CN109998165A - Cigarette filter stick plasticizer, preparation method thereof and cigarette filter stick - Google Patents
Cigarette filter stick plasticizer, preparation method thereof and cigarette filter stick Download PDFInfo
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- CN109998165A CN109998165A CN201910267797.4A CN201910267797A CN109998165A CN 109998165 A CN109998165 A CN 109998165A CN 201910267797 A CN201910267797 A CN 201910267797A CN 109998165 A CN109998165 A CN 109998165A
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- Prior art keywords
- filter stick
- cigarette filter
- agent
- floral
- plasticizer
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 80
- 239000004014 plasticizer Substances 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000003205 fragrance Substances 0.000 claims abstract description 48
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical group CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000002826 coolant Substances 0.000 claims abstract description 34
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 28
- 239000001087 glyceryl triacetate Substances 0.000 claims abstract description 18
- 235000013773 glyceryl triacetate Nutrition 0.000 claims abstract description 18
- 229960002622 triacetin Drugs 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 11
- 239000000796 flavoring agent Substances 0.000 claims abstract description 10
- 235000019634 flavors Nutrition 0.000 claims abstract description 10
- 239000012452 mother liquor Substances 0.000 claims abstract description 9
- 230000008569 process Effects 0.000 claims abstract description 8
- 239000010413 mother solution Substances 0.000 claims abstract description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 78
- 239000000243 solution Substances 0.000 claims description 28
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical group CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 27
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 27
- 229940041616 menthol Drugs 0.000 claims description 27
- 239000002904 solvent Substances 0.000 claims description 26
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 23
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
- 241000220317 Rosa Species 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 244000172533 Viola sororia Species 0.000 claims description 9
- 239000000834 fixative Substances 0.000 claims description 9
- 241000628997 Flos Species 0.000 claims description 7
- YZSJUQIFYHUSKU-UHFFFAOYSA-N ethanol;propane-1,2-diol Chemical compound CCO.CC(O)CO YZSJUQIFYHUSKU-UHFFFAOYSA-N 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 6
- 240000004153 Hibiscus sabdariffa Species 0.000 claims description 5
- 235000001018 Hibiscus sabdariffa Nutrition 0.000 claims description 5
- 235000010254 Jasminum officinale Nutrition 0.000 claims description 4
- 229960005150 glycerol Drugs 0.000 claims description 4
- 229940087068 glyceryl caprylate Drugs 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
- 229960004063 propylene glycol Drugs 0.000 claims description 4
- GHBFNMLVSPCDGN-UHFFFAOYSA-N rac-1-monooctanoylglycerol Chemical compound CCCCCCCC(=O)OCC(O)CO GHBFNMLVSPCDGN-UHFFFAOYSA-N 0.000 claims description 4
- 235000005206 Hibiscus Nutrition 0.000 claims description 3
- 235000007185 Hibiscus lunariifolius Nutrition 0.000 claims description 3
- 241000234435 Lilium Species 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims 2
- 244000284380 Hibiscus rosa sinensis Species 0.000 claims 1
- 240000005385 Jasminum sambac Species 0.000 claims 1
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 claims 1
- 241000208125 Nicotiana Species 0.000 abstract description 13
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 13
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 239000002304 perfume Substances 0.000 abstract description 5
- 238000012545 processing Methods 0.000 abstract description 4
- 230000002708 enhancing effect Effects 0.000 abstract description 3
- 239000000779 smoke Substances 0.000 description 10
- 210000000214 mouth Anatomy 0.000 description 8
- 230000001953 sensory effect Effects 0.000 description 7
- 230000000391 smoking effect Effects 0.000 description 6
- 241000207840 Jasminum Species 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 230000002045 lasting effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000000638 stimulation Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 241000218033 Hibiscus Species 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000008368 mint flavor Substances 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 241001672685 Ionopsis Species 0.000 description 1
