CN105747266A - Method for preparing tobacco cigarettes conducting non-combustion heating - Google Patents

Method for preparing tobacco cigarettes conducting non-combustion heating Download PDF

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Publication number
CN105747266A
CN105747266A CN201610247576.7A CN201610247576A CN105747266A CN 105747266 A CN105747266 A CN 105747266A CN 201610247576 A CN201610247576 A CN 201610247576A CN 105747266 A CN105747266 A CN 105747266A
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China
Prior art keywords
tobacco
heating
cigarette
nicotiana tabacum
preparation
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CN201610247576.7A
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CN105747266B (en
Inventor
刘剑
阮艺斌
胡世龙
王维维
黄新民
谢顺萍
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China Tobacco Guizhou Industrial Co Ltd
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China Tobacco Guizhou Industrial Co Ltd
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Priority to CN201610247576.7A priority Critical patent/CN105747266B/en
Publication of CN105747266A publication Critical patent/CN105747266A/en
Priority to PCT/CN2016/108255 priority patent/WO2017181684A1/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The invention discloses a method for preparing tobacco cigarettes conducting non-combustion heating.The method comprises the following steps that tobacco raw materials are selected and immersed in water and filtered, and then the filtered tobacco is pulped to obtain tobacco size; tobacco bases are prepared; one or more of flue-cured tobacco, air-cured tobacco or sun-cured tobacco is selected, and tobacco essential oil is prepared through a molecular distillation method; by weight, 1-40 parts of tobacco essential oil, 2-20 parts of tobacco flavor and 4-80 parts of atomizing agent are weighed and then evenly mixed, and coating liquid is obtained; the coating liquid with the weight being 25-40% of the tobacco bases is weighed, and the coating liquid is sprayed to the tobacco bases; the tobacco bases are prepared into the tobacco cigarettes conducting non-combustion heating.The cigarettes are full in smoke and have the smoking feeling similar to that of traditional cigarettes; fragrance is rich, and especially the tobacco fragrance is obvious; good satisfied feeling is achieved.

Description

A kind of preparation method heating not burning tobacco Cigarette
Technical field
The present invention relates to technical field of tobacco, be more particularly to one and heat not burning tobacco Medicated cigarette The preparation method of cigarette.
Background technology
The heating Medicated cigarette that do not burns is not provide the consumer with Ni Gu by the way of burning tobacco by heating Fourth and Nicotiana tabacum L. characteristic perfume, meet consumer demand, main flume can be greatly lowered simultaneously The coal-tar middle oil burst size with harmful substance, is the important trend of following tobacco market development.
Owing to its occupation mode and traditional cigarette exist huge difference, heat the Cigarette that do not burns Design be necessarily different from traditional cigarette.Related experiment shows the common cigarette without special handling Prop up to use in general smoking set and satisfied amount of smoke and fragrance cannot be provided.
Reconstituted tobacco is important tobacco material, has heating not use in burning tobacco goods Three below benefit: (1) can make flaky material, can come off by upper solution Nicotiana tabacum L. largely Phenomenon;(2) ensure the homogeneity of tobacco product quality greatly, it is provided that on sense organ more Consistent sucks impression;(3) due to can be the biggest in the preparation process of reconstituted tobacco The chemical constituent of Nicotiana tabacum L. is changed, to the matter improving heating non-combustion-cigarette straw-made articles in degree Amount, meets individual needs on market and has clear superiority.But the reconstituted tobacco produced at present is main Purpose is to improve tobacco material service efficiency, increases economic efficiency, and the raw material used is typically Discarded offal, Nicotiana tabacum L. and cabo, lack Medicated cigarette feature at the bottom of the most most tobacco-based Fragrance, this perfume of Nicotiana tabacum L. is not enough, and miscellaneous QI and xylon gas are heavier.Meanwhile, reconstituted tobacco is mainly cut Adding in Medicated cigarette after Si and use, the humectant content typically used is relatively low, in heating non-burning The use of tobacco product cannot provide the smog of high concentration.
