JP2007323052A - Composite tooth for dental arch model, and method of producing the same and application thereof - Google Patents
Composite tooth for dental arch model, and method of producing the same and application thereof Download PDFInfo
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Abstract
Description
本発明は、歯科医師を目指す学生が、口腔内作業を体験し、治療の練習をする顎歯模型用に用いる歯牙である。具体的には支台歯形成、窩洞形成等の形体付与を体験する為に用いる歯牙の製造方法に関する。 The present invention is a tooth used for a jaw model in which a student aiming at a dentist experiences intraoral work and practice treatment. Specifically, the present invention relates to a method for manufacturing a tooth used for experiencing formation of abutments, formation of a cavity, and the like.
口腔内治療練習用の顎歯模型用の歯牙は、エポキシ樹脂、メラミン樹脂で製造されることが多く、一般に普及している。
しかし、エポキシ樹脂、メラミン樹脂では切削感が異なることから支台歯形成や窩洞形成の練習をしても実際の口腔内での作業をした場合では異なる切削感、作業性から当惑する事が多かった。具体的には、天然歯は硬いために思った様に切削できない傾向にあり、更にデンチン部分は硬いが、エナメル部分は更に硬い構造となっている為、エポキシ樹脂、メラミン樹脂は軟らかく切削を多くしてしまう傾向にある。その結果、強く削ってしまい、上手く形体を作れないことも発生する可能性がある。
Teeth for a jaw and tooth model for intraoral treatment practice are often made of epoxy resin and melamine resin, and are widely used.
However, since epoxy resin and melamine resin have different cutting feelings, even when practicing abutment tooth formation and cavity formation, it is often embarrassed by the different cutting feeling and workability when working in the actual oral cavity. It was. Specifically, natural teeth tend to be hard to cut as expected, and the dentin part is harder, but the enamel part is harder, so the epoxy resin and melamine resin are softer and more cut. It tends to end up. As a result, there is a possibility that it will be sharply cut and the shape cannot be made well.
もう少し、硬い材料を求められた結果、コンポジットタイプのものが市販されている。コンポジットタイプの歯牙であっても、デンチン部分とエナメル部分が同一の切削感であるから、天然歯と切削感が異なり、支台歯形成や窩洞形成の練習をしても実際の口腔内での作業をした場合では異なる切削感、作業性から当惑する事が多かった。分かりやすい表現では滑る感覚があり、天然歯とは大きく違う切削感である。
特開平5−224591には、天然歯と極めて類似した切削性を有し、歯科教育切削実習用として好適な歯牙模型を提供することが示されている。主要構成成分として、無機物粉体と架橋型樹脂とを、重量比で20%対80%乃至70%対30%の割合で含有している。
As a result of a demand for a harder material, a composite type is commercially available. Even in composite type teeth, the dentin part and enamel part have the same cutting feeling, so the cutting feeling is different from natural teeth, and even if you practice abutment tooth formation and cavity formation, When working, it was often embarrassed by the different cutting feeling and workability. The easy-to-understand expression has a feeling of slipping, and the cutting feeling is very different from natural teeth.
Japanese Patent Application Laid-Open No. 5-224591 shows that a tooth model having cutting ability very similar to natural teeth and suitable for dental education cutting practice is provided. As main constituent components, inorganic powder and cross-linked resin are contained in a weight ratio of 20% to 80% to 70% to 30%.
本発明の歯牙模型を構成する無機物粉体としては、例えば、アルミナ、ジルコニア、チタニア、シリカ、等々が紹介され、上記化合物に限定されるものではなく、各種の無機物粉体を用いることができる。
しかし、天然歯と切削感が異なることから支台歯形成や窩洞形成の練習をしても実際の口腔内での作業をした場合では異なる切削感、作業性から当惑する事が多かった。また、無機物粉末体の開示のみである。特に天然歯独特の粘り気を有する歯牙を求める要望があり、また、エナメル部分とデンチン部分の切削性の違いを示せる歯牙模型ではなかった。
As the inorganic powder constituting the tooth model of the present invention, for example, alumina, zirconia, titania, silica and the like are introduced, and the inorganic powder is not limited to the above compounds, and various inorganic powders can be used.
