Hsu, 2011 - Google Patents

Coupling Mass Spectrometry with Liquid Chromatography (LC-MS) for Hydrocarbon Research

Hsu, 2011

View PDF
Document ID
6360201572874430743
Author
Hsu C
Publication year
Publication venue
Analytical Advances for Hydrocarbon Research

External Links

Snippet

Petroleum and other fossil fuels, such as coals and shale oils, are complex hydrocarbon mixtures that contain thousands of components. 1 Numerous analytical techniques have been developed to characterize bulk properties and composition of petroleum and its …
Continue reading at www.academia.edu (PDF) (other versions)

Classifications

    • H—ELECTRICITY
    • H01—BASIC ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometer or separator tubes
    • H01J49/02—Details
    • H01J49/10—Ion sources; Ion guns
    • H01J49/16—Ion sources; Ion guns using surface ionisation, e.g. field-, thermionic- or photo-emission
    • H01J49/165—Electrospray ionisation
    • H—ELECTRICITY
    • H01—BASIC ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometer or separator tubes
    • H01J49/02—Details
    • H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/72—Mass spectrometers
    • H—ELECTRICITY
    • H01—BASIC ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometer or separator tubes
    • H01J49/02—Details
    • H01J49/10—Ion sources; Ion guns
    • H01J49/107—Arrangements for using several ion sources
    • H—ELECTRICITY
    • H01—BASIC ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometer or separator tubes
    • H01J49/02—Details
    • H01J49/06—Electron- or ion-optical arrangements
    • H01J49/062—Ion guides
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
    • H—ELECTRICITY
    • H01—BASIC ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometer or separator tubes
    • H01J49/26—Mass spectrometers or separator tubes
    • H01J49/34—Dynamic spectrometers
    • H01J49/42—Stability-of-path spectrometers, e.g. monopole, quadrupole, multipole, farvitrons
    • H—ELECTRICITY
    • H01—BASIC ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometer or separator tubes
    • H01J49/004—Combinations of spectrometers, tandem spectrometers, e.g. MS/MS, MSn
    • H01J49/0045—Combinations of spectrometers, tandem spectrometers, e.g. MS/MS, MSn characterised by the fragmentation or other specific reaction
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00—Investigating or analysing materials by the use of electric, electro-chemical, or magnetic means
    • G01N27/62—Investigating or analysing materials by the use of electric, electro-chemical, or magnetic means by investigating the ionisation of gases; by investigating electric discharges, e.g. emission of cathode
    • G01N27/622—Investigating or analysing materials by the use of electric, electro-chemical, or magnetic means by investigating the ionisation of gases; by investigating electric discharges, e.g. emission of cathode separating and identifying ionized molecules based on their mobility in a carrier gas, i.e. ion mobility spectrometry

Similar Documents

Publication Publication Date Title
Han et al. Molecular characterization of sulfur-containing compounds in petroleum
Niyonsaba et al. Recent advances in petroleum analysis by mass spectrometry
JP6166661B2 (en) Formation of petroleum composition models by high resolution mass spectrometry and related analyses.
Rodgers et al. Combating selective ionization in the high resolution mass spectral characterization of complex mixtures
Cho et al. Developments in FT‐ICR MS instrumentation, ionization techniques, and data interpretation methods for petroleomics
Kim et al. Improved abundance sensitivity of molecular ions in positive-ion APCI MS analysis of petroleum in toluene
JP2016503884A (en) Characterization of petroleum saturates using MALDI and FT ion cyclotron resonance mass spectrometry
Giraldo-Dávila et al. Selective ionization by electron-transfer MALDI-MS of vanadyl porphyrins from crude oils
Leyva et al. Understanding the structural complexity of dissolved organic matter: isomeric diversity
Schaub et al. Speciation of aromatic compounds in petroleum refinery streams by continuous flow field desorption ionization FT-ICR mass spectrometry
Chacon-Patino et al. Lessons learned from a decade-long assessment of asphaltenes by ultrahigh-resolution mass spectrometry and implications for complex mixture analysis
EP2936134B1 (en) Analysis of hydrocarbon solid samples
Carvalho et al. Revealing the chemical characterization of asphaltenes fractions produced by N-methylpyrrolidone using FTIR, molecular fluorescence, 1H NMR, and ESI (±) FT-ICR MS
Hsu et al. On-line liquid chromatography/mass spectrometry for heavy hydrocarbon characterization
Hsu et al. High-boiling aromatic hydrocarbons characterized by liquid chromatography-thermospray-mass spectrometry
Bojkovic et al. Analytics driving kinetics: advanced mass spectrometric characterization of petroleum products
Yerabolu et al. Molecular profiling of crude oil by using Distillation Precipitation Fractionation Mass Spectrometry (DPF-MS)
Hsu Coupling Mass Spectrometry with Liquid Chromatography (LC-MS) for Hydrocarbon Research
Pereira et al. Fourier transform mass spectrometry applied to petroleomics
US20220208539A1 (en) Method and apparatus for mass spectrometry
Herod Limitations of mass spectrometric methods for the characterization of polydisperse materials
de Vos et al. Detection of petrol (gasoline) in fire debris by gas chromatography/mass spectrometry/mass spectrometry (GC/MS/MS)
Wang et al. Identification of Artifacts in the Methylation Process of Sulfur Compounds in Petroleum
Mansoori Isomeric identification and quantification of polycyclic aromatic hydrocarbons in environmental samples by liquid chromatography tandem mass spectrometry using a high pressure quadrupole collision cell
Borisov et al. 2.4 Analysis of Heavy Crude Oil and Its Refined Products by Various Chromatographic and Mass Spectrometry Methods