CN102772340A - Tibetan saussurea toothpaste and preparation method thereof - Google Patents

Tibetan saussurea toothpaste and preparation method thereof Download PDF

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Publication number
CN102772340A
CN102772340A CN2012102960340A CN201210296034A CN102772340A CN 102772340 A CN102772340 A CN 102772340A CN 2012102960340 A CN2012102960340 A CN 2012102960340A CN 201210296034 A CN201210296034 A CN 201210296034A CN 102772340 A CN102772340 A CN 102772340A
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China
Prior art keywords
maxim
kir
extract
toothpaste
saussurea involucrata
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CN2012102960340A
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Chinese (zh)
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韩成芳
杜连平
陈海莲
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Qinghai Arula Tibetan Medicine And Pharmacology Research And Development Co Ltd
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Qinghai Arula Tibetan Medicine And Pharmacology Research And Development Co Ltd
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Priority to CN2012102960340A priority Critical patent/CN102772340A/en
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Abstract

The invention relates to an article for daily use, in particular to Tibetan saussurea toothpaste and a preparation method thereof. The Tibetan saussurea toothpaste contains calcium carbonate, sorbitol, carboxyl cellulose, guar gum, saccharin sodium, sodium sulfovinate alcoholate, sodium pyrophosphate, silicon oxide, methyl sodium, propylene glycol, deionized water, essence, menthol, Tibetan saussurea extract, white tea extract, nano angelica and nano halite. The Tibetan saussurea toothpaste takes Tibetan saussurea as a main ingredient and takes white tea as an auxiliary ingredient and is extracted by the modern technological process; and the repeated tests show that the formula is scientific and reasonable. The Tibetan saussurea toothpaste has the functions of resisting bacteria and diminishing inflammation, has good effects on preventing and curing oral inflammation, and has the functions of expelling toxins and reducing pathogenic fire as well as improving the immunity of the oral cavity. Through the invention, the production method is simple and low in cost, and the product has a wide range of application, thereby providing a good way for the wide application of Tibetan saussurea.