However, since the cutting feeling is different from that of natural teeth, even when practicing abutment tooth formation and cavity formation, when working in the actual oral cavity, it was often embarrassed by the different cutting feeling and workability. Moreover, only an inorganic powder body is disclosed. In particular, there has been a demand for a tooth having a stickiness peculiar to natural teeth, and it was not a tooth model that could show a difference in machinability between an enamel part and a dentin part.
実開平1‐90068には、エナメル質層に金雲母結晶[NaMg3(Si3AlO10)F2]およびリチア・アルミナ・シリカ系結晶(Li2O・Al2O3・2SiO2,Li2O・Al2O3・4SiO2)が同時に析出したビッカース硬さ350〜450に制御されたガラス・セラミックスから構成され、歯根層には、ポリオール(主剤)に白色・赤色および黄色の着色剤を加え、さらにイソシアネートプレポリマー(硬化剤)を混入してシリコーンゴム母型に真空下で注入して、常温で硬化させ事前に準備をし、エナメル質層と歯根層との間に介在し、両者を合着している象牙質認識層はオペーク色を呈した接着性レジンで形成されていることが示している。 In Japanese Utility Model Laid-Open No. 1-90068, Vickers hardness in which phlogopite crystal [NaMg3 (Si3AlO10) F2] and lithia / alumina / silica-based crystal (Li2O.Al2O3.2SiO2, Li2O.Al2O3.4SiO2) are simultaneously precipitated on the enamel layer. It is composed of glass and ceramics controlled to 350-450, and the root layer is added with white, red and yellow colorants in the polyol (main agent), and further mixed with an isocyanate prepolymer (curing agent) to form a silicone rubber base. The dentin recognition layer, which is injected into the mold under vacuum, hardened at room temperature and prepared in advance, is interposed between the enamel layer and the root layer, and is bonded together, has an opaque color. It is shown that it is formed with a sex resin.
しかしながら、エナメル質層が金雲母結晶やリチア・アルミナ・シリカ系結晶にて構成されたものでは天然歯に比べ、切削感が硬すぎるため使用に耐える物ではなく、更に象牙質認識層は接着性レジンで形成されている為、接着剤の切削感が柔らかすぎる為、使用に耐える物ではなかった。 However, when the enamel layer is composed of phlogopite crystals or lithia / alumina / silica crystals, the cutting feeling is too hard compared to natural teeth, so it is not durable and the dentin recognition layer is adhesive. Since it was made of resin, the cutting feeling of the adhesive was too soft, so it was not durable.
特開平5−216395には、天然歯と極めて類似した切削性を有し、歯科教育切削実習用として好適な歯牙模型及びその製造方法を提供することが紹介されている。歯牙模型の主要構成成分として、気孔率が40〜80%のヒドロキシアパタイト粉末と、(メタ)アクリル酸エステル系樹脂とを、重量比で20%対80%乃至50%対50%の割合で含有しているものである。
従来の歯牙模型は、切削性において満足できる状況にない。従って、天然歯と切削性において類似する歯牙模型の開発が望まれていることが示されているものの、十分な切削感を示すものではなかった。特に天然歯独特の粘り気を有する歯牙を求める要望があり、また、エナメル部分とデンチン部分の切削性の違いを示せる歯牙模型ではなかった。
Japanese Patent Application Laid-Open No. 5-216395 introduces the provision of a tooth model having a cutting ability very similar to that of a natural tooth and suitable for dental education cutting practice and a manufacturing method thereof. Contains hydroxyapatite powder with porosity of 40-80% and (meth) acrylic ester resin as a major component of the tooth model in a weight ratio of 20% to 80% to 50% to 50% It is what you are doing.
Conventional tooth models are not in a satisfactory state in terms of machinability. Therefore, although it has been shown that development of a tooth model similar to natural teeth in machinability is desired, it does not show sufficient cutting feeling. In particular, there is a demand for a tooth having a stickiness peculiar to natural teeth, and it is not a tooth model that can show a difference in machinability between an enamel part and a dentin part.