Application publication number is that the patent document of CN 103181613 provides a kind of electric dry distillation type Nicotiana tabacum L. Preparation of sections method.In this patent document in reconstituted tobacoo chip base be coated with tobacco extract, Plant extract and smoke agent, be applied in electricity destructive distillation device to produce smog.But this patent File the most simply modifying common thin slice in the way of thin slice coating, does not considers that thin slice is right after rolling Cigarette be fuming impact and on tobacco aroma release impact.
(1) to solve the technical problem that
The technical problem to be solved in the present invention be how improve heating do not burn the Medicated cigarette amount of being fuming and Tobacco aroma, uses the smog impression that can provide good in smoking set is not burnt in heating and enriches Tobacco aroma, and provide a kind of preparation method heating not burning tobacco Cigarette.
(2) technical scheme
In order to solve above-mentioned technical problem, the invention provides one and heat not burning tobacco Medicated cigarette The preparation method of cigarette, the method comprises the steps (raw materials used equal city available from):
Step one: at the bottom of preparation tobacco-based: choose tobacco material, be immersed in water, water temperature For 60-80 DEG C, soak time is 0.5-2h, filters, and then Nicotiana tabacum L. making beating after filter is obtained Nicotiana tabacum L. Serosity;Weigh Nicotiana tabacum L. serosity 50-80 part in parts by weight, wood pulp 8-25 part, binding agent 4-8 part, The most uniformly mix, mixed slurry is delivered to paper machine molding, be dried to moisture content and be 10-15%, obtains at the bottom of tobacco-based;
Step 2: prepare essential oil of tobaccos: choose one or more in flue-cured tobacco, air-curing of tobacco leaves or suncured tabacco, Solvent extraction method is first used to prepare Nicotiana tabacum L. primary extract;Use molecularly distilled by Nicotiana tabacum L. primary extract again Prepare essential oil of tobaccos;
Step 3: prepare coating fluid: weigh the essential oil of tobaccos 1-40 that step 2 obtains in parts by weight Part, flavouring essence for tobacco 2-20 part, propellant 40-80 part, the most uniformly mix, obtain coating fluid;
Step 4: at the bottom of coating tobacco-based: according to the 25-40% of the Nicotiana tabacum L. substrate by weight that step one obtains Weigh the coating fluid that step 3 obtains, coating fluid is sprayed at the bottom of tobacco-based, at constant temperature and humidity Under the conditions of stand 40-60h, obtain coating tobacco-based at the bottom of;
Step 5: prepare tobacco smoke cigarette: by size system at the bottom of tobacco-based step 4 obtained Become tobacco rod, tobacco rod is connected with filter tip and obtains heating not burning tobacco Cigarette.
Preferably, in step one, described tobacco material include cabo, offal, broken leaf and One or more in short silk.
Preferably, in step one, described wood pulp is PiceameyeriRehd. Et Wils. bleached kraft pulp, poplar drift One or several in white sulfate pulp, needlebush bleached kraft pulp and Eucalyptus bleached kraft pulp Kind.
Preferably, in step one, described binding agent is xanthan gum, arabic gum and Guar One or more in glue.