Description

A kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste and manufacture method
One, technical field
The present invention relates to a kind of article of everyday use, particularly a kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste and manufacture method.
Two, background technology
Saussurea involucrata Kar. et Kir. et Maxim., Tibetan language transliteration " just lamb plain crust ", its former plant is Saussurea medusa, also claims Saussurea medusa Maxim. (Saussurea medusa Maxim.).Saussurea involucrata Kar. et Kir. et Maxim. originates in ground such as Tibet, Qinghai, Sichuan, Yunnan and Kashmir; Being born in the high mountain flowstone beach of height above sea level 3900~5600 m, is one type of rare species with nutritious tonifying and pharmacological function that ground ethnic groups such as China Qinghai, Tibet, Xinjiang are used, and the Tibetan medicine thinks; Its hardship of Saussurea involucrata Kar. et Kir. et Maxim., cold; Heat-clearing and toxic substances removing, wind-damp dispelling, the meridian dredging, and can enrich blood, can be used for gynaecopathias such as menoxenia, metrorrhagia and leukorrhagia, placenta retention.Modern study shows, contains multiple bioactive ingredients such as flavonoid, polysaccharide and phenols in the Saussurea involucrata Kar. et Kir. et Maxim., has anti-damage, antioxidation and removes effects such as free radical, bactericidal antiphlogistic and anticancer growth.Yet at present but very original to the development and use of Saussurea involucrata Kar. et Kir. et Maxim., traditional habit pattern such as mostly adopt decoction, steep in wine, the industrialized developing degree is very low, and corresponding product is also fewer, fails to be popularized for masses, and the Saussurea involucrata Kar. et Kir. et Maxim. resource is not fully used.Toothpaste is to use one of the highest article of everyday use of popularity rate; Though at present the effect toothpaste on the domestic and international daily use chemicals market is a feast for the eyes, Saussurea involucrata Kar. et Kir. et Maxim. is not carried out scientific and reasonable compatibility, makes full use of the unique effect of Saussurea involucrata Kar. et Kir. et Maxim. and form the health-care toothpaste of specific therapeutical.
Three, summary of the invention
The purpose of this invention is to provide the scientific and reasonable compatibility of a kind of process and have the health-care toothpaste of eliminating oral inflammation, pathogenic fire reducing, strong tooth.Technical scheme of the present invention is: a kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste is characterized in that in its component, containing by weight: calcium carbonate 40 ~ 50, sorbitol 15 ~ 25, carboxymethylated cellulose 0.2 ~ 1.5, guar gum 0.1 ~ 1, saccharin sodium 0 ~ 0.5, pure sodium sulfovinate 0.5 ~ 2.5, tetrasodium pyrophosphate 0 ~ 1, silica 1 ~ 5, methyl ester sodium 0 ~ 0.5, propylene glycol 1 ~ 3.5, deionized water 15 ~ 30, essence 0 ~ 0.8, Mentholum 0 ~ 1, Saussurea involucrata Kar. et Kir. et Maxim. extract 0.2 ~ 1.5, Ramulus et Folium Mussaendae Pubescentis extract 0 ~ 0.6, nano angelica root 0 ~ 0.6, nanometer halite 0 ~ 0.6; Its manufacture method is: earlier sorbitol is joined in the vacuum Manufacturing medicine extract machine, add carboxymethylated cellulose, guar gum, pure sodium sulfovinate, tetrasodium pyrophosphate, silicon dioxide, methyl ester sodium, the abundant mixing of propylene glycol again, add deionized water then; Mixing under the vacuum stirring state, adds the Saussurea involucrata Kar. et Kir. et Maxim. extract, Ramulus et Folium Mussaendae Pubescentis extract, nano angelica root, nanometer halite, saccharin sodium, calcium carbonate, the Mentholum that carry out dispersing and dissolving with deionized water successively once more; Under vacuum state; (20 ~ 6000rpm) stir abundant mixing, add essence at last, once more under vacuum state to carry out high speed; Carry out the fully emulsified mixing of high-speed stirred, promptly get product; Saussurea involucrata Kar. et Kir. et Maxim. extract of the present invention is the Saussurea involucrata Kar. et Kir. et Maxim. raw material through adding volume ratio is 85% alcohol reflux 2 times, each 1.5 ~ 2 h, and merge extractive liquid, filters, and is condensed into relative density and is 1.25 ~ 1.30 extractum; Ramulus et Folium Mussaendae Pubescentis extract of the present invention is the Ramulus et Folium Mussaendae Pubescentis extract juice that Ramulus et Folium Mussaendae Pubescentis obtains after supercritical carbon dioxide extraction method extracts, removes slag; Essence of the present invention is Herba Menthae essence or jasmine flower essence or Flos Chrysanthemi Indici absolute oil or other plant essence or synthetic class essence.