特開平5−224591には、歯科医学生の歯周疾患治療実習に最適に用いることができる歯牙模型を提供する。構成として歯牙模型は、歯冠部の少なくとも表面がヌープ硬度70以上を有し、歯根部の少なくとも表面がヌープ硬度10〜40を有するものである。
本文中に「歯牙模型の作製法及び経済的な観点から如何なる硬度の素材、例えば金属、セラミクス、樹脂で形成されていてもよく、更には空洞であってもよい。」との記載があるが、切削感の観点から解決されていない。特に天然歯独特の粘り気を有する歯牙を求める要望があり、また、エナメル部分とデンチン部分の切削性の違いを示せる歯牙模型ではなかった。
特開平5−241498、特開平5−241499、特開平5−241500には、無機充填材の記載やハイドロキシアパタイト充填材の記載があるがいずれも樹脂を母材とするものであり、切削感の解決には至っていない。特に天然歯独特の粘り気を有する歯牙を求める要望があり、また、エナメル部分とデンチン部分の切削性の違いを示せる歯牙模型ではなかった。
JP-A-5-224591 provides a dental model that can be optimally used for a periodontal disease treatment practice of a dentist. As a constitution, at least the surface of the crown portion has a Knoop hardness of 70 or more, and at least the surface of the root portion has a Knoop hardness of 10 to 40.
In the text, there is a description that “it may be made of a material of any hardness, for example, metal, ceramics, resin, and may be a cavity from the viewpoint of the preparation method of the tooth model and economical viewpoint”. It has not been solved from the viewpoint of cutting feeling. In particular, there has been a demand for a tooth having a stickiness peculiar to natural teeth, and it was not a tooth model that could show a difference in machinability between an enamel part and a dentin part.
In JP-A-5-241498, JP-A-5-241499, and JP-A-5-241500, there are descriptions of inorganic fillers and hydroxyapatite fillers. It has not yet been resolved. In particular, there has been a demand for a tooth having a stickiness peculiar to natural teeth, and it was not a tooth model that could show a difference in machinability between an enamel part and a dentin part.
特開2004−94049には、レーザー光線を利用した正確な形状計測を可能とする歯科実習用模型歯を提供する発明が記載している。
明細書中には、「本発明の模型歯の歯冠部表面を構成する材料としては、一般的に公知のものを用いることが可能であり、例えば、セラミックス等の磁器あるいはアクリル、ポリスチレン、ポリカーボネート、アクリロニトリルスチレンブタジエン共重合体(ABS)、ポリプロピレン、ポリエチレン、ポリエステル等の熱可塑性樹脂材料や、メラミン、ユリア、不飽和ポリエステル、フェノール、エポキシ等の熱硬化性樹脂材料、さらには、これらの主原料にガラス繊維、カーボン繊維、パルプ、合成樹脂繊維等の有機、無機の各種強化繊維、タルク、シリカ、マイカ、炭酸カルシウム、硫酸バリウム、アルミナ等の各種充填材、顔料や染料等の着色剤、あるいは耐候剤や帯電防止剤等の各種添加剤を添加したものを用いることが出来る。」との記載があるが、好ましい材質の記載がなく、切削感を解決するものでは無かった。
Japanese Patent Application Laid-Open No. 2004-94049 describes an invention for providing a dental training model tooth that enables accurate shape measurement using a laser beam.
In the specification, “as the material constituting the surface of the crown portion of the model tooth of the present invention, generally known materials can be used. For example, ceramics or other porcelain or acrylic, polystyrene, polycarbonate , Thermoplastic resin materials such as acrylonitrile styrene butadiene copolymer (ABS), polypropylene, polyethylene and polyester, thermosetting resin materials such as melamine, urea, unsaturated polyester, phenol and epoxy, and their main raw materials Glass fiber, carbon fiber, pulp, synthetic resin fiber and other organic and inorganic reinforcing fibers, talc, silica, mica, calcium carbonate, barium sulfate, alumina and other fillers, pigments, dyes and other colorants, or What added various additives, such as a weathering agent and an antistatic agent, can be used. Is described with, but there is no description of the preferred material, it was not intended to resolve the grinding feel.
今までの開発では天然歯独特の粘り気を有する歯牙のエナメル部分とデンチン部分は開発されておらず、切削性の違いを示せる歯牙模型ではなかった。更にこの切削感を実現する為の具体的な組成としての開示がなく、それらの製造方法についても記載されていない。
顎歯模型はこれらの課題を抱えているにも関わらず、研究報告されているものは見当たらない。
In the development so far, the enamel part and dentin part of the tooth with the stickiness peculiar to natural teeth have not been developed, and it was not a tooth model that could show the difference in machinability. Furthermore, there is no disclosure as a specific composition for realizing this cutting feeling, and no description is given of a manufacturing method thereof.
