CN104921288A - Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes - Google Patents
Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes Download PDFInfo
- Publication number
- CN104921288A CN104921288A CN201510336314.3A CN201510336314A CN104921288A CN 104921288 A CN104921288 A CN 104921288A CN 201510336314 A CN201510336314 A CN 201510336314A CN 104921288 A CN104921288 A CN 104921288A
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- China
- Prior art keywords
- lily
- extract
- cigarette
- glycerol triacetate
- triacetyl glycerine
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses lily glycerol triacetate extract and application of the lily glycerol triacetate extract in cigarettes. Lily powder which is completely washed, dried and smashed to range from 10 meshes to 40 meshes serves as raw materials, glycerol triacetate serves as an extracting agent, firstly, extraction is conducted in a heating reflux mode, and then the lily glycerol triacetate extract is prepared through microwave extraction. The glycerol triacetate serves as a solvent, the lily glycerol triacetate extract is prepared into a solution with the concentration ranging from 2% to 5%, the solution is evenly sprayed to filter stick tows according to the 7-8% weight ratio of acetic acid fiber tows, cigarette filter sticks are prepared, and the cigarettes with the filter sticks containing effective lily components are prepared in the conventional cigarette rolling process. The extract can remarkably improve sweetness of the cigarettes, cigarette smell is abundant and coordinated, irritation and offensive odor are relieved, and the smoking quality of the cigarettes is effectively improved. The lily glycerol triacetate extract is simple in production process, high in operability and standardization and low in cost, raw materials are easy to obtain, industrial production is conveniently achieved, and good application prospects are achieved.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of lily triacetyl glycerine extract.Meanwhile, the invention still further relates to the described application of lily triacetyl glycerine extract in cigarette.
Background technology
Sweet, the micro-hardship of lily taste, cold nature, itself has fragrant and sweet gas, is the rare species resource of dietotherapeutic.Except main starch material, lily contains abundant amino acid, trace element, phosphatide, reduced sugar, steroid saponin, flavonoids and is similar to the multiple alkaloid component of autumn waters--limid eyes alkali.These composition comprehensive functions, in human body, have clearing away the lungheat and moisturizing, and enriching yin disappears effect of heat, clearing away the heart fire and tranquillizing, tonifying middle-Jiao and Qi, reducing fever and causing diuresis, detoxify cool blood, strengthening the spleen and stomach, is the good medicine that applicating history is long simply.In addition, lily also has antiviral, anti-oxidant, immunological regulation, antitumor, hypoglycemic, the anti-ageing effect of waiting for a long time.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN 103271441A) thereof, a kind of filter stick fiber base material additive and application (CN 103126073 A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN 104161303 A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in triacetyl glycerine dissolve add in cigarette, or the additive some being insoluble in triacetyl glycerine is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the solvability of triacetyl glycerine to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in triacetyl glycerine, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by triacetyl glycerine, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco business in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of Bulbus Lilii extract prepared using triacetyl glycerine as extractant is provided, this extract is applied to the fresh and sweet fragrance that cigarette can make to present in cigarette lily, and soft cigarette perfume is also coordinated with cigarette perfume, improves and modifies cigarette smoke.
The present invention also aims to provide the embody rule of described lily triacetyl glycerine extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage adopted in the present invention is mass percent.
A kind of lily triacetyl glycerine extract, is obtained by the method for following steps:
(1) cleaned by lily, drying 10 ~ 15 hours under 40 ~ 50 DEG C of conditions, pulverizing is 10 ~ 40 object powder, for subsequent use;
(2) take 3 ~ 5 parts of lily powder according to weight portion and be placed in round-bottomed flask, add 10 ~ 30 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 3 ~ 8 hours, refluxing extraction is carried out under 70 ~ 150 DEG C of conditions, extraction time is 4 ~ 10 hours, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in Microwave Extraction Equipment, under 200 ~ 600W, 2500MHZ condition, Extracting temperature is 50 ~ 90 DEG C, 15 ~ 55 minutes extraction times, cross the settled solution obtained after filtering filter residue and be required lily triacetyl glycerine extract.
The described application of lily triacetyl glycerine extract in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described lily triacetyl glycerine extract is mixed with the solution that concentration is 2 ~ 5%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the lily triacetyl glycerine extract prepared by the present invention, can dissolve each other in any proportion with triacetyl glycerine, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that lily exists by prior art when filter stick additive is mixed and is fitted in plasticizer.
2. adopt triacetyl glycerine to be that extractant extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in triacetyl glycerine in lily fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to triacetyl glycerine time, the loss of effective efficiency composition.
3. gained lily triacetyl glycerine extract can enrich and coordinate cigarette cigarette perfume, abirritate, cover assorted gas, increases the clear and rich sense of flue gas simultaneously, improves cigarette smoking quality.
4. material used herein is food-grade, has higher safety in utilization.
5. production technology of the present invention is simple, operability and normative strong, and raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
Lily is cleaned, drying 10 hours under 50 DEG C of conditions, be crushed to 40 orders and obtain lily powder, take 5 parts of lily powder according to weight portion and be placed in round-bottomed flask, add 15 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 4 hours, to be cooled to room temperature, lily after described refluxing extraction and triacetyl glycerine are placed in Microwave Extraction Equipment (400W, 2500MHZ), Extracting temperature is 50 DEG C, 30 minutes extraction times, cross after filtering filter residue and obtain settled solution, required lily triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, lily triacetyl glycerine extract is mixed with the solution that concentration is 2%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains lily active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette cigarette perfume adding above-mentioned lily triacetyl glycerine extract increases, and the sweet sense of flue gas and concentration promote to some extent, and excitant alleviates, pleasant impression is totally comfortable.
