JPH01139140A - Drying agent for pressed flower and production of pressed flowers - Google Patents
Drying agent for pressed flower and production of pressed flowersInfo
- Publication number
- JPH01139140A JPH01139140A JP29686787A JP29686787A JPH01139140A JP H01139140 A JPH01139140 A JP H01139140A JP 29686787 A JP29686787 A JP 29686787A JP 29686787 A JP29686787 A JP 29686787A JP H01139140 A JPH01139140 A JP H01139140A
- Authority
- JP
- Japan
- Prior art keywords
- flowers
- drying
- pressed
- magnesium sulfate
- pressed flowers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002274 desiccant Substances 0.000 title claims abstract description 18
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims abstract description 57
- 238000001035 drying Methods 0.000 claims abstract description 34
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims abstract description 28
- 235000019341 magnesium sulphate Nutrition 0.000 claims abstract description 28
- 239000004480 active ingredient Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 19
- 238000002425 crystallisation Methods 0.000 abstract description 8
- 230000008025 crystallization Effects 0.000 abstract description 8
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 238000005562 fading Methods 0.000 abstract 2
- 238000004321 preservation Methods 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 description 8
- 238000000034 method Methods 0.000 description 6
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 4
- 239000001110 calcium chloride Substances 0.000 description 4
- 229910001628 calcium chloride Inorganic materials 0.000 description 4
- 238000002845 discoloration Methods 0.000 description 4
- 239000011777 magnesium Substances 0.000 description 3
- 241000723353 Chrysanthemum Species 0.000 description 2
- 235000007516 Chrysanthemum Nutrition 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 238000010981 drying operation Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- LPLLVINFLBSFRP-UHFFFAOYSA-N 2-methylamino-1-phenylpropan-1-one Chemical compound CNC(C)C(=O)C1=CC=CC=C1 LPLLVINFLBSFRP-UHFFFAOYSA-N 0.000 description 1
- 244000293323 Cosmos caudatus Species 0.000 description 1
- 235000005956 Cosmos caudatus Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 101100145155 Escherichia phage lambda cIII gene Proteins 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 241001533590 Junonia Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- VCUFZILGIRCDQQ-KRWDZBQOSA-N N-[[(5S)-2-oxo-3-(2-oxo-3H-1,3-benzoxazol-6-yl)-1,3-oxazolidin-5-yl]methyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C1O[C@H](CN1C1=CC2=C(NC(O2)=O)C=C1)CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F VCUFZILGIRCDQQ-KRWDZBQOSA-N 0.000 description 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
- 235000004031 Viola x wittrockiana Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003826 tablet Substances 0.000 description 1
Landscapes
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
【発明の詳細な説明】
産業上の利用分野
本発明は、押し花月乾燥剤及び押し花の乾燥方法に関す
る。本願明細書においては、押し花の材料となる“草花
“とは、植物の葉、花、花びら等のいわゆる押し花乃至
押し葉の対象となる全ての部分を包含する。また、特許
請求の範囲第3項における“一次乾燥“とは、脱水乾燥
操作を意味し、特許請求の範囲第2項における“乾燥”
及び特許請求の範囲第3項における“二次乾燥“とは、
脱水乾燥操作のみならず、乾燥状態を維持するための操
作をも意味する。DETAILED DESCRIPTION OF THE INVENTION Field of the Invention The present invention relates to a pressed flower desiccant and a method for drying pressed flowers. In the present specification, the term "flowers" used as materials for pressed flowers includes all parts of plants such as leaves, flowers, petals, etc. that are the objects of so-called pressed flowers or pressed leaves. Furthermore, "primary drying" in claim 3 means a dehydration drying operation, and "drying" in claim 2 means
and “secondary drying” in claim 3,
This refers not only to dehydration and drying operations, but also to operations for maintaining a dry state.