Although the jaw model has these problems, no research report has been found.
従来の顎歯模型用歯牙は、天然歯形体をしているものの切削感が異なる。天然歯の切削感を体験するために、抜去歯を切削するなどの工夫は見られた。抜去歯は人体や動物からの材料であり衛生上の問題があり、衛生管理も十分に行なわないと感染の可能性があり、自由に練習を妨げられ感染予防を十分に行なわなければならなかった。また、天然生体であるため腐敗の問題があり、保存にも十分な注意が必要であった。
天然歯牙を用いずに歯牙の切削感を体験する方法が求められれていた。特に天然歯独特の粘り気を有する歯牙を求める要望があり、また、歯牙のエナメル部分からデンチン部分の切削感が変るところが求められており、当然にして、エナメル部分はエナメル質の切削感、デンチン部分はデンチン質の切削感が求められていたが、それを解決する方法は見つかっていなかった。
研究の結果、天然歯牙の切削感を出す為には無機系の焼成体を用いることが必要であり、それだけでは十分な切削感が得られない為に新たな工夫が必要であった。天然歯独特の粘り気を有する歯牙を求める要望があった。
Although the conventional tooth for jaw model has a natural tooth form, it has a different cutting feeling. In order to experience the cutting feeling of natural teeth, some ideas such as cutting extracted teeth were seen. The extracted tooth is a material from the human body and animals, and there are problems with hygiene. There is a possibility of infection if hygiene is not adequately controlled, and practice must be freely prevented to prevent infection. . Moreover, since it is a natural living body, there is a problem of spoilage, and sufficient caution is required for storage.
There has been a demand for a method for experiencing the cutting feeling of a tooth without using a natural tooth. In particular, there is a demand for a tooth having a stickiness peculiar to natural teeth, and there is a demand for a change in the cutting feeling of the dentin part from the enamel part of the tooth. Naturally, the enamel part has an enamel cutting feeling and a dentin part. Was demanded of a dentin-like cutting feeling, but no method was found to solve it.
As a result of research, it was necessary to use an inorganic calcined body in order to give a cutting feeling to natural teeth, and it was not possible to obtain a sufficient cutting feeling by itself. There has been a demand for a tooth having a stickiness unique to natural teeth.
天然歯独特の粘り気の切削感を表現する為には、数々の方法が試されてきたが、樹脂やコンポジット等々では十分な切削感を得ることができなかった。歯牙を切削した折に飛散する切削粉を軽減する方法を求められていた。 A number of methods have been tried to express the sticky cutting feeling unique to natural teeth, but sufficient cutting feeling cannot be obtained with resin, composites, and the like. There has been a demand for a method of reducing the cutting powder scattered in the folds of teeth.
本発明は治療練習用の顎歯模型用の歯牙であって、歯牙がセラミックス焼成体から作製されており、セラミックス焼成体の空隙部分に樹脂またはシリコンの内何れかを含浸していることを特徴とする顎歯模型用歯牙である。
本発明は治療練習用の顎歯模型用の歯牙であって、歯牙がセラミックス焼成体から作製されており、セラミックス焼成体の空隙部分に熱硬化性樹脂または熱可塑性樹脂が含浸していることを特徴とする顎歯模型用歯牙である。
本発明は治療練習用の顎歯模型用の歯牙であって、歯牙がセラミックス焼成体から作製されたデンチン部分とエナメル部分からなる顎歯模型用歯牙において、デンチン部分のセラミックス焼成体の空隙部分にアクリル樹脂またはエポキシ樹脂が含浸していることを特徴とする顎歯模型用歯牙である。
The present invention is a tooth for a jaw and tooth model for therapeutic practice, wherein the tooth is made of a ceramic fired body, and a void portion of the ceramic fired body is impregnated with either resin or silicon. It is a tooth for a jaw tooth model.
The present invention relates to a tooth for a jaw and tooth model for therapeutic practice, wherein the tooth is made of a ceramic fired body, and a void portion of the ceramic fired body is impregnated with a thermosetting resin or a thermoplastic resin. This is a characteristic tooth for jaw model.
