is added
Auspicious palmitic acid fruit oil, is sufficiently mixed uniformly, obtains final product the plant extracts.
Embodiment 2
The present embodiment provides a kind of oil-control and receives the plant extracts in fine, soft fur hole, and raw material components include：
Rice zymotic fluid, 25 weight portions；
Pot marigold extract solution, 25 weight portions；
Aloe leaf extract, 25 weight portions；
The auspicious palmitic acid fruit oil of hair, 25 weight portions.
Further, the oil-control and receive fine, soft fur hole plant extracts preparation method, comprise the following steps that：
(1) rice zymotic fluid is prepared
(A1) rice is taken, after adding 2 times of quality water to carry out immersion 15h, is cooked, obtain shortening rice；
(A2) to aspergillus oryzae is inoculated with shortening rice described in step (A1), the inoculation quality of the aspergillus oryzae accounts for described ripe
The 3% of rice milling meal quality, afterwards temperature be 33 DEG C, humidity be 95% under conditions of carry out cultivate 9 days, through centrifugation, filtering, i.e.,
Obtain the rice zymotic fluid；
(2) pot marigold extract solution is prepared
(B1) pot marigold is taken, through 55 DEG C of dryings, is crushed, obtain the pot marigold fine powder that particle diameter is 45 mesh；
(B2) it is 35% ethanol to volumetric concentration is added in the pot marigold fine powder in step (B1) for the first time, and controls described
Pot marigold fine powder is 1 with the mass volume ratio of addition ethanol for the first time:20g/ml, carries out refluxing extraction 1h at 85 DEG C afterwards, from
The heart, filtering, obtain the first filtrate and the first filter residue；
It is 35% ethanol to add volumetric concentration to second in first filter residue, and controls first filter residue and second
The mass volume ratio of secondary addition ethanol is 1:20g/ml, carries out refluxing extraction 1h at 85 DEG C afterwards, and centrifugation, filtering obtain second
Filtrate and the second filter residue；
To adding volumetric concentration in second filter residue for the third time for 35% ethanol, and control second filter residue and the 3rd
The mass volume ratio of secondary addition ethanol is 1:20g/ml, carries out refluxing extraction 1h at 85 DEG C afterwards, and centrifugation, filtering obtain the 3rd
Filtrate and the 3rd filter residue；
First filtrate, the second filtrate, the 3rd filtrate are merged, 45 DEG C carry out removing ethanol concentrated under reduced pressure, adopt afterwards
Micro porous filtration is carried out with the filter membrane that aperture is 0.5 μm, the pot marigold extract solution is obtained final product；
(3) aloe leaf extract is prepared
(C1) Chinese aloe leaf is taken, ultraviolet-sterilization after peeling, and slurry is broken into, obtain aloe slurries；
(C2) it is 90% ethanol to volumetric concentration is added in the aloe slurries in step (C1), and controls the ethanol and institute
The mass ratio for stating aloe slurries is 2.5:1, after immersion 40min, centrifugation, filtering obtain solid content；
To distilled water is added in the solid content for the first time and control the solid content with addition distilled water mass ratio be
1:12, after immersion 40min, insulation is carried out at 100 DEG C and extracts 1h, centrifugation, filtering obtain the first filtrate and the first filter residue；
Distilled water is added to second in first filter residue and control first filter residue with second addition distilled water
Mass ratio be 1:12, insulation is carried out at 100 DEG C afterwards and extracts 1h, centrifugation, filtering obtain the second filtrate and the second filter residue；
First filtrate is merged with the second filtrate, concentration is carried out under 95 DEG C of water bath conditions and is removed distilled water, Zhi Houyong
Aperture carries out micro porous filtration for 0.5 μm of filter membrane, obtains final product the aloe leaf extract；
(4) after taking the rice zymotic fluid, pot marigold extract solution and aloe leaf extract respectively and being mixed, hair is added
Auspicious palmitic acid fruit oil, is sufficiently mixed uniformly, obtains final product the plant extracts.
Embodiment 3
The present embodiment provides a kind of oil-control and receives the plant extracts in fine, soft fur hole, and raw material components include：
Rice zymotic fluid, 20 weight portions；
Pot marigold extract solution, 30 weight portions；
Aloe leaf extract, 20 weight portions；
The auspicious palmitic acid fruit oil of hair, 30 weight portions.