Preferably, in step one, described Nicotiana tabacum L. substrate thickness is 10-300 μm;Tobacco-based Base thickness degree grammes per square metre is at 20-200g/m2
Preferably, in step 2, described air-curing of tobacco leaves is the one in burley tobaccos or Maryland Or two kinds;Described suncured tabacco is the one in Turkish tobaccos, Dark sun-cured, Sun cured tobacco or Nicotiniana rustica or several Kind;Described molecular distillation condition is as follows: charging rate 2-10mL/min, vacuum 15-20Pa, Injector temperature 80 DEG C, heating-up temperature 60-80 DEG C, chilling temperature 10-20 DEG C, rotating speed 300-400 r/min。
Preferably, in step 3, described described flavouring essence for tobacco be vanillin, benzoic acid, Phenylacetic acid, 10% Peru's extractum, 5% tree moss concrete, 90% Oleum Caryophylli, anisic aldehyde, 10% Pineapple ketone, benzyl alcohol, phenethanol, toluene ethyl ketone, ethyl phenylacetate, small bell Fructus Armeniacae Mume extractum, Hyacinthin, 1-Phenylethanone., angelica lactone, method Buddhist nun's ketone, lauric acid/dodecanoic acid, isovaleric acid, benzyl butyrate, Capryl alcohol, tetramethylpyazine, citric acid, ethylmaltol, sclareol, (+)-Norambreinolide, Ambergris ether, davana oil, petitgrain oil, oil of Rhizoma et radix valerianae, vetiver oil, labdanum concrete, Styrax soak Cream, angelica grosseserrata root tincture, tart fruit fluid extract, Fructus Tamarindi Indicae extractum, Chamomile extractum, vanilla extractum, nothing Flowers and fruits extractum, Sucus Mali pumilae, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone, palm fibre Palmitic acid acid, geranyl acetone one or more;Preferably, by weight percentage vanillin 1%, Benzoic acid 0.2%, phenylacetic acid 0.5%, Peru's extractum 1.0%, tree moss concrete 5%, Oleum Caryophylli 0.5%, Anisic aldehyde 0.5%, Fructus Ananadis comosi aldehyde 0.5%, phenethanol 0.4%, toluene ethyl ketone 0.2%, phenylacetic acid second Ester 0.2%, ethanol 25% and the combination of propylene glycol 65%.
Preferably, in step 3, described propellant be propylene glycol, 2,2'-ethylenedioxybis(ethanol)., 1,3-fourth two Alcohol, glycerol, dipropylene glycol, Polyethylene Glycol one or more;Preferably glycerine.
Present invention also offers above-mentioned heating not burning tobacco Cigarette preparation method prepare Nicotiana tabacum L. cigarette.
The preparation method that present invention also offers above-mentioned heating not burning tobacco Cigarette prepares Nicotiana tabacum L. cigarette do not burn the application in smoking set in heating, Nicotiana tabacum L. cigarette that will be above-mentioned is positioned over In smoking set, setting heating-up temperature as 200-500 DEG C, heat time heating time, 10-30s, arrived heat time heating time After start suction.
The tobacco material section of cigarette of the present invention is to use paper filter stick to produce apparatus processing to process.Excellent Selection of land, the quantification of 20-120g/m of gained substrate2, preferably 50g/m2;Width is 60-300mm, Preferably 110mm.Preferably, the production equipment of paper filter stick is prepared with 10-80m/min speed. Preferably, substrate needs through embossed, and concrete shape does not limits, and more excellent embosses for bar shaped; Forming paper used can be common forming paper, preferably has the material of impermeable function.
The present invention also provides at the bottom of tobacco-based and filter stick combination process.In order to ensure the cigarette after rolling Can fully discharge flue gas and fragrance in a heated condition, mistake compound with filter stick at the bottom of by tobacco-based Journey to be followed and farthest reduces draw resistance.The filter stick used in the present invention is the filter of vinegar fibre Rod, preferably hollow shaped filter stick, can reduce the filter stick obstruct to flue gas to the full extent Effect.Concrete, the filter stick specification used is circumference 22.0-25.0mm, and filter lengths is 100-150mm, strand specification is filament denier 1.8~6.0 danier.Nozzle portion filter stick can For whole hollow-core constructions, it is also possible to the common filter stick of bound fraction, the most complete hollow filter stick, The a length of 23+7mm of more excellent filter stick, wherein 23mm is hollow filter stick, and 7mm is common filter stick. Hollow plug shape does not limits, and can use circle, square, or other polymorphic structures.Above-mentioned substrate The cigarette tobacco material section produced through paper filter stick process equipment is combined with filter stick.Design filter stick is long Degree is 15-40mm, preferably 15-30mm;The a length of 10-40mm of tobacco material, preferably For 20mm.The finished cigarettes for heating non-burning smoking set it is after Fu He.
The present invention finally provides compound rear cigarette using effect in smoking set.Cigarette by preparation It is positioned in smoking set, sets heating-up temperature as 200-500 DEG C, preferably 250-300 DEG C, add Hot 10-30s, preferably 20s;Starting suction after arriving the setting time, flue gas is full, possesses The suction impression similar with traditional cigarette;Fragrance enriches simultaneously, and particularly tobacco aroma shows; There is good gratification.