従来技術とその問題点
押し花の製造方法としては、古来から、雑誌、本、新聞
紙等の紙葉の間に草花を挾み入れて長期間放置し、乾燥
させる方法が知られている。しかしながら、この方法に
は、押し花の退色が著しく、得られる押し花の色合いが
一定せず、また紙葉からのインキ移りがある等の欠点が
ある。BACKGROUND OF THE INVENTION As a method for producing pressed flowers, it has been known since ancient times to sandwich flowers between sheets of paper such as magazines, books, newspapers, etc. and leave them to dry for a long period of time. However, this method has drawbacks such as significant discoloration of the pressed flowers, uneven hue of the obtained pressed flowers, and ink transfer from the paper sheets.
近年、吸湿性の紙、或いはシリカゲル、塩化カルシウム
等の吸湿性の強い化学物質を使用する押し花の製造が行
われるようになってきた。しかしながら、紙、シリカゲ
ル等は、吸湿能力、特に初期吸湿能力が低いため、乾燥
期間が長くなり、その結果、退色を生じやすく、押し花
の色合いも一定しないという問題点がある。塩化カルシ
ウムは、吸湿能力には優れているが、吸湿が過度に進行
した場合には、潮解し始める。そして、吸湿水分量が7
0重量%を超えると、水滴を発生させて、管理に1・分
留窓しない場合には、反って乾燥した押し花に多量の水
分を与える場合がある。しかも、塩化カルシウムは、僅
かに発生する塩化水素により、押し花を著しく脱色乃至
退色させるのも、大きな欠点である。In recent years, pressed flowers have been manufactured using hygroscopic paper or highly hygroscopic chemical substances such as silica gel and calcium chloride. However, paper, silica gel, and the like have a low moisture absorption capacity, particularly a low initial moisture absorption capacity, resulting in a long drying period, resulting in easy discoloration and uneven coloration of pressed flowers. Calcium chloride has excellent moisture absorption ability, but if moisture absorption progresses excessively, it begins to deliquesce. And the moisture absorption amount is 7
If it exceeds 0% by weight, water droplets may be generated, and if a fractionation window is not used for management, a large amount of water may be applied to the pressed flowers that have warped and dried. Moreover, calcium chloride has a major drawback in that the small amount of hydrogen chloride generated causes the pressed flowers to noticeably bleach or discolor.
問題点を解決するための手段
本発明者は、上記の如き技術の現況に鑑みて種々研究を
重ねた結果、特定の含水硫酸マグネシウムが、押し花月
の乾燥剤として極めて有用であることを見出した。Means for Solving the Problems The present inventor has conducted various studies in view of the current state of technology as described above, and has discovered that a specific hydrated magnesium sulfate is extremely useful as a desiccant for pressed flower moons. .
即ち、本発明は、下記の如き押し花月の乾燥剤及び押し
花の乾燥方法を提供するものである2OM・nH2O(
0≦n≦5)で表される硫酸マグネシウムを有効成分と
する押し花月乾燥剤;
■Mg5O・n1HO(2≦n1≦5)で表される硫酸
マグネシウムにより草花の乾燥を行なうことを特徴とす
る押し花製造方法;
■Mg5O・n1H2O(2≦n1≦5)で表される硫
酸マグネシウムにより草花の一次乾燥を行った後、Mg
SO4・n2H2O(0≦n2≦3、但しn2くnl)
で表される硫酸マグネシウムにより該一次乾燥を終えた
草花の二次乾燥を行なうことを特徴とする押し花の乾燥
方法。That is, the present invention provides a desiccant for pressed flowers and a method for drying pressed flowers as described below.
Pressed flower moon desiccant containing magnesium sulfate expressed as 0≦n≦5) as an active ingredient; ■Characterized by drying flowers with magnesium sulfate expressed as Mg5O・n1HO (2≦n1≦5) Pressed flower production method; ■After primary drying of flowers with magnesium sulfate represented by Mg5O・n1H2O (2≦n1≦5), Mg
SO4・n2H2O (0≦n2≦3, however, n2 x nl)
A method for drying pressed flowers, which comprises performing secondary drying of the flowers after the primary drying using magnesium sulfate represented by:
本発明で押し花月乾燥剤として使用する硫酸マグネシウ
ムは、弐Mg5O・nH2O(但し、0≦n≦5)で表
されるものである。The magnesium sulfate used as the pressed flower moon desiccant in the present invention is represented by 2Mg5O.nH2O (0≦n≦5).