Further, the oil-control and receive fine, soft fur hole plant extracts preparation method, comprise the following steps that：
(1) rice zymotic fluid is prepared
(A1) rice is taken, after adding 1.5 times of quality water to carry out immersion 12h, is cooked, obtain shortening rice；
(A2) to aspergillus oryzae is inoculated with shortening rice described in step (A1), the inoculation quality of the aspergillus oryzae accounts for described ripe
The 2% of rice milling meal quality, afterwards temperature be 36 DEG C, humidity be 93% under conditions of carry out cultivate 3 days, through centrifugation, filtering, i.e.,
Obtain the rice zymotic fluid；
(2) pot marigold extract solution is prepared
(B1) pot marigold is taken, through 50 DEG C of dryings, is crushed, obtain the pot marigold fine powder that particle diameter is 40 mesh；
(B2) it is 30% ethanol to volumetric concentration is added in the pot marigold fine powder in step (B1) for the first time, and controls described
Pot marigold fine powder is 1 with the mass volume ratio of addition ethanol for the first time:18g/ml, carries out refluxing extraction 1.5h at 80 DEG C afterwards,
Centrifugation, filtering, obtain the first filtrate and the first filter residue；
It is 30% ethanol to add volumetric concentration to second in first filter residue, and controls first filter residue and second
The mass volume ratio of secondary addition ethanol is 1:18g/ml, carries out refluxing extraction 1.5h at 80 DEG C afterwards, centrifugation, filtering, obtains the
Two filtrates and the second filter residue；
To adding volumetric concentration in second filter residue for the third time for 30% ethanol, and control second filter residue and the 3rd
The mass volume ratio of secondary addition ethanol is 1:18g/ml, carries out refluxing extraction 1.5h at 80 DEG C afterwards, centrifugation, filtering, obtains the
Three filtrates and the 3rd filter residue；
First filtrate, the second filtrate, the 3rd filtrate are merged, 40 DEG C carry out removing ethanol concentrated under reduced pressure, adopt afterwards
Micro porous filtration is carried out with the filter membrane that aperture is 0.45 μm, the pot marigold extract solution is obtained final product；
(3) aloe leaf extract is prepared
(C1) Chinese aloe leaf is taken, ultraviolet-sterilization after peeling, and slurry is broken into, obtain aloe slurries；
(C2) it is 80% ethanol to volumetric concentration is added in the aloe slurries in step (C1), and controls the ethanol and institute
The mass ratio for stating aloe slurries is 2:1, after immersion 30min, centrifugation, filtering obtain solid content；
To distilled water is added in the solid content for the first time and control the solid content with addition distilled water mass ratio be
1:10, after immersion 30min, insulation is carried out at 95 DEG C and extracts 1.5h, centrifugation, filtering obtain the first filtrate and the first filter residue；
Distilled water is added to second in first filter residue and control first filter residue with second addition distilled water
Mass ratio be 1:10, insulation is carried out at 95 DEG C afterwards and extracts 1.5h, centrifugation, filtering obtain the second filtrate and the second filter residue；
First filtrate is merged with the second filtrate, concentration is carried out under 90 DEG C of water bath conditions and is removed distilled water, Zhi Houyong
Aperture carries out micro porous filtration for 0.45 μm of filter membrane, obtains final product the aloe leaf extract；
(4) after taking the rice zymotic fluid, pot marigold extract solution and aloe leaf extract respectively and being mixed, hair is added
Auspicious palmitic acid fruit oil, is sufficiently mixed uniformly, obtains final product the plant extracts.
Experimental example
1st, prepared by laboratory sample
Using basic components (glycerine stearic acid ester 2wt%, cetostearyl alcohol 3wt%, glycerine 5wt%, butanediol
10wt%, Nexbase 2004 6wt%, olive oil 4wt%, ceteth -20 are 1wt%, laruyl alcohol sodium sulfovinate
0.5wt%, Carbomer 0.2wt%, xanthans 0.3wt%, NaOH 0.1wt%, Phenoxyethanol 1.0wt%, deionized water
Surplus) as carrier, it is respectively that rice zymotic fluid, pot marigold extract solution, aloe leaf extract, the auspicious palmitic acid fruit of hair is oily (one-component)
And the plant extracts described in embodiment 3 and basic components compounded after (wherein one-component or the plant extracts
The mass fraction for accounting for basic components is 2wt%), sample liquid A, sample liquid B, sample liquid C, sample liquid D, sample liquid E is obtained, it
Carry out oil-control experiment, skin respectively afterwards and receive the measurement in fine, soft fur hole.