The present invention has following advantage and effect: the present invention says from compatibility, is main with Saussurea involucrata Kar. et Kir. et Maxim., and the Ramulus et Folium Mussaendae Pubescentis that being aided with property is refrigerant, the heat drop fire that disappears, relieve summer heating Detoxication have the title of " five kinds of tea " extract with the modern crafts method, and through repetition test, scientific formulation is reasonable; Has effect antibiotic, antiinflammatory; Oral inflammation such as oral ulcer, stomatitis, gingivitis, periodontitis, pharyngitis had good preventing and health-care effect; Also have the effect of toxin expelling pathogenic fire reducing and improve oral immunisation power, production method of the present invention is simple, cost is low, and application range of products is wide; No matter men and women, old and young can use product of the present invention, for Saussurea involucrata Kar. et Kir. et Maxim. widely-used provides good approach.
Four, the specific embodiment
Embodiment 1: a kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste; Wherein calcium carbonate 40kg, sorbitol 25kg, carboxymethylated cellulose 0.2kg, guar gum 0.1kg, saccharin sodium 0.0kg, pure sodium sulfovinate 0.5kg, tetrasodium pyrophosphate 0.0kg, silica 1 kg, methyl ester sodium 0.0kg, propylene glycol 1kg, deionized water 15kg, jasmine flower essence 0.8kg, Mentholum 0.0kg, Saussurea involucrata Kar. et Kir. et Maxim. extractum 0.2kg, Ramulus et Folium Mussaendae Pubescentis extract 0.05kg, nano angelica root 0.0 kg, nanometer halite 0.0 kg.Its manufacture method is: earlier sorbitol is joined in the vacuum Manufacturing medicine extract machine, add carboxymethylated cellulose, guar gum, pure sodium sulfovinate, tetrasodium pyrophosphate, silicon dioxide, methyl ester sodium, the abundant mixing of propylene glycol again, add deionized water then; Mixing under the vacuum stirring state, adds the Saussurea involucrata Kar. et Kir. et Maxim. extract, Ramulus et Folium Mussaendae Pubescentis extract, nano angelica root, nanometer halite, saccharin sodium, calcium carbonate, the Mentholum that carry out dispersing and dissolving with deionized water successively once more; Under vacuum state; (20 ~ 6000rpm) stir abundant mixing, add essence at last, once more under vacuum state to carry out high speed; Carry out the fully emulsified mixing of high-speed stirred, promptly get product; The Saussurea involucrata Kar. et Kir. et Maxim. extract be the Saussurea involucrata Kar. et Kir. et Maxim. raw material through adding volume ratio is 85% alcohol reflux 2 times in the present embodiment; Each 2 h; Merge extractive liquid; Filter, be condensed into relative density and be 1.25 extractum, Ramulus et Folium Mussaendae Pubescentis extract is the Ramulus et Folium Mussaendae Pubescentis extract juice that Ramulus et Folium Mussaendae Pubescentis obtains after supercritical carbon dioxide extraction method extracts, removes slag;
Embodiment 2: a kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste; Wherein calcium carbonate 50kg, sorbitol 15kg, carboxymethylated cellulose 1.5kg, guar gum 1kg, saccharin sodium 0.5kg, pure sodium sulfovinate 2.5kg, tetrasodium pyrophosphate 1kg, silicon dioxide 5kg, methyl ester sodium 0.5kg, propylene glycol 3.5kg, deionized water 30kg, jasmine flower essence 0.8kg, Mentholum 1kg, Saussurea involucrata Kar. et Kir. et Maxim. extract 1.5kg, Ramulus et Folium Mussaendae Pubescentis extract 0.6kg; Nano angelica root 0.6 kg, nanometer halite 0.6kg, method for preparing is with embodiment 1; The Saussurea involucrata Kar. et Kir. et Maxim. extract be the Saussurea involucrata Kar. et Kir. et Maxim. raw material through adding volume ratio is 85% alcohol reflux 2 times in the present embodiment; Each 1.5 h; Merge extractive liquid; Filter, be condensed into relative density and be 1.30 extractum, Ramulus et Folium Mussaendae Pubescentis extract is the Ramulus et Folium Mussaendae Pubescentis extract juice that Ramulus et Folium Mussaendae Pubescentis obtains after supercritical carbon dioxide extraction method extracts, removes slag;