Embodiment 2
Lily is cleaned, drying 10 hours under 40 DEG C of conditions, pulverizing is 20 object powder, take 5 parts of lily powder according to weight portion and be placed in round-bottomed flask, add 25 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 8 hours, refluxing extraction is carried out under 120 DEG C of conditions, extraction time is 4 hours, to be cooled to room temperature, lily after described refluxing extraction and triacetyl glycerine are placed in Microwave Extraction Equipment (200W, 2500MHZ), Extracting temperature is 60 DEG C, 55 minutes extraction times, cross after filtering filter residue and obtain settled solution, required lily triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, lily triacetyl glycerine extract is mixed with the solution that concentration is 3%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains lily active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned lily triacetyl glycerine extract is pure and fresh simple and elegant, fine and smooth soft, and the fragrant rich increase of cigarette, assorted gas alleviates, pleasant impression is totally comfortable.
Embodiment 3
Lily is cleaned, drying 12 hours under 45 DEG C of conditions, pulverizing is 10 object powder, take 5 parts of lily powder according to weight portion and be placed in round-bottomed flask, add 20 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 3 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 48 hours, to be cooled to room temperature, lily after described refluxing extraction and triacetyl glycerine are placed in micro-extraction equipment (200W, 2500MHZ), Extracting temperature is 50 DEG C, 15 minutes extraction times, cross after filtering filter residue and obtain settled solution, required lily triacetyl glycerine extract can be obtained.
Take triacetyl glycerine as solvent, lily triacetyl glycerine extract is mixed with the solution that concentration is 5%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains lily active ingredient.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the sweet sense of cigarette flue gas adding above-mentioned lily triacetyl glycerine extract is obvious, and flue gas excitant and assorted gas obviously alleviate, and pleasant impression is more comfortable.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a lily triacetyl glycerine extract, is obtained by the method for following steps:
(1) cleaned by lily, drying 10 ~ 15 hours under 40 ~ 50 DEG C of conditions, pulverizing is 10 ~ 40 object powder, for subsequent use;
(2) take 3 ~ 5 parts of lily powder according to weight portion and be placed in round-bottomed flask, add 10 ~ 30 parts of glycerol triacetate for tobacco as extractant, soaking at room temperature is after 3 ~ 8 hours, refluxing extraction is carried out under 70 ~ 150 DEG C of conditions, extraction time is 4 ~ 10 hours, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in Microwave Extraction Equipment, under 200 ~ 600W, 2500MHZ condition, Extracting temperature is 50 ~ 90 DEG C, 15 ~ 55 minutes extraction times, cross the settled solution obtained after filtering filter residue and be required lily triacetyl glycerine extract.
2. the application of lily triacetyl glycerine extract according to claim 1 in cigarette, it is characterized in that: take triacetyl glycerine as solvent, described lily triacetyl glycerine extract is mixed with the solution that concentration is 2 ~ 5%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510336314.3A CN104921288A (en) | 2015-06-17 | 2015-06-17 | Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510336314.3A CN104921288A (en) | 2015-06-17 | 2015-06-17 | Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes |
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| CN104921288A true CN104921288A (en) | 2015-09-23 |
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| CN201510336314.3A Pending CN104921288A (en) | 2015-06-17 | 2015-06-17 | Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105733810A (en) * | 2016-03-18 | 2016-07-06 | 云南中烟工业有限责任公司 | Angelica sinensis glycerol triacetate extract and application thereof to cigarettes |
| CN109998165A (en) * | 2019-04-03 | 2019-07-12 | 红云红河烟草(集团)有限责任公司 | Cigarette filter stick plasticizer, preparation method thereof and cigarette filter stick |
| CN109998164A (en) * | 2019-04-03 | 2019-07-12 | 红云红河烟草(集团)有限责任公司 | Cigarette filter stick flavor enhancing particle and cigarette filter stick |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5074319A (en) * | 1990-04-19 | 1991-12-24 | R. J. Reynolds Tobacco Company | Tobacco extraction process |
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN104031741A (en) * | 2014-06-13 | 2014-09-10 | 广西中烟工业有限责任公司 | Preparation method for maillard reaction production particles of tobacco leaf extract |
| CN104403794A (en) * | 2014-09-24 | 2015-03-11 | 云南中烟工业有限责任公司 | Preparation method and application of Pu'er tea extract to cigarettes |
-
2015
- 2015-06-17 CN CN201510336314.3A patent/CN104921288A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5074319A (en) * | 1990-04-19 | 1991-12-24 | R. J. Reynolds Tobacco Company | Tobacco extraction process |
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN104031741A (en) * | 2014-06-13 | 2014-09-10 | 广西中烟工业有限责任公司 | Preparation method for maillard reaction production particles of tobacco leaf extract |
| CN104403794A (en) * | 2014-09-24 | 2015-03-11 | 云南中烟工业有限责任公司 | Preparation method and application of Pu'er tea extract to cigarettes |
Non-Patent Citations (1)
| Title |
|---|
| 罗金花: "微波辅助萃取百合多糖的工艺研究", 《宜春学院学报》, vol. 30, no. 4, 31 August 2008 (2008-08-31), pages 25 - 26 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105733810A (en) * | 2016-03-18 | 2016-07-06 | 云南中烟工业有限责任公司 | Angelica sinensis glycerol triacetate extract and application thereof to cigarettes |
| CN109998165A (en) * | 2019-04-03 | 2019-07-12 | 红云红河烟草(集团)有限责任公司 | Cigarette filter stick plasticizer, preparation method thereof and cigarette filter stick |
| CN109998164A (en) * | 2019-04-03 | 2019-07-12 | 红云红河烟草(集团)有限责任公司 | Cigarette filter stick flavor enhancing particle and cigarette filter stick |
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Application publication date: 20150923 |
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