2nd, volunteer requires：
Effective people of volunteer 20；Age is between 25 years old~60 years old；Without serious systemic disease, without immune deficiency or itself exempt from
Epidemic disease disease patient；No active anaphylactia person；Previously to skin-care cosmetics without severe allergy history person；In nearly 1 month not
Once hormone medicine and immunodepressant person are used；Other clinical test persons are not participated in；Use according to regulations tested material and data is neat
Entirely；All volunteers should fill in Informed Consent Form before test.
First, oil-control experiment
It is effect of test each sample liquid (sample liquid A-E) in terms of oil-control.20 volunteers of selection carry out skin
The both effectiveness testing experiment of oil-control, using double-dummy design, contrast test is investigated.
Oil content test uses universally acknowledgedMethod, it is based on photometer principle.It is maximum
Advantage be test probe small volume, it is easy to use, any position of skin can be tested.Between a kind of this grease glandular secretion thing
Mensuration is connect, as a result can be used to distinguish different skin types, made to understand exactly and caused by inside and outside reason
Grease change is possibly realized.
Test environment conditions：
Test environment temperature is 26 ± 1 DEG C, and humidity is 50% ± 5%, and carries out real-time dynamic monitoring.
Test procedure：
Selection volunteer's face is test position, and every volunteer's test zone recorded respectively.Volunteer is every
Its morning and evening respectively uses test sample liquid (sample liquid A-E), and (volunteer is facial during test by personal habits use for applying amount
The cosmetics similar with test sample liquid must not be used), test period is 4 weeks.Used 1 week, 2 weeks using preceding, product in product
After 4 weeks, the skin oil and fat in facial test zone is tested.Each test zone of skin oil and fat content test 1 time.Survey
Amount result is evaluated with skin oil and fat changes of contents rate.Skin oil and fat changes of contents rate formula is as follows：
Grease rate of change %=(using fat content before sample liquid-use fat content after sample liquid)/use sample liquid
Preceding fat content * 100%
Measurement result is as shown in table 1.
Table 1- uses the measure of skin oil and fat changes of contents rate before and after each sample liquid
Although from table 1 it follows that the auspicious palmitic acid fruit oil of rice zymotic fluid, pot marigold extract solution, aloe leaf extract, hair
(sample liquid A-D) has certain inhibition to fat secretion, but by above-mentioned each component carry out it is compound after this hair for being formed
Influence of the bright plant extracts (sample liquid E) to fat secretion is maximum, and effective oil-control secretion, skin oil and fat contains quantitative change
Rate is up to 24.58%.
2nd, skin receives fine, soft fur hole measurement
It is test sample liquid A (basic components+account for the sample liquid that basic components 2wt% rice ferment filtrates are made into) and sample
Liquid E (basic components+account for the sample liquid that the gained plant extracts of basic components 2wt% embodiments 3 is made into) is in terms of pore is improved
Effect.20 volunteers of selection carry out pore aperture and observe both effectiveness testing experiment, and using double-dummy design, contrast test is entered
Row is investigated.
Using DIGIMIC800 type skin image analyzers to front and rear same position (wing of nose or the wing of nose and homonymy canthus outside
The midpoint of line) pore shooting (amplify 20 times), 3 width pictures of intake every time, then the big of pore aperture is drawn with graphical analysis
It is small, finally take its average value.The product is assessed to skin using the change of front and rear skin pore Numerical Aperture by comparative product
Effect that skin pore compacts.
Selection volunteer's face is test position, and every volunteer's test zone recorded respectively.Volunteer is every
Its morning and evening is each using test sample liquid A, a sample liquid E, and (volunteer is facial not during test by personal habits use for applying amount
The cosmetics similar with test sample liquid must be used), test period is 4 weeks.Used 1 week, 2 weeks and 4 using preceding, product in product
Zhou Hou, to the pore shooting in facial test zone.3 width pictures are absorbed every time, then draw the big of pore aperture with graphical analysis
It is small, finally take its average value.