Embodiment 3: a kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste; Wherein calcium carbonate 46 kg, sorbitol 20 kg, carboxycellulose 1.05 kg, guar gum 0.35 kg, saccharin sodium 0.2 kg, pure sodium sulfovinate 1.85 kg, tetrasodium pyrophosphate 0.35 kg, silicon dioxide 2.5 kg, methyl ester sodium 0.15 kg, propylene glycol 2.5 kg, deionized water 23 kg, Flos Chrysanthemi Indici absolute oil essence 0.5 kg, Mentholum 0.4 kg, Saussurea involucrata Kar. et Kir. et Maxim. extract 0.5kg, Ramulus et Folium Mussaendae Pubescentis extract 0.5 kg, nano angelica root 0.5 kg, nanometer halite 0.5 kg, method for preparing is with embodiment 1; The Saussurea involucrata Kar. et Kir. et Maxim. extract be the Saussurea involucrata Kar. et Kir. et Maxim. raw material through adding volume ratio is 85% alcohol reflux 2 times in the present embodiment; Each 1.8 h; Merge extractive liquid; Filter, be condensed into relative density and be 1.28 extractum, Ramulus et Folium Mussaendae Pubescentis extract is the Ramulus et Folium Mussaendae Pubescentis extract juice that Ramulus et Folium Mussaendae Pubescentis obtains after supercritical carbon dioxide extraction method extracts, removes slag.
Embodiment 4: formula for a product of the present invention: calcium carbonate 42kg, sorbitol 18kg, carboxymethylated cellulose 0.5kg, guar gum 0.7kg, saccharin sodium 0.3kg, pure sodium sulfovinate 2.2kg, tetrasodium pyrophosphate 0.5kg, silicon dioxide 3kg, methyl ester sodium 0.3kg, propylene glycol 2kg, deionized water 25kg, synthetic class essence 0.5kg, Mentholum 0.6kg, Saussurea involucrata Kar. et Kir. et Maxim. extractum 1kg, Ramulus et Folium Mussaendae Pubescentis extract 0.6kg, and method for preparing is with embodiment 1; The Saussurea involucrata Kar. et Kir. et Maxim. extract be the Saussurea involucrata Kar. et Kir. et Maxim. raw material through adding volume ratio is 85% alcohol reflux 2 times in the present embodiment; Each 1.8 h; Merge extractive liquid; Filter, be condensed into relative density and be 1.28 extractum, Ramulus et Folium Mussaendae Pubescentis extract is the Ramulus et Folium Mussaendae Pubescentis extract juice that Ramulus et Folium Mussaendae Pubescentis obtains after supercritical carbon dioxide extraction method extracts, removes slag.
Embodiment 5: formula for a product of the present invention: calcium carbonate 48kg, sorbitol 22kg, carboxymethylated cellulose 1.2kg, guar gum 0.2kg, saccharin sodium 0.1kg, pure sodium sulfovinate 0.8kg, tetrasodium pyrophosphate 0.2kg, silicon dioxide 2kg, methyl ester sodium 0.1kg, propylene glycol 3kg, deionized water 20kg, Herba Menthae essence 0.1kg, Mentholum 0.2kg, Saussurea involucrata Kar. et Kir. et Maxim. extractum 0.2kg, Ramulus et Folium Mussaendae Pubescentis extract 0.2kg, and method for preparing is with embodiment 1; The Saussurea involucrata Kar. et Kir. et Maxim. extract be the Saussurea involucrata Kar. et Kir. et Maxim. raw material through adding volume ratio is 85% alcohol reflux 2 times in the present embodiment; Each 2 h; Merge extractive liquid; Filter, be condensed into relative density and be 1.30 extractum, Ramulus et Folium Mussaendae Pubescentis extract is the Ramulus et Folium Mussaendae Pubescentis extract juice that Ramulus et Folium Mussaendae Pubescentis obtains after supercritical carbon dioxide extraction method extracts, removes slag.
Embodiment 6: formula for a product of the present invention: calcium carbonate 44kg, sorbitol 22kg, carboxymethylated cellulose 0.8kg, guar gum 0.8kg, saccharin sodium 0.2kg, pure sodium sulfovinate 2kg, tetrasodium pyrophosphate 0.8kg, silicon dioxide 4kg, methyl ester sodium 0.4kg, propylene glycol 2.5kg, deionized water 25kg, Herba Menthae essence 0.7kg, Mentholum 0.2kg, Saussurea involucrata Kar. et Kir. et Maxim. extractum 1.2kg, Ramulus et Folium Mussaendae Pubescentis extract 0.5kg, and method for preparing is with embodiment 1; The Saussurea involucrata Kar. et Kir. et Maxim. extract be the Saussurea involucrata Kar. et Kir. et Maxim. raw material through adding volume ratio is 85% alcohol reflux 2 times in the present embodiment; Each 1.8 h; Merge extractive liquid; Filter, be condensed into relative density and be 1.28 extractum, Ramulus et Folium Mussaendae Pubescentis extract is the Ramulus et Folium Mussaendae Pubescentis extract juice that Ramulus et Folium Mussaendae Pubescentis obtains after supercritical carbon dioxide extraction method extracts, removes slag.