(3) beneficial effect
The inventive method can prepare the cigarette that quality is homogeneous, for ensureing by mouth aspiration procedure The concordance of middle flue gas quality provides basis;The inventive method uses the processing of original paper process technology At the bottom of tobacco-based, it is ensured that the probability of the industrialized production of cigarette;The inventive method uses hollow filter Rod ensure that the rich of new cigarette amount of smoke and tobacco aroma to the full extent.Employing Tobacco blending has, and on the premise of ensureing that puff number is consistent with traditional cigarette, reduces tobacco material Usage amount, reduces production cost;Cigarette flue gas of the present invention is full, possesses similar with traditional cigarette Suction impression;Fragrance enriches simultaneously, and particularly tobacco aroma shows;There is good meeting Sense.
Detailed description of the invention
Below in conjunction with embodiment, embodiments of the present invention are described in further detail.Following reality Execute example for the present invention is described, but can not be used for limiting the scope of the present invention.
Embodiment 1
Cabo and offal are mixed, adds the water of 3-4 times of weight, heating, filter to obtain filtering residue;Filtering residue is beaten Slurry obtains Nicotiana tabacum L. serosity, takes Nicotiana tabacum L. serosity 65Kg, wood pulp 20Kg, xanthan gum 4Kg uniformly mix Close, manufacture paper with pulp the most on a papermaking machine and obtain substrate;Preparing coating fluid, it forms percentage by weight For: flue-cured tobacco essential oil of tobaccos: 15%;Flavouring essence for tobacco: 10%;Glycerol: 75%, and by tobacco-based The coating fluid laryngeal spray of end weight 30% is uniformly sprayed at the bottom of tobacco-based;Permanent at constant temperature Balance under the conditions of in wet tank, adjusting ambient temperature is (22 ± 1) DEG C, relative humidity (60 ± 2) % 48h, obtains 1# sample;
Choose quantification of 50g/m2;Width is the substrate of 80mm, and processed equipment processes and obtains The tobacco rod of embossing, produces device rate and controls at 40m/min in production process;By compound Tobacco rod and filter tip are connected by equipment makes cigarette, and wherein filter length is 30mm, tobacco rod A length of 20mm.
Cigarette obtained above is inserted in smoking set, and sets smoking set heating-up temperature as 250 DEG C, Suction is started after heating 20s.
Embodiment 2
Cabo and offal are mixed, adds the water of 3-4 times of weight, heating, filter to obtain filtering residue;Will Filtering residue making beating obtains Nicotiana tabacum L. serosity, takes Nicotiana tabacum L. serosity 80Kg, wood pulp 25Kg, xanthan gum 8Kg Uniformly mixing, manufactures paper with pulp the most on a papermaking machine and obtains substrate;Preparing coating fluid, it forms weight Percentage ratio is: flue-cured tobacco essential oil of tobaccos: 15%;Flavouring essence for tobacco: 10%;Glycerol: 75%, and The coating fluid laryngeal spray of Nicotiana tabacum L. substrate by weight 15% is uniformly sprayed at the bottom of selected tobacco-based On.In climatic chamber, adjusting ambient temperature is (22 ± 1) DEG C, relative humidity (60 ± 2) % Under the conditions of balance 48h, obtain 2# sample;
Choose quantification of 35g/m2;Width is the substrate of 110mm, and processed equipment processes and obtains The tobacco rod of embossing, produces device rate and controls at 60m/min in production process;By compound Tobacco rod and filter tip are connected by equipment makes cigarette, and wherein filter length is 30mm, tobacco rod A length of 20mm.
Cigarette obtained above is inserted in smoking set, and sets smoking set heating-up temperature as 300 DEG C, Suction is started after heating 10s.