Skin pore varying aperture was reflected in test period, and Experimental Area pore aperture changes over time rule.Its value
Smaller, pore seems smaller, and skin is finer and smoother, conversely, pachylosis, pore is thick.
Measurement result is as shown in Figure 1.As seen from Figure 1, although can make subject using sample liquid A and sample liquid E
Skin of face pore aperture reduce, and with the extension of product use time, pore aperture persistently tapers into.Wherein use
The subject of sample liquid E becomes apparent (P ＜ 0.05) compared with the subjects skin's pore varying aperture using sample liquid A, illustrates sample
The effect for receiving fine, soft fur hole of product liquid E is stronger, i.e., " sample liquid containing the gained plant extracts of embodiment 3 " is to changing within experimental period
Kind pore aperture is to receive fine, soft fur hole to have good effect, and will be apparently higher than the receipts of " only containing the sample liquid of rice ferment filtrate "
Fine, soft fur hole effect.
The above, specific embodiment only of the invention, but protection scope of the present invention is not limited thereto, and it is any
Those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, should all contain
Cover within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of oil-control and the plant extracts in fine, soft fur hole is received, it is characterised in that raw material components include：
Rice zymotic fluid, 15-25 weight portions；
Pot marigold extract solution, 25-35 weight portions；
Aloe leaf extract, 15-25 weight portions；
The auspicious palmitic acid fruit oil of hair, 25-35 weight portions.
2. oil-control according to claim 1 and the plant extracts in fine, soft fur hole is received, it is characterised in that the rice zymotic fluid
Adopt and prepare with the following method：
(A1) rice is taken, after soaking, is cooked, obtain shortening rice；
(A2) to aspergillus oryzae is inoculated with shortening rice described in step (A1), the inoculation quality of the aspergillus oryzae accounts for the shortening rice
The 1-3% of meal quality, afterwards temperature be 30-33 DEG C, humidity be 55-65% under conditions of carry out cultivation 48-32h, through centrifugation,
Filtering, obtains final product the rice zymotic fluid.
3. oil-control according to claim 1 and the plant extracts in fine, soft fur hole is received, it is characterised in that the pot marigold is extracted
Liquid is adopted and prepared with the following method：
(B1) pot marigold is taken, through drying, is crushed, obtain pot marigold fine powder；
(B2) to ethanol is added for the first time in the pot marigold fine powder in step (B1), refluxing extraction 1-2h is carried out at 35-85 DEG C, from
The heart, filtering, obtain the first filtrate and the first filter residue；Ethanol is added to second in first filter residue and carried out at 35-85 DEG C
Refluxing extraction 1-2h, centrifugation, filtering, obtains the second filtrate and the second filter residue；To adding ethanol for the third time in second filter residue
And refluxing extraction 1-2h is carried out at 35-85 DEG C, centrifugation, filtering obtain the 3rd filtrate and the 3rd filter residue；By first filtrate,
Second filtrate, the 3rd filtrate merge, and concentration carries out micro porous filtration after removing ethanol, obtains final product the pot marigold extract solution.
4. oil-control according to claim 3 and the plant extracts in fine, soft fur hole is received, it is characterised in that in step (B1), institute
It is 45-55 DEG C to state drying temperature, and the particle diameter of the pot marigold fine powder is 35-45 mesh.
