JPS577465A - Preparation of indole derivative - Google Patents
Preparation of indole derivativeInfo
- Publication number
- JPS577465A JPS577465A JP7912880A JP7912880A JPS577465A JP S577465 A JPS577465 A JP S577465A JP 7912880 A JP7912880 A JP 7912880A JP 7912880 A JP7912880 A JP 7912880A JP S577465 A JPS577465 A JP S577465A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- alkyl
- water
- basic substance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Indole Compounds (AREA)
Abstract
PURPOSE: To obtain the titled compound useful for the remedy and prevention of arrhythmia and atrial fibrillation by a simple and economical means in high purity and yield, by reacting 4-hydroxyindole with an oxazolidine derivative in the presence of water and a basic substance.
CONSTITUTION: A compound of formula I (Y is H or equivalent amount of a metallic atom) is reacted with an oxazolidine derivative of formula I (R is alkyl; X is halogen, alkyl or arylsulfonyloxy) in the presence of water and a basic substance, e.g. potassium hydroxide, in a solvent, e.g. dimethylformamide, preferably at 50W 150°C, to give a compound of formula III. The compound of formula II is synthesized by alkylating the nitrogen atom at the 3-position of a 5-halogenomethyloxazolidin-2- one with an alkyl halide.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP7912880A JPS577465A (en) | 1980-06-13 | 1980-06-13 | Preparation of indole derivative |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP7912880A JPS577465A (en) | 1980-06-13 | 1980-06-13 | Preparation of indole derivative |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS577465A true JPS577465A (en) | 1982-01-14 |
Family
ID=13681298
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP7912880A Pending JPS577465A (en) | 1980-06-13 | 1980-06-13 | Preparation of indole derivative |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS577465A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2366431A1 (en) * | 2010-03-19 | 2011-09-21 | Universitätsklinikum Hamburg-Eppendorf | Myeloperoxidase as a target in atrial fibrillation |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS53119824A (en) * | 1977-03-24 | 1978-10-19 | Sandoz Ag | Improvement in organic compound |
JPS5622765A (en) * | 1979-08-02 | 1981-03-03 | Fujimoto Seiyaku Kk | Novel method of preparing pindolol |
JPS5683471A (en) * | 1979-12-10 | 1981-07-08 | Fujimoto Seiyaku Kk | Novel preparation of pindolol |
-
1980
- 1980-06-13 JP JP7912880A patent/JPS577465A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS53119824A (en) * | 1977-03-24 | 1978-10-19 | Sandoz Ag | Improvement in organic compound |
JPS5622765A (en) * | 1979-08-02 | 1981-03-03 | Fujimoto Seiyaku Kk | Novel method of preparing pindolol |
JPS5683471A (en) * | 1979-12-10 | 1981-07-08 | Fujimoto Seiyaku Kk | Novel preparation of pindolol |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2366431A1 (en) * | 2010-03-19 | 2011-09-21 | Universitätsklinikum Hamburg-Eppendorf | Myeloperoxidase as a target in atrial fibrillation |
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