Claims (4)

1. a Saussurea involucrata Kar. et Kir. et Maxim. toothpaste is characterized in that in its component, containing by weight: calcium carbonate 40 ~ 50, sorbitol 15 ~ 25, carboxymethylated cellulose 0.2 ~ 1.5, guar gum 0.1 ~ 1, saccharin sodium 0 ~ 0.5, pure sodium sulfovinate 0.5 ~ 2.5, tetrasodium pyrophosphate 0 ~ 1, silica 1 ~ 5, methyl ester sodium 0 ~ 0.5, propylene glycol 1 ~ 3.5, deionized water 15 ~ 30, essence 0 ~ 0.8, Mentholum 0 ~ 1, Saussurea involucrata Kar. et Kir. et Maxim. extract 0.2 ~ 1.5, Ramulus et Folium Mussaendae Pubescentis extract 0.05 ~ 0.6, nano angelica root 0 ~ 0.6, nanometer halite 0 ~ 0.6; Its manufacture method is: earlier sorbitol is joined in the vacuum Manufacturing medicine extract machine, add carboxymethylated cellulose, guar gum, pure sodium sulfovinate, tetrasodium pyrophosphate, silicon dioxide, methyl ester sodium, the abundant mixing of propylene glycol again, add deionized water then; Mixing under the vacuum stirring state, adds the Saussurea involucrata Kar. et Kir. et Maxim. extract, Ramulus et Folium Mussaendae Pubescentis extract, nano angelica root, nanometer halite, saccharin sodium, calcium carbonate, the Mentholum that carry out dispersing and dissolving with deionized water successively once more; Under vacuum state; (20 ~ 6000rpm) stir abundant mixing, add essence at last, once more under vacuum state to carry out high speed; Carry out the fully emulsified mixing of high-speed stirred, promptly get product.
2. a kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste as claimed in claim 1; It is characterized in that described Saussurea involucrata Kar. et Kir. et Maxim. extract be the Saussurea involucrata Kar. et Kir. et Maxim. raw material through adding volume ratio is 85% alcohol reflux 2 times, each 1.5 ~ 2 h, merge extractive liquid; Filter, be condensed into relative density and be 1.25 ~ 1.30 extractum.
3. a kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste as claimed in claim 1 is characterized in that described Ramulus et Folium Mussaendae Pubescentis extract is the Ramulus et Folium Mussaendae Pubescentis extract juice that Ramulus et Folium Mussaendae Pubescentis obtains after supercritical carbon dioxide extraction method extracts, removes slag.
4. a kind of Saussurea involucrata Kar. et Kir. et Maxim. toothpaste as claimed in claim 1 is characterized in that described essence is Herba Menthae essence or jasmine flower essence or Flos Chrysanthemi Indici absolute oil or other plant essence or synthetic class essence.
CN2012102960340A 2012-08-20 2012-08-20 Tibetan saussurea toothpaste and preparation method thereof Pending CN102772340A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103462841A (en) * 2013-09-06 2013-12-25 广州立白企业集团有限公司 Toothpaste containing saussurea involucrate component
CN110169931A (en) * 2019-06-11 2019-08-27 青海通天河中藏药饮片有限公司 A kind of halite toothpaste and preparation method thereof

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CN102106802A (en) * 2011-02-22 2011-06-29 云南龙润茶业集团有限公司 Tea-salt toothpaste and preparation method thereof
CN102579305A (en) * 2012-03-29 2012-07-18 安徽两面针·芳草日化有限公司 Natural medicine toothpaste with saussurea involucrata as major material

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Publication number Priority date Publication date Assignee Title
CN102106802A (en) * 2011-02-22 2011-06-29 云南龙润茶业集团有限公司 Tea-salt toothpaste and preparation method thereof
CN102579305A (en) * 2012-03-29 2012-07-18 安徽两面针·芳草日化有限公司 Natural medicine toothpaste with saussurea involucrata as major material

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103462841A (en) * 2013-09-06 2013-12-25 广州立白企业集团有限公司 Toothpaste containing saussurea involucrate component
CN110169931A (en) * 2019-06-11 2019-08-27 青海通天河中藏药饮片有限公司 A kind of halite toothpaste and preparation method thereof

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Application publication date: 20121114