Embodiment 3
Cabo and offal are mixed, adds the water of 3-4 times of weight, heating, filter to obtain filtering residue;Will Filtering residue making beating obtains Nicotiana tabacum L. serosity, takes Nicotiana tabacum L. serosity 50Kg, wood pulp 8Kg, arabic gum 6Kg Uniformly mixing, manufactures paper with pulp the most on a papermaking machine and obtains substrate;Preparing coating fluid, it forms weight Percentage ratio is: flue-cured tobacco essential oil of tobaccos: 40%;Flavouring essence for tobacco: 10%;Glycerol: 50%, and The coating fluid laryngeal spray of Nicotiana tabacum L. substrate by weight 45% is uniformly sprayed at the bottom of tobacco-based. In climatic chamber, adjusting ambient temperature is (22 ± 1) DEG C, relative humidity (60 ± 2) % Under the conditions of balance 48h, obtain 3# sample;
Choose quantification of 70g/m2;Width is the substrate of 220mm, and processed equipment processes and obtains The tobacco rod of embossing, produces device rate and controls at 20m/min in production process;By compound Tobacco rod and filter tip are connected by equipment makes cigarette, and wherein filter length is 30mm, tobacco rod A length of 20mm.
Cigarette obtained above is inserted in smoking set, and sets smoking set heating-up temperature as 200 DEG C, Suction is started after heating 15s.
Result shows: the not burning tobacco goods of the heating in above-described embodiment are in low-temperature heat condition Lower produced flue gas is less to throat irritation, and fragrance enriches, and Nicotiana tabacum L. highlights, unique wind Lattice, gratification is good, and pleasant impression is purer comfortable, and the amount of being fuming is sufficient.
Embodiment of above is merely to illustrate the present invention, rather than limitation of the present invention.Although ginseng Being described in detail the present invention according to embodiment, those of ordinary skill in the art should manage Solve, technical scheme is carried out various combination, amendment or equivalent, does not takes off From the spirit and scope of technical solution of the present invention, all should contain in scope of the presently claimed invention In the middle of.

Claims (10)

1. the preparation method heating not burning tobacco Cigarette, it is characterised in that the party Method comprises the steps:
Step one: at the bottom of preparation tobacco-based: choose tobacco material, be immersed in water, water temperature For 60-80 DEG C, soak time is 0.5-2h, filters, and then Nicotiana tabacum L. making beating after filter is obtained Nicotiana tabacum L. Serosity;Weigh Nicotiana tabacum L. serosity 50-80 part, wood pulp 8-25 part, binding agent 4-8 in parts by weight Part, the most uniformly mix, mixed slurry is delivered to paper machine molding, is dried to moisture content For 10-15%, obtain at the bottom of tobacco-based;
Step 2: prepare essential oil of tobaccos: choose one or more in flue-cured tobacco, air-curing of tobacco leaves or suncured tabacco, Solvent extraction method is first used to prepare Nicotiana tabacum L. primary extract;Use molecularly distilled by Nicotiana tabacum L. primary extract again Prepare essential oil of tobaccos;
Step 3: prepare coating fluid: weigh the essential oil of tobaccos 1-40 that step 2 obtains in parts by weight Part, flavouring essence for tobacco 2-20 part, propellant 40-80 part, the most uniformly mix, obtain coating fluid;
Step 4: at the bottom of coating tobacco-based: according to the 25-40% of the Nicotiana tabacum L. substrate by weight that step one obtains Weigh the coating fluid that step 3 obtains, coating fluid is sprayed at the bottom of tobacco-based, at constant temperature and humidity Under the conditions of stand 40-60h, obtain coating tobacco-based at the bottom of;
Step 5: prepare tobacco smoke cigarette: by size system at the bottom of tobacco-based step 4 obtained Become tobacco rod, tobacco rod is connected with filter tip and obtains heating not burning tobacco Cigarette.
The preparation method of heating the most according to claim 1 not burning tobacco Cigarette, It is characterized in that, in step one, described tobacco material include cabo, offal, broken leaf and One or more in short silk.
The preparation method of heating the most according to claim 1 not burning tobacco Cigarette, It is characterized in that, in step one, described wood pulp is PiceameyeriRehd. Et Wils. bleached kraft pulp, poplar drift One or several in white sulfate pulp, needlebush bleached kraft pulp and Eucalyptus bleached kraft pulp Kind.