本発明による押し花乾燥方法においては、まず、M・n
HO(2≦n1≦5)で表さ■■
れる結晶水量の多い硫酸マグネシウムにより草花の一次
乾燥を行なう。通常、この一次乾燥用の硫酸マグネシウ
ムは、水溶液の状態で紙(和紙、洋紙)、布、発泡プラ
スチックシート等に含浸させ、乾燥させた状態で使用す
る。より詳細には、この様な含浸材間に草花を挾み入れ
、荷重下又は荷重を加えることなく、保持する。このよ
うな実施態様による一次乾燥に要する日数は、草花の種
類、気温、湿度、加圧の程度等により異なるが、通常夏
朋で2〜3日程度、冬期で3〜5日程度である。In the pressed flower drying method according to the present invention, first, M.n.
Primary drying of flowers is carried out using magnesium sulfate which has a large amount of crystallized water expressed as HO (2≦n1≦5). Usually, magnesium sulfate for primary drying is impregnated into paper (Japanese paper, Western paper), cloth, foamed plastic sheet, etc. in the form of an aqueous solution, and used after being dried. More specifically, flowers are sandwiched between such impregnated materials and held under or without load. The number of days required for primary drying in this embodiment varies depending on the type of flower, temperature, humidity, degree of pressure, etc., but is usually about 2 to 3 days in summer and 3 to 5 days in winter.
シートに対する硫酸マグネシウムの含浸量は、通常Mg
50 ・3H2として、30〜50g/耐程度である
。尚、一次乾燥剤は、粉末、顆粒、錠剤等の形態でも使
用可能である。一次乾燥に際し、上記の式においてnl
が2未満の無水乃至低結晶水量の硫酸マグネシウムを使
用する場合には、乾燥が急速に進行し過ぎて、押し花が
退色して、その色調が損なわれることがある。The amount of magnesium sulfate impregnated into the sheet is usually Mg
50・3H2, it is about 30 to 50 g/proof. Note that the primary desiccant can also be used in the form of powder, granules, tablets, and the like. During primary drying, nl in the above formula
If magnesium sulfate is anhydrous or has a low crystallization water content of less than 2, drying may proceed too rapidly and the pressed flowers may fade and lose their color tone.
上記の一次乾燥により、そのまま乾燥押し花として製品
化されるものもあるが、草花の種類によっては、更に乾
燥を必要とする場合もある。この様な場合には、M・n
2HO
(0≦n2≦3、但しn2<n’ )で示される無水乃
至比較的低結晶水量の硫酸マグネシウムを乾燥剤として
引き続き二次乾燥を行う。二次乾燥に際しては、該硫酸
マグネシウムを紙性、有性等の袋に入れ、密閉空間内で
一次乾燥された草花の乾燥を行えば良い。或いは、一次
乾燥の場合と同様に、硫酸マグネシウム含浸シートを使
用しても良い。二次乾燥に際し、上記の式においてn2
が3を1−回る高結晶水量の硫酸マグネシウムを使用す
る場合には、乾燥の進行が緩やかで、長時間を必要とす
るので、経済的に不利である。After the above-mentioned primary drying, some flowers can be directly produced as dried pressed flowers, but depending on the type of flower, further drying may be required. In such a case, M・n
Secondary drying is then performed using anhydrous or relatively low amount of crystallized water magnesium sulfate represented by 2HO (0≦n2≦3, where n2<n') as a drying agent. For secondary drying, the magnesium sulfate may be placed in a paper bag, plastic bag, etc., and the primary dried flowers may be dried in a closed space. Alternatively, a magnesium sulfate-impregnated sheet may be used as in the case of primary drying. During secondary drying, in the above formula, n2
When using magnesium sulfate with a high amount of water of crystallization (1 - 3 times), drying progresses slowly and requires a long time, which is economically disadvantageous.