The present invention is a tooth for a jaw and tooth model for treatment practice, and in a tooth for a jaw and tooth model consisting of a dentin part and an enamel part, wherein the tooth is made of a ceramic fired body, A tooth for a jaw and tooth model, which is impregnated with an acrylic resin or an epoxy resin.
本発明は治療練習用の顎歯模型用の歯牙であって、歯牙がセラミックス焼成体から作製されたデンチン部分とエナメル部分からなる顎歯模型用歯牙において、デンチン部分のセラミックス焼成体の空隙部分に化学重合性樹脂が含浸していることを特徴とする顎歯模型用歯牙である。
本発明は治療練習用の顎歯模型用の歯牙であって、デンチン部分およびエナメル部分が無機粉末焼成体からなることを特徴とする顎歯模型用歯牙である。
本発明は治療練習用の顎歯模型用の歯牙であって、デンチン部分とエナメル部分からなり、デンチン部分とエナメル部分を作製した後に、デンチン部分とエナメル部分を接着することを特徴とする顎歯模型用歯牙である。
本発明の接着剤が有機性樹脂組成物であることを特徴とする顎歯模型用歯牙である。
The present invention is a tooth for a jaw and tooth model for treatment practice, and in a tooth for a jaw and tooth model consisting of a dentin part and an enamel part, wherein the tooth is made of a ceramic fired body, A tooth for a jaw and tooth model, which is impregnated with a chemically polymerizable resin.
The present invention relates to a tooth for a jaw and tooth model for practice of treatment, wherein the dentin portion and the enamel portion are made of an inorganic powder fired body.
The present invention relates to a tooth for a jaw and tooth model for therapeutic practice, which comprises a dentin portion and an enamel portion, and after the dentin portion and the enamel portion are prepared, the dentine portion and the enamel portion are bonded to each other. This is a model tooth.
A tooth for a jaw and tooth model, wherein the adhesive of the present invention is an organic resin composition.
本発明は、CIM技術を用いて射出成形し、脱脂、焼成の工程を経てデンチン部分およびエナメル部分を成形し、接着剤を用いてデンチン部分およびエナメル部分を接着させることを特徴とする顎歯模型用歯牙の製造方法である。 The present invention relates to a jaw and tooth model characterized by injection molding using CIM technology, forming a dentin portion and an enamel portion through degreasing and firing steps, and bonding the dentin portion and the enamel portion using an adhesive. This is a method for producing dental teeth.
本発明の方法によれば、デンチン部分、エナメル部分両方とも天然歯と同じ様な切削感を得られ、エナメル部分からデンチン部分へ移行する切削感が天然歯に近いことから、模型であっても天然歯牙を削る練習が容易に行なえる。
抜去歯は生体からの材料であり衛生上の問題があるため、感染予防等の処置を取らなくても安全に用いることができ、抜去歯の様な体感ができる歯牙が求められていた。また、衛生管理も特に必要なく、腐敗の恐れもない材料が求められていた。
According to the method of the present invention, both the dentin part and the enamel part can obtain the same cutting feeling as that of the natural tooth, and the cutting feeling that shifts from the enamel part to the dentin part is close to that of the natural tooth. Practice cutting natural teeth easily.
Since the extracted tooth is a material from a living body and has a hygiene problem, a tooth that can be used safely without taking measures such as infection prevention and has a feeling similar to that of the extracted tooth has been demanded. In addition, there is a need for a material that does not require any sanitary management and is free from the risk of corruption.
本発明の歯牙を用いて支台歯形成、窩洞形成をすることによって、一早く天然歯牙と同様な切削感を体験でき、形成体験が容易に行える。また、これらの形成技術を早く取得することができる。
本顎歯模型用歯牙は人体の中で最も硬い天然歯牙の代用物質で、通常の材料では切削時に軟らかく感じてしまうのに対し、天然歯牙と同様な切削感を得ることができる。口腔内での400000回転/分という高速回転するダイヤモンド研削材(エアータービン使用)を用いた切削と同じような切削体験ができる。
By forming an abutment tooth and a cavity using the tooth of the present invention, a cutting feeling similar to that of a natural tooth can be experienced quickly, and the formation experience