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 238000005422 blasting Methods 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- GHVNFZFCNZKVNT-UHFFFAOYSA-M decanoate Chemical compound CCCCCCCCCC([O-])=O GHVNFZFCNZKVNT-UHFFFAOYSA-M 0.000 description 1
- PHALYIWLKRSLME-UHFFFAOYSA-N decanoic acid;2,3-dihydroxypropyl octanoate Chemical compound CCCCCCCCCC(O)=O.CCCCCCCC(=O)OCC(O)CO PHALYIWLKRSLME-UHFFFAOYSA-N 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 229940080812 glyceryl caprate Drugs 0.000 description 1
- 229940061567 glyceryl caprylate-caprate Drugs 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a cigarette filter stick plasticizer, a preparation method thereof and a cigarette filter stick, wherein the cigarette filter stick plasticizer comprises a floral scent agent, a cooling agent and a mother solution; the mass ratio of the flower fragrance agent to the cooling agent is 1:2-1:10, and the sum of the mass of the flower fragrance agent and the mass of the cooling agent is 5% -10% of the mass of the mother liquor; the mother liquor is glyceryl triacetate. The cigarette filter stick plasticizer disclosed by the invention can be directly added into a cigarette filter stick, the processing difficulty in the process of adding the plasticizer into the filter stick is small, the adding mode is simple, the mass production is easy to realize, the surface aroma loss of a tobacco shred flavoring link can be reduced, the flavor enhancing and flavoring cost can be favorably reduced, and the perfume pollution can be avoided.
Description
Technical Field
The invention relates to the technical field of cigarette production, in particular to a cigarette filter stick plasticizer, a preparation method thereof and a cigarette filter stick.
Background
In the cigarette production process, the tobacco shred flavoring process has important significance for forming cigarette style. The traditional tobacco shred flavoring process is to spray surface aroma on the surface of tobacco shreds in a flavoring roller in a spraying mode. The surface aroma of the flavoring mode is only attached to the surface of the cut tobacco and is difficult to permeate into the cut tobacco, so the surface aroma loss is easily caused. Moreover, the surface aroma changes on the surface of the cut tobacco due to combustion, and is not easy to be caught by consumers. In addition, when there are many volatile substances in the top note, the ability to fix the note is difficult to ensure. If the fragrance fixing capacity of the top note needs to be improved, a fragrance fixing agent which is difficult to volatilize needs to be added in the top note, so that the perfuming roller is polluted, the cleaning cost of perfuming equipment is increased, and the problem of perfume pollution among different batches also exists.
The above problems can be effectively solved by adding the characteristic incense into the filter stick. As the flavor substances in the filter stick do not participate in combustion, the flavor substances with low boiling points can be reserved, thereby providing good smoking experience for consumers. At present, the flavoring mode of the filter stick mainly comprises adding bead blasting, gel, aromatic threads or flavoring particles and the like into the filter stick. The flavoring mode of the filter stick can better keep the flavor style characteristics, but the flavor-carrying material has higher cost and large processing difficulty in the process of adding the flavor-carrying material into the filter stick, so the flavoring mode is more suitable for being used in middle-high-grade cigarettes.
Therefore, how to provide a low-cost cigarette filter stick flavoring way becomes a technical problem which needs to be solved urgently in the field.
Disclosure of Invention
The invention aims to provide a novel technical scheme of a low-cost cigarette filter stick plasticizer.
According to a first aspect of the present invention, there is provided a cigarette filter rod plasticiser.
The cigarette filter stick plasticizer comprises a floral scent agent, a cooling agent and a mother solution; wherein,
the mass ratio of the flower fragrance agent to the cooling agent is 1:2-1:10, and the sum of the mass of the flower fragrance agent and the mass of the cooling agent is 5% -10% of the mass of the mother liquor;
the mother liquor is glyceryl triacetate.
Optionally, the floral scent is a floral scent solution comprising 10-50 wt% of a floral scent source, and the floral scent source is at least one of a rose extract, a jasmine extract, a lily extract, a roselle extract and a violet extract, and the solvent of the floral scent solution is at least one of triacetin, glyceryl caprylate, propylene glycol and glycerol.
Optionally, the solvent of the floral solution is propylene glycol.
