Liang et al., 2004 - Google Patents
Peralkylated-β-cyclodextrin used as gas chromatographic stationary phase prepared by sol–gel technology for capillary columnLiang et al., 2004
- Document ID
- 18060484550944580786
- Author
- Liang M
- Qi M
- Zhang C
- Fu R
- Publication year
- Publication venue
- Journal of Chromatography A
External Links
Snippet
For the first time, three peralkylated-β-cyclodextrins (β-CD), permethylated-β-CD, perethylated-β-CD and perpentylated-β-CD, were coated onto the fused-silica capillary by sol–gel method with simplicity and rapidity. Multiple steps in conventional column …
- 210000001736 Capillaries 0 title abstract description 33
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/60—Construction of the column
- G01N30/6052—Construction of the column body
- G01N30/6073—Construction of the column body in open tubular form
- G01N30/6078—Capillaries
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/60—Construction of the column
- G01N30/6004—Construction of the column end pieces
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/60—Construction of the column
- G01N30/6034—Construction of the column joining multiple columns
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N2030/022—Column chromatography characterised by the kind of separation mechanism
- G01N2030/025—Gas chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8665—Signal analysis for calibrating the measuring apparatus
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
- G01N30/94—Development
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Liu et al. | Preparation of stir bars for sorptive extraction using sol–gel technology | |
US8685240B2 (en) | High efficiency sol-gel gas chromatography column | |
Miyamoto et al. | High-efficiency liquid chromatographic separation utilizing long monolithic silica capillary columns | |
Kotoni et al. | Introducing enantioselective ultrahigh-pressure liquid chromatography (eUHPLC): theoretical inspections and ultrafast separations on a new sub-2-μm Whelk-O1 stationary phase | |
Gritti et al. | Measurement of the eddy diffusion term in chromatographic columns. I. Application to the first generation of 4.6 mm ID monolithic columns | |
Serrano et al. | Assessing the reliability of wall-coated microfabricated gas chromatographic separation columns | |
Shende et al. | Sol− gel poly (ethylene glycol) stationary phase for high-resolution capillary gas chromatography | |
LaCourse | Column liquid chromatography: equipment and instrumentation | |
Dewoolkar et al. | Amine gradient stationary phases on in-house built monolithic columns for liquid chromatography | |
Chankvetadze et al. | Very fast enantioseparation in high-performance liquid chromatography using cellulose tris (3, 5-dimethylphenylcarbamate) coated on monolithic silica support | |
Dores‐Sousa et al. | Resolving power in liquid chromatography: A trade‐off between efficiency and analysis time | |
Jiang et al. | Sol‐gel technique for the preparation of β‐cyclodextrin gold nanoparticles as chiral stationary phase in open‐tubular capillary electrochromatography | |
Liang et al. | Peralkylated-β-cyclodextrin used as gas chromatographic stationary phase prepared by sol–gel technology for capillary column | |
Jespers et al. | Chip-based multicapillary column with maximal interconnectivity to combine maximum efficiency and maximum loadability | |
Folprechtová et al. | The degree of substitution affects the enantioselectivity of sulfobutylether‐β‐cyclodextrin chiral stationary phases | |
Plachká et al. | Columns in analytical‐scale supercritical fluid chromatography: From traditional to unconventional chemistries | |
Gholizadeh et al. | Ionic liquid stationary phase coating optimization for semi-packed microfabricated columns | |
Lv et al. | Enantioselectivity of monolithic silica stationary phases immobilized with different concentrations cellulose tris (3, 5‐dimethylphenylcarbamate), analyzed with different mobile phases in capillary electrochromatography | |
Wang et al. | Dynamic evaluation of a trilobal capillary‐channeled polymer fiber shape for reversed phase protein separations and comparison to the eight‐channeled form | |
Wen et al. | Development of a compound-specific isotope analysis method for atmospheric formaldehyde and acetaldehyde | |
Liu et al. | Amylose‐3, 5‐dimethylphenylcarbamate immobilized on monolithic silica stationary phases for chiral separations in capillary electrochromatography | |
Rybka et al. | Single‐Molecule and Ensemble Diffusivities in Individual Nanopores with Spatially Dependent Mobility | |
Malsche et al. | Separations using a porous‐shell pillar array column on a capillary LC instrument | |
Meziani et al. | Evaluation of gas chromatography columns with radially elongated pillars as second-dimension columns in comprehensive two-dimensional gas chromatography | |
Leonard et al. | Programmable control of column selectivity for high-speed GC |