5. oil-control according to claim 3 and the plant extracts in fine, soft fur hole is received, it is characterised in that in step (B2), three
The volumetric concentration of secondary addition ethanol is 65-35%；
The pot marigold fine powder is 1 with the mass volume ratio of addition ethanol for the first time:15-1:20g/ml, first filter residue with
The mass volume ratio of second addition ethanol is 1:15-1:20g/ml, second filter residue adds the quality of ethanol with third time
Volume ratio is 1:15-1:20g/ml；
The concentration is concentrated under reduced pressure, and the temperature of the concentration is 35-45 DEG C, and the filter sizes for carrying out the micro porous filtration are
0.4-0.5μm。
6. oil-control according to claim 1 and the plant extracts in fine, soft fur hole is received, it is characterised in that the Chinese aloe leaf is extracted
Liquid is adopted and prepared with the following method：
(C1) Chinese aloe leaf is taken, slurry is broken into after peeling, obtain aloe slurries；
(C2) to ethanol is added in the aloe slurries in step (C1), after immersion 20-40min, centrifugation, filtering obtain solid content；
To distilled water is added in the solid content for the first time, after immersion 20-40min, insulation is carried out at 90-100 DEG C and extracts 1-2h, from
The heart, filtering, obtain the first filtrate and the first filter residue；Distilled water is added to second in first filter residue and enter at 90-100 DEG C
1-2h is extracted in row insulation, and centrifugation, filtering obtain the second filtrate and the second filter residue；First filtrate is merged with the second filtrate,
Concentration carries out micro porous filtration after removing distilled water, obtains final product the aloe leaf extract.
7. oil-control according to claim 6 and the plant extracts in fine, soft fur hole is received, it is characterised in that in step (C2), institute
It is 1.5 that ethanol is stated with the mass ratio of the aloe slurries:1-2.5:1, the volumetric concentration of the ethanol is 30-90%；
The solid content is 1 with the mass ratio of addition distilled water for the first time:8-1:12；First filter residue steams with second addition
The mass ratio of distilled water is 1:8-1:12.
8. oil-control according to claim 6 and the plant extracts in fine, soft fur hole is received, it is characterised in that the concentration is water-bath
Concentration, the temperature of the concentration is 85-95 DEG C, and the filter sizes for carrying out the micro porous filtration are 0.4-0.5 μm.
9. oil-control described in a kind of any one of claim 1-8 and the preparation method of the plant extracts for receiving fine, soft fur hole, its feature
It is to concretely comprise the following steps：
After taking the rice zymotic fluid, pot marigold extract solution and aloe leaf extract respectively and being mixed, the auspicious palmitic acid of hair is added really
Oil, is sufficiently mixed uniformly, obtains final product the plant extracts.
10. application of the plant extracts described in any one of claim 1-8 in the skin care item for preparing oil-control and receiving fine, soft fur hole.
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| CN103230353A (en) * | 2013-05-03 | 2013-08-07 | 湖南御泥坊化妆品有限公司 | Additive-free natural whitening cosmetic and preparation method thereof |
| CN103417428A (en) * | 2013-07-17 | 2013-12-04 | 吴克 | Silky-smooth emulsion |
| CN105267122A (en) * | 2015-11-04 | 2016-01-27 | 皖南医学院 | Natural moisturizing and pore shrinking gel and preparation method thereof |
| CN106137916A (en) * | 2016-08-11 | 2016-11-23 | 胡安平 | The cosmetic composition of a kind of removing acnes and controlling oil whitening and application thereof |
| CN106176556A (en) * | 2016-08-31 | 2016-12-07 | 张进 | A kind of removing acnes and controlling oil whitening cream |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103230353A (en) * | 2013-05-03 | 2013-08-07 | 湖南御泥坊化妆品有限公司 | Additive-free natural whitening cosmetic and preparation method thereof |
| CN103417428A (en) * | 2013-07-17 | 2013-12-04 | 吴克 | Silky-smooth emulsion |
| CN105267122A (en) * | 2015-11-04 | 2016-01-27 | 皖南医学院 | Natural moisturizing and pore shrinking gel and preparation method thereof |
| CN106137916A (en) * | 2016-08-11 | 2016-11-23 | 胡安平 | The cosmetic composition of a kind of removing acnes and controlling oil whitening and application thereof |
| CN106176556A (en) * | 2016-08-31 | 2016-12-07 | 张进 | A kind of removing acnes and controlling oil whitening cream |
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Effective date of registration: 20200601 Address after: 210000 floor 14-15, building B, Beiwei International Center, No. 1, Chuangzhi Road, Jianye District, Nanjing City, Jiangsu Province Patentee after: Jiangsu Sumi International Fashion Management Co.,Ltd. Address before: 100071, room 720, room 72, No. 18, Feng Bei Road, Beijing, Fengtai District Patentee before: BEIJING HUAAO GUANGCHENG COSMETICS Co.,Ltd. |