Optionally, the cooling agent is a menthol solution, the mass ratio of the menthol to the solvent in the menthol solution is 1:1-2:1, the solvent in the menthol solution comprises ethanol and a fragrance fixative in the mass ratio of 1:2-1:10, and the fragrance fixative is at least one of glyceryl triacetate, glyceryl caprylate, propylene glycol and glycerol.
Optionally, the fixative is propylene glycol.
Optionally, the solvents of the floral scent and the cooling agent are the same in kind.
According to a second aspect of the invention, a preparation method of the cigarette filter stick plasticizer is provided.
The preparation method of the cigarette filter stick plasticizer comprises the following steps:
(1) preparing a floral scent agent and a cooling agent;
(2) uniformly mixing the floral scent agent and the cooling agent according to the mass ratio of 1:2-1:10 to obtain a flavoring mixture;
(3) adding the flavoring mixture into the glyceryl triacetate according to the proportion of 5-10 wt%, and uniformly stirring to obtain the cigarette filter stick plasticizer.
Optionally, the process for preparing the floral scent in the step (1) is specifically as follows:
adding at least one of flos Rosae Rugosae extract, flos Jasmini sambac extract, Bulbus Lilii extract, Hibiscus Sabdariffae extract and violet extract into propylene glycol at a ratio of 10-50 wt%.
Optionally, the process for preparing the cooling agent in the step (1) is specifically as follows:
dissolving menthol into an ethanol-propylene glycol mixed solution according to the mass ratio of 1:1-2:1, wherein the ethanol-propylene glycol mixed solution comprises ethanol and propylene glycol in the mass ratio of 1:2-1: 10.
According to a third aspect of the present invention, there is provided a cigarette filter rod.
The cigarette filter stick comprises the cigarette filter stick plasticizer disclosed by the invention, and the cigarette filter stick plasticizer is added into the cigarette filter stick in an adding amount of 3-5 mg/mm.
The cigarette filter stick plasticizer disclosed by the invention can be directly added into a cigarette filter stick, the processing difficulty in the process of adding the plasticizer into the filter stick is small, the adding mode is simple, the mass production is easy to realize, the surface aroma loss of a tobacco shred flavoring link can be reduced, the flavor enhancing and flavoring cost can be favorably reduced, and the perfume pollution can be avoided.
The cigarette filter stick plasticizer disclosed by the invention combines the flower fragrance with the tobacco original fragrance, the flower fragrance is lasting, almost no attenuation is caused along with the time, the comfortable cool feeling of the oral cavity and the throat can be generated, the stimulation is reduced, the cigarette filter stick plasticizer is elegant and elegant during smoking, and the sensory quality of cigarettes can be improved.
Other features of the present invention and its advantages will become apparent from the following detailed description of exemplary embodiments of the invention.
Detailed Description
Various exemplary embodiments of the present invention will now be described in detail. It should be noted that: the relative arrangement of the components and steps, the numerical expressions and numerical values set forth in these embodiments do not limit the scope of the present invention unless specifically stated otherwise.
The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses.
Techniques, methods, and apparatus known to those of ordinary skill in the relevant art may not be discussed in detail but are intended to be part of the specification where appropriate.
In all examples shown and discussed herein, any particular value should be construed as merely illustrative, and not limiting. Thus, other examples of the exemplary embodiments may have different values.
The cigarette filter stick plasticizer disclosed by the invention comprises a floral scent agent, a cooling agent and mother liquor.
The mass ratio of the flower fragrance agent to the cooling agent is 1:2-1:10, and the sum of the mass of the flower fragrance agent and the mass of the cooling agent is 5% -10% of the mass of the mother liquor. The proportion of the flower fragrance agent and the cooling agent can be selected by the person skilled in the art according to the actual requirement.
Common floral fragrances may be, for example, floral or floral essences. A common cooling agent may for example be menthol or menthol.
The mother liquor is glyceryl triacetate. Glyceryl triacetate is not easy to volatilize, has lasting fragrance fixing ability, can not change fragrance characteristics after being stored for a long time, and does not cause pollution to smoke.