ちなみに、第1図に本発明で使用する硫酸マグネシウム
の結晶水と吸水能との関係を示す。試験時の温度は、2
5℃、相対湿度は、90%である。Incidentally, FIG. 1 shows the relationship between water of crystallization and water absorption capacity of magnesium sulfate used in the present invention. The temperature during the test was 2
5° C. and relative humidity 90%.
グラフの縦軸は、硫酸マグネシウム重量当たりの吸水量
を示す。本発明は、このような吸水量の差を効果的に利
用するものである。The vertical axis of the graph indicates the amount of water absorbed per weight of magnesium sulfate. The present invention effectively utilizes such a difference in water absorption amount.
なお、本発明で使用することにより吸湿湿潤した乾燥剤
は、電気アイロン、電子レンジ等の任意の加熱手段によ
り、容易に加熱脱水され、再生される。また、本発明方
法により得られた押し花は、品質(色調等)が安定して
いるので、無水硫酸マグネシウムを充填又は担持した乾
燥剤シート上で長期間保存することができる。Note that the desiccant that has absorbed moisture and become moist when used in the present invention is easily heated and dehydrated by any heating means such as an electric iron or a microwave oven, and then regenerated. Moreover, since the pressed flowers obtained by the method of the present invention have stable quality (color tone, etc.), they can be stored for a long period of time on a desiccant sheet filled with or supported with anhydrous magnesium sulfate.
発明の効果 本発明によれば、以下の如き顕著な効果が達成される。Effect of the invention According to the present invention, the following remarkable effects are achieved.
(1)乾燥進行中の押し花の退色が最少限に押さえられ
る。また、塩化カルシウムを使用する場合に認められる
著るしい退色も、生じない。(1) Discoloration of pressed flowers during drying can be minimized. Also, the significant discoloration observed when using calcium chloride does not occur.
(2)従って、得られる押し花の色調が優れている。特
に、緑色の鮮やかさは、従来法による製品に比して、際
立っている。(2) Therefore, the color tone of the obtained pressed flowers is excellent. In particular, the vividness of the green color is outstanding compared to products produced by conventional methods.
(3)乾燥剤として使用する特定結晶水量の硫酸マグネ
シウムは、乾燥保持状態において、微小曾の水分を放出
するものと推測される。この僅かの水分放出も、乾燥終
了後の押し花の優れた色調維持に貢献しているものと思
われる。(3) Magnesium sulfate with a specific amount of crystallization water used as a desiccant is presumed to release very small amounts of water when kept dry. This small amount of moisture release also seems to contribute to maintaining the excellent color tone of the pressed flowers after drying.
(4)本発明乾燥剤は、吸水飽和状態においても、潮解
若しくは水分による“べとつき”を生じないので、取扱
が容易である。(4) The desiccant of the present invention is easy to handle because it does not deliquesce or become "sticky" due to water even when saturated with water.
(5)乾燥剤自体は、加熱により容易に脱水され、再使
用可能となる。(5) The desiccant itself is easily dehydrated by heating and can be reused.
(6)対象とする草花の種類等に応じて、一次乾燥剤と
二次乾燥剤の結晶水量を適宜選択して組み合わせること
により、最適条件下に押し花を製造することができる。(6) Pressed flowers can be produced under optimal conditions by appropriately selecting and combining the amounts of crystallization water in the primary desiccant and secondary desiccant depending on the type of target flower.
実施例
以下実施例を示し、本発明の特徴とするところをより一
層明確にする。EXAMPLES Examples will be shown below to further clarify the features of the present invention.
実施例1
硫酸マグネシウム(M g S Oa ・3H2O)を
3浸した乾燥紙(含浸量的40g/cI#、以下乾燥シ
ートという)を10枚重ねて綴り和紙で包んだ後、その
−ヒに草花(小菊)を置き、ポリウレタンマットを被せ
、更に乾燥シートを置くという手順を繰り返すことによ
り、多段の積み重ねを行った。Example 1 10 sheets of dry paper soaked with magnesium sulfate (MgS Oa ・3H2O) (impregnated amount: 40 g/cI#, hereinafter referred to as dry sheet) were stacked and wrapped in Japanese paper, and then flowers were placed on top of them. By repeating the procedure of placing a small chrysanthemum (small chrysanthemum), covering it with a polyurethane mat, and then placing a drying sheet, multiple layers were stacked.