The preparation method of heating the most according to claim 1 not burning tobacco Cigarette, It is characterized in that, in step one, described binding agent is xanthan gum, arabic gum and Guar One or more in glue.
The preparation method of heating the most according to claim 1 not burning tobacco Cigarette, It is characterized in that, in step one, described Nicotiana tabacum L. substrate thickness is 10-300 μm;Tobacco-based Base thickness degree grammes per square metre is at 20-200g/m2
The preparation method of heating the most according to claim 1 not burning tobacco Cigarette, It is characterized in that, in step 2, described air-curing of tobacco leaves is the one in burley tobaccos or Maryland Or two kinds;Described suncured tabacco is the one in Turkish tobaccos, Dark sun-cured, Sun cured tobacco or Nicotiniana rustica or several Kind;Described molecular distillation condition is as follows: charging rate 2-10mL/min, vacuum 15-20Pa, Injector temperature 80 DEG C, heating-up temperature 60-80 DEG C, chilling temperature 10-20 DEG C, rotating speed 300-400 r/min。
The preparation method of heating the most according to claim 1 not burning tobacco Cigarette, It is characterized in that, in step 3, described flavouring essence for tobacco is vanillin, benzoic acid, benzene second Acid, 10% Peru's extractum, 5% tree moss concrete, 90% Oleum Caryophylli, anisic aldehyde, 10% pineapple ketone, Benzyl alcohol, phenethanol, toluene ethyl ketone, ethyl phenylacetate, small bell Fructus Armeniacae Mume extractum, hyacinthin, 1-Phenylethanone., angelica lactone, method Buddhist nun's ketone, lauric acid/dodecanoic acid, isovaleric acid, benzyl butyrate, capryl alcohol, four Methylpyrazine, citric acid, ethylmaltol, sclareol, (+)-Norambreinolide, ambergris ether, Davana oil, petitgrain oil, oil of Rhizoma et radix valerianae, vetiver oil, labdanum concrete, Styrax extractum, Radix Angelicae Pubescentis Tincture, tart fruit fluid extract, Fructus Tamarindi Indicae extractum, Chamomile extractum, vanilla extractum, Fructus Fici extractum, Sucus Mali pumilae, Megastigmatrienone, dihydroactinidiolide, alpha, beta-lonone, Palmic acid, Herba Pelargonii Graveolentis One or more of benzylacetone.
8. according to the system of the not burning tobacco Cigarette of the heating described in any one of claim 1-7 Preparation Method, it is characterised in that in step 3, described propellant be propylene glycol, 2,2'-ethylenedioxybis(ethanol)., 1,3 butylene glycol, glycerol, dipropylene glycol, Polyethylene Glycol one or more.
9. the preparation side of the not burning tobacco Cigarette of the heating described in any one of claim 1-8 The Nicotiana tabacum L. cigarette that method prepares.
10. the preparation method of the not burning tobacco Cigarette of the heating described in claim 9 prepares Nicotiana tabacum L. cigarette do not burn the application in smoking set in heating, it is characterised in that by claim 1-8 Nicotiana tabacum L. cigarette described in any one is positioned in smoking set, sets heating-up temperature as 200-500 DEG C, adds Heat time 10-30s, starts suction after arriving heat time heating time.