The cigarette filter stick plasticizer is added with a cooling agent on the basis of the fragrance of the flower, so that the mouth and the throat feel cool more obviously and more comfortably. Meanwhile, sweet and greasy feeling brought by the flower fragrance is counteracted to a certain extent, and the cigarette is more elegant and elegant during smoking.
The cigarette filter stick plasticizer disclosed by the invention can be directly added into a cigarette filter stick, the processing difficulty in the process of adding the plasticizer into the filter stick is small, the adding mode is simple, the mass production is easy to realize, the surface aroma loss of a tobacco shred flavoring link can be reduced, the flavor enhancing and flavoring cost can be favorably reduced, and the perfume pollution can be avoided.
The cigarette filter stick plasticizer disclosed by the invention combines the flower fragrance with the tobacco original fragrance, the flower fragrance is lasting, almost no attenuation is caused along with the time, the comfortable cool feeling of the oral cavity and the throat can be generated, the stimulation is reduced, the cigarette filter stick plasticizer is elegant and elegant during smoking, and the sensory quality of cigarettes can be improved.
In practice of the cigarette filter rod plasticizer of the present disclosure, the floral agent may be a floral solution comprising 10-50 wt% of a floral source, and the floral source is at least one of a rose extract, a jasmine extract, a lily extract, a roselle extract, and a violet extract. The solvent of the flower fragrance solution is at least one of glyceryl triacetate, glyceryl caprylate-caprate, propylene glycol and glycerol. The skilled person can select suitable floral source type and solvent type according to actual needs.
One or more of glyceryl triacetate, caprylic capric acid glyceride, propylene glycol, glycerol and the like are used as a solvent, so that the volatilization of the floral fragrance source is reduced while the floral fragrance source is effectively dissolved, the fragrance fixing capacity is durable, the fragrance characteristics can not be changed after the floral fragrance source is stored for years, and the smoke can not be polluted.
Further, the solvent of the floral solution is propylene glycol.
When the cigarette filter stick plasticizer disclosed by the invention is implemented, the cooling agent can be a menthol solution, and the mass ratio of the menthol to the solvent in the menthol solution is 1:1-2: 1. The solvent of the menthol solution comprises ethanol and a fragrance fixing agent in a mass ratio of 1:2-1:10, wherein the fragrance fixing agent is at least one of glyceryl triacetate, glyceryl caprylate/caprate, propylene glycol and glycerol. The skilled person can select the appropriate menthol content and solvent type according to the actual needs.
The compound solvent which contains one or more of ethanol, glyceryl triacetate, caprylic capric acid glyceride, propylene glycol, glycerol and the like as the flavor fixative is used, the volatilization of the menthol is reduced while the menthol is effectively dissolved, the flavor fixative capacity is durable, the cool flavor characteristic can not be changed after the menthol is stored for years, and the smoke can not be polluted.
Further, the perfume fixative is propylene glycol.
When the cigarette filter stick plasticizer disclosed by the invention is implemented, the types of solvents of the floral scents and the cooling agent are the same. The same kind of solvents can be exemplified by: the flower scent agent adopts propylene glycol as a solvent, the cooling agent adopts ethanol-propylene glycol as a solvent, and the content of the propylene glycol in the solvent of the cooling agent is greater than that of the ethanol. The solvent types of the flower fragrance agent and the cooling agent of the cigarette filter stick plasticizer are the same, so that the flower fragrance agent and the cooling agent are further fused, and the sensory quality of cigarettes is improved.
The disclosure also provides a preparation method of the cigarette filter stick plasticizer, which comprises the following steps:
step (1): preparing floral scents and cooling agents.
Step (2): and uniformly mixing the floral scent agent and the cooling agent according to the mass ratio of 1:2-1:10 to obtain the aroma-enhancing mixture.
And (3): adding the flavoring mixture into the glyceryl triacetate according to the proportion of 5-10 wt%, and uniformly stirring to obtain the cigarette filter stick plasticizer.
When the preparation method of the cigarette filter stick plasticizer disclosed by the invention is implemented, the process for preparing the floral scent agent in the step (1) can be specifically as follows:
adding at least one of flos Rosae Rugosae extract, flos Jasmini sambac extract, Bulbus Lilii extract, Hibiscus Sabdariffae extract and violet extract into propylene glycol at a ratio of 10-50 wt%.