これらを防湿用塩化ビニル樹脂シートで包んだ後、上下
に押し板を当て、紐で締め付け、約10kg/cIII
の荷重を掛け、3日間保持した。After wrapping these with a moisture-proof vinyl chloride resin sheet, press plates are placed on the top and bottom, and tightened with strings. Approximately 10 kg/cIII
A load was applied and maintained for 3 days.
かくして、緑色の鮮やかな押し花が得られた。In this way, bright green pressed flowers were obtained.
更に、パンジー及びコスモスを同様にして乾燥処理した
ところ、鮮やかな色調の押し花が得られた。Furthermore, when pansies and cosmos were dried in the same manner, pressed flowers with bright colors were obtained.
第1図は、本発明で使用する硫酸マグネシウムの結晶水
と吸水能との関係を示すグラフである。
(以上)FIG. 1 is a graph showing the relationship between water of crystallization and water absorption capacity of magnesium sulfate used in the present invention. (that's all)
Claims (3)
れる硫酸マグネシウムを有効成分とする押し花用乾燥剤
。(1) A desiccant for pressed flowers containing magnesium sulfate represented by MgSO_4·nH_2O (0≦n≦5) as an active ingredient.
)で表される硫酸マグネシウムにより草花の乾燥を行な
うことを特徴とする押し花製造方法。(2) MgSO_4・n^1H_2O (2≦n^1≦5
) A method for producing pressed flowers characterized by drying flowers using magnesium sulfate.
)で表される硫酸マグネシウムにより草花の一次乾燥を
行った後、MgSO_4・n^2H_2O(0≦n^2
≦3、但しn^2<n^1)で表される硫酸マグネシウ
ムにより該一次乾燥を終えた草花の二次乾燥を行なうこ
とを特徴とする押し花製造方法。(3) MgSO_4・n^1H_2O (2≦n^1≦5
) After primary drying of flowers with magnesium sulfate, MgSO_4・n^2H_2O (0≦n^2
≦3, provided that n^2<n^1) A method for producing pressed flowers, which comprises performing secondary drying of the flowers after the primary drying using magnesium sulfate.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP29686787A JPH01139140A (en) | 1987-11-25 | 1987-11-25 | Drying agent for pressed flower and production of pressed flowers |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP29686787A JPH01139140A (en) | 1987-11-25 | 1987-11-25 | Drying agent for pressed flower and production of pressed flowers |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH01139140A true JPH01139140A (en) | 1989-05-31 |
JPH0516298B2 JPH0516298B2 (en) | 1993-03-04 |
Family
ID=17839189
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP29686787A Granted JPH01139140A (en) | 1987-11-25 | 1987-11-25 | Drying agent for pressed flower and production of pressed flowers |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH01139140A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2096532A1 (en) * | 1995-07-27 | 1997-03-01 | Perez Juana Maria Collantes | Process for drying flowers |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60109501A (en) * | 1983-11-16 | 1985-06-15 | Toshiyuki Sugino | Method for direct manufacturing of pressed flower |
JPS62136683A (en) * | 1985-12-10 | 1987-06-19 | 安斉 清 | Preservation of pressed flower |
-
1987
- 1987-11-25 JP JP29686787A patent/JPH01139140A/en active Granted
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60109501A (en) * | 1983-11-16 | 1985-06-15 | Toshiyuki Sugino | Method for direct manufacturing of pressed flower |
JPS62136683A (en) * | 1985-12-10 | 1987-06-19 | 安斉 清 | Preservation of pressed flower |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2096532A1 (en) * | 1995-07-27 | 1997-03-01 | Perez Juana Maria Collantes | Process for drying flowers |
Also Published As
Publication number | Publication date |
---|---|
JPH0516298B2 (en) | 1993-03-04 |
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