CN201610247576.7A 2016-04-20 2016-04-20 Preparation method of cigarette rod without burning tobacco by heating Active CN105747266B (en)

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PCT/CN2016/108255 WO2017181684A1 (en) 2016-04-20 2016-12-01 Method for manufacturing heat-not-burn tobacco cigarette

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WO2017181684A1 (en) * 2016-04-20 2017-10-26 贵州中烟工业有限责任公司 Method for manufacturing heat-not-burn tobacco cigarette
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CN108998241A (en) * 2018-07-26 2018-12-14 湖北中烟工业有限责任公司 For heating curing scent of fire cured tobacco essence in the cigarette that do not burn and its preparation method and application
CN108991588A (en) * 2018-10-09 2018-12-14 湖北中烟工业有限责任公司 For improving the essence and its preparation method and application for heating not burning tobacco mouthfeel
CN109043639A (en) * 2018-07-05 2018-12-21 福建金闽再造烟叶发展有限公司 It is a kind of for heating the preparation method of the reconstituted tobacco for the tobacco product that do not burn
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Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101039597A (en) * 2004-08-18 2007-09-19 布朗及威廉森控股公司 Reconstituted tobacco sheet and smoking article therefrom
US20080078417A1 (en) * 2002-11-19 2008-04-03 Wanna Joseph T Process for making a bandcast tobacco sheet and smoking article therefrom
CN103750535A (en) * 2014-01-22 2014-04-30 红云红河烟草(集团)有限责任公司 Preparation method of heating non-combustion type cigarette block
CN204362975U (en) * 2015-01-20 2015-06-03 川渝中烟工业有限责任公司 The aspirator of a kind of electrical heating not burning tobacco
CN204362974U (en) * 2015-01-20 2015-06-03 川渝中烟工业有限责任公司 A kind of charcoal heats the aspirator of not burning tobacco
CN104770874A (en) * 2015-03-21 2015-07-15 南通烟滤嘴有限责任公司 Hollow filter stick and production method thereof
CN104856215A (en) * 2015-06-25 2015-08-26 云南中烟工业有限责任公司 Reconstituted tobacco suitable for heating non-combustion type cigarettes
CN105105317A (en) * 2015-08-14 2015-12-02 贵州中烟工业有限责任公司 Strong-flavor type tobacco product being nonflammable while heating and preparation method thereof
CN105146734A (en) * 2015-08-14 2015-12-16 贵州中烟工业有限责任公司 Maotai-flavor tobacco product capable of avoiding burning as being heated and preparation method of tobacco product

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4955399A (en) * 1988-11-30 1990-09-11 R. J. Reynolds Tobacco Company Smoking article
US20050056294A1 (en) * 2002-11-19 2005-03-17 Wanna Joseph T. Modified reconstituted tobacco sheet
CN105249524A (en) * 2015-08-14 2016-01-20 贵州中烟工业有限责任公司 Fragrance type heating nonflammable tobacco product and preparation method thereof
CN204969442U (en) * 2015-08-18 2016-01-20 河南中烟工业有限责任公司 Novel for cigarette cigarette of electrical heating type heating incombustible
CN105747266B (en) * 2016-04-20 2021-05-28 贵州中烟工业有限责任公司 Preparation method of cigarette rod without burning tobacco by heating

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080078417A1 (en) * 2002-11-19 2008-04-03 Wanna Joseph T Process for making a bandcast tobacco sheet and smoking article therefrom
CN101039597A (en) * 2004-08-18 2007-09-19 布朗及威廉森控股公司 Reconstituted tobacco sheet and smoking article therefrom
CN103750535A (en) * 2014-01-22 2014-04-30 红云红河烟草(集团)有限责任公司 Preparation method of heating non-combustion type cigarette block
CN204362975U (en) * 2015-01-20 2015-06-03 川渝中烟工业有限责任公司 The aspirator of a kind of electrical heating not burning tobacco
CN204362974U (en) * 2015-01-20 2015-06-03 川渝中烟工业有限责任公司 A kind of charcoal heats the aspirator of not burning tobacco
CN104770874A (en) * 2015-03-21 2015-07-15 南通烟滤嘴有限责任公司 Hollow filter stick and production method thereof
CN104856215A (en) * 2015-06-25 2015-08-26 云南中烟工业有限责任公司 Reconstituted tobacco suitable for heating non-combustion type cigarettes
CN105105317A (en) * 2015-08-14 2015-12-02 贵州中烟工业有限责任公司 Strong-flavor type tobacco product being nonflammable while heating and preparation method thereof
CN105146734A (en) * 2015-08-14 2015-12-16 贵州中烟工业有限责任公司 Maotai-flavor tobacco product capable of avoiding burning as being heated and preparation method of tobacco product

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘良才 等: "外加植物纤维对造纸法烟草薄片物理性能的影响", 《中华纸业》 *

Cited By (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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