When the preparation method of the cigarette filter stick plasticizer disclosed by the present disclosure is implemented, the process of preparing the cooling agent in step (1) may be specifically as follows:
dissolving menthol into an ethanol-propylene glycol solution according to the mass ratio of 1:1-2:1, wherein the ethanol-propylene glycol solution comprises ethanol and propylene glycol in the mass ratio of 1:2-1: 10.
The cigarette filter stick plasticizer disclosed by the invention can be added into a cigarette filter stick in an adding amount of 3-5mg/mm (3-5 mg of plasticizer is added into each mm of cigarette filter stick).
The experimental procedures used in the examples below are conventional unless otherwise specified, the materials and reagents used therein are commercially available, and the equipment used in the experiments are well known to those skilled in the art without otherwise specified.
Example 1
The rose extract was dissolved in propylene glycol at a ratio of 25 wt% to make a rose floral solution. Dissolving menthol in a solvent comprising ethanol and propylene glycol (mass ratio of 1:10) at a ratio of 1.5:1, and making into menthol solution. And mixing the rose fragrance solution and the menthol solution according to the mass ratio of 1:3 to obtain the flavoring mixture. The flavoring mixture is dissolved in glyceryl triacetate according to the proportion of 8 wt%, and the rose mint flavor plasticizer is prepared.
The prepared rose mint-flavored plasticizer is added into a cigarette filter stick (5mg/mm), and then the cigarette is rolled, and sensory evaluation results show that: the flavored filter stick can obviously improve the characteristics of smoke, has obvious rose characteristic fragrance, cool feeling in the oral cavity and the throat, and is fresh and comfortable in the oral cavity after being sucked and has light fragrance residue. Compared with cigarettes made by rolling common filter sticks, the cigarette stimulation of the flavoring filter stick is obviously reduced, the rose fragrance and the tobacco fragrance are coordinated, the richness is increased, the sweet and charm feeling of smoke is increased during smoking, the oral cavity generates body fluid and returns sweet after smoking, and the sensory quality of the cigarettes is obviously improved.
The flavoring effect of the cigarette filter stick is not reduced after the cigarettes are stored for 6 months.
Example 2
Dissolving Hibiscus sabdariffa extract, flos Jasmini sambac extract, and violet extract in propylene glycol at a ratio of 20 wt%, 10 wt%, and making into mixed flower fragrance solution. Dissolving menthol in a solvent comprising ethanol and propylene glycol (mass ratio of 1:10) at a ratio of 1.5:1, and making into menthol solution. And mixing the mixed flower fragrance solution and the menthol solution according to the mass ratio of 1:2 to obtain the aroma-enhancing mixture. The flavoring mixture is dissolved in glyceryl triacetate at a ratio of 6 wt% to obtain the mixed floral mint flavor plasticizer.
The prepared mixed floral mint plasticizer is added into a cigarette filter stick (5mg/mm), and then the cigarette is rolled, and sensory evaluation results show that: the flavored filter stick can obviously improve the style characteristics of smoke, the smoke with flower fragrance has the characteristics of front, middle and back blending, the aroma characteristics presented by different flower fragrances can be sensed in each stage of suction, the aroma is roselle, jasmine and violet in sequence, and the residual taste in the oral cavity is mainly violet. Compared with cigarettes made by rolling common filter sticks, the cigarette with the flavoring filter stick has the advantages that the smoke richness is increased, the cigarette has the layering property, the mixed flower fragrance and the tobacco fragrance are coordinated, the smoke is soft and comfortable, the mouth cavity and the throat part have cooling feeling, and the fresh violet orchid fragrance is accompanied. The smoke irritation is obviously improved, and the integral sensory quality of the cigarette is obviously improved.
The flavoring effect of the cigarette filter stick is not reduced after the cigarettes are stored for 6 months.
Although some specific embodiments of the present invention have been described in detail by way of examples, it should be understood by those skilled in the art that the above examples are for illustrative purposes only and are not intended to limit the scope of the present invention. It will be appreciated by those skilled in the art that modifications may be made to the above embodiments without departing from the scope and spirit of the invention. The scope of the invention is defined by the appended claims.
Claims (10)
1. The cigarette filter stick plasticizer is characterized by comprising a floral scent agent, a cooling agent and a mother solution; wherein,
the mass ratio of the flower fragrance agent to the cooling agent is 1:2-1:10, and the sum of the mass of the flower fragrance agent and the mass of the cooling agent is 5% -10% of the mass of the mother liquor;
the mother liquor is glyceryl triacetate.
2. The cigarette filter stick plasticizer according to claim 1, wherein the floral agent is a floral solution comprising 10-50 wt% of a floral source, and the floral source is at least one of rose extract, jasmine extract, lily extract, roselle extract and violet extract, and the solvent of the floral solution is at least one of triacetin, caprylin, propylene glycol and glycerin.
3. The cigarette filter stick plasticizer according to claim 2, wherein the solvent of the floral solution is propylene glycol.
4. The cigarette filter stick plasticizer according to claim 1, wherein the cooling agent is a menthol solution, the mass ratio of menthol to a solvent in the menthol solution is 1:1-2:1, the solvent in the menthol solution comprises ethanol and a fragrance fixative in the mass ratio of 1:2-1:10, and the fragrance fixative is at least one of glyceryl triacetate, glyceryl caprylate, propylene glycol and glycerol.
5. The cigarette filter stick plasticizer according to claim 4, wherein the fixative is propylene glycol.
6. The cigarette filter stick plasticizer according to any one of claims 1 to 5, wherein the solvents of the flower flavor agent and the cooling agent are the same.
7. A preparation method of a cigarette filter stick plasticizer is characterized by comprising the following steps:
(1) preparing a floral scent agent and a cooling agent;
(2) uniformly mixing the floral scent agent and the cooling agent according to the mass ratio of 1:2-1:10 to obtain a flavoring mixture;
(3) adding the flavoring mixture into the glyceryl triacetate according to the proportion of 5-10 wt%, and uniformly stirring to obtain the cigarette filter stick plasticizer.
8. The preparation method according to claim 7, wherein the process of preparing the floral scent in step (1) is as follows:
adding at least one of flos Rosae Rugosae extract, flos Jasmini sambac extract, Bulbus Lilii extract, Hibiscus Sabdariffae extract and violet extract into propylene glycol at a ratio of 10-50 wt%.
9. The method according to claim 7, wherein the step (1) of preparing the cooling agent comprises the following steps:
dissolving menthol into an ethanol-propylene glycol mixed solution according to the mass ratio of 1:1-2:1, wherein the ethanol-propylene glycol mixed solution comprises ethanol and propylene glycol in the mass ratio of 1:2-1: 10.
10. A cigarette filter stick, characterized in that the cigarette filter stick comprises the cigarette filter stick plasticizer according to any one of claims 1 to 6, and the cigarette filter stick plasticizer is added into the cigarette filter stick at an addition amount of 3-5 mg/mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910267797.4A CN109998165A (en) | 2019-04-03 | 2019-04-03 | Cigarette filter stick plasticizer, preparation method thereof and cigarette filter stick |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910267797.4A CN109998165A (en) | 2019-04-03 | 2019-04-03 | Cigarette filter stick plasticizer, preparation method thereof and cigarette filter stick |
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| Publication Number | Publication Date |
|---|---|
| CN109998165A true CN109998165A (en) | 2019-07-12 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910267797.4A Pending CN109998165A (en) | 2019-04-03 | 2019-04-03 | Cigarette filter stick plasticizer, preparation method thereof and cigarette filter stick |
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| Country | Link |
|---|---|
| CN (1) | CN109998165A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111418892A (en) * | 2020-05-20 | 2020-07-17 | 云南如茨生物科技有限公司 | Cigarette filter stick additive and application thereof |
| CN113817547A (en) * | 2021-11-03 | 2021-12-21 | 江苏大亚滤嘴材料有限公司 | Hawthorn essence for cigarettes and application of hawthorn essence to filter stick |
| CN114828812A (en) * | 2019-12-20 | 2022-07-29 | 欧莱雅 | Composition comprising rose plant extract |
| WO2023021292A1 (en) * | 2021-08-18 | 2023-02-23 | Essentra Filter Products Development Co Pte Ltd. | A cooling element |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040107971A1 (en) * | 2002-09-17 | 2004-06-10 | Abhijit De | Gum based chewing product and process for preparing the same |
| CN1994164A (en) * | 2006-12-13 | 2007-07-11 | 云南瑞升烟草技术（集团）有限公司 | Acetate plasticizer for improving smoking property of cigarette and method for preparing same |
| US20110083676A1 (en) * | 2009-10-09 | 2011-04-14 | Philip Morris Usa Inc. | Coated impregnated porous filter plug |
| CN103211304A (en) * | 2013-05-13 | 2013-07-24 | 湖北中烟工业有限责任公司 | Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate |
| CN104921288A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes |
| CN105029696A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Black tea glycerol triacetate extract and application thereof in cigarettes |
| CN105410997A (en) * | 2015-11-24 | 2016-03-23 | 云南养瑞科技集团有限公司 | Cigarette filter stick additive and application thereof |
| CN104161303B (en) * | 2014-07-16 | 2018-11-30 | 广西中烟工业有限责任公司 | A kind of cool taste mint type cigarette filter stick additive preparation method and applications |
| CN109156895A (en) * | 2018-08-07 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of reduction cigarette smoking dry sensation and irritating filter stick additive, preparation method and the usage |
| CN109275956A (en) * | 2018-09-20 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of additives of filter tip and preparation method thereof based on the cool taste component of the eastern purple perilla of purification |
-
2019
- 2019-04-03 CN CN201910267797.4A patent/CN109998165A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040107971A1 (en) * | 2002-09-17 | 2004-06-10 | Abhijit De | Gum based chewing product and process for preparing the same |
| CN1994164A (en) * | 2006-12-13 | 2007-07-11 | 云南瑞升烟草技术（集团）有限公司 | Acetate plasticizer for improving smoking property of cigarette and method for preparing same |
| US20110083676A1 (en) * | 2009-10-09 | 2011-04-14 | Philip Morris Usa Inc. | Coated impregnated porous filter plug |
| CN103211304A (en) * | 2013-05-13 | 2013-07-24 | 湖北中烟工业有限责任公司 | Preparation method of filter stick using cigarette harm-reducing synergistic agent containing glycerol triacetate |
| CN104161303B (en) * | 2014-07-16 | 2018-11-30 | 广西中烟工业有限责任公司 | A kind of cool taste mint type cigarette filter stick additive preparation method and applications |
| CN104921288A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes |
| CN105029696A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Black tea glycerol triacetate extract and application thereof in cigarettes |
| CN105410997A (en) * | 2015-11-24 | 2016-03-23 | 云南养瑞科技集团有限公司 | Cigarette filter stick additive and application thereof |
| CN109156895A (en) * | 2018-08-07 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of reduction cigarette smoking dry sensation and irritating filter stick additive, preparation method and the usage |
| CN109275956A (en) * | 2018-09-20 | 2019-01-29 | 云南中烟工业有限责任公司 | A kind of additives of filter tip and preparation method thereof based on the cool taste component of the eastern purple perilla of purification |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114828812A (en) * | 2019-12-20 | 2022-07-29 | 欧莱雅 | Composition comprising rose plant extract |
| CN111418892A (en) * | 2020-05-20 | 2020-07-17 | 云南如茨生物科技有限公司 | Cigarette filter stick additive and application thereof |
| WO2023021292A1 (en) * | 2021-08-18 | 2023-02-23 | Essentra Filter Products Development Co Pte Ltd. | A cooling element |
| CN113817547A (en) * | 2021-11-03 | 2021-12-21 | 江苏大亚滤嘴材料有限公司 | Hawthorn essence for cigarettes and application of hawthorn essence to filter stick |
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Application publication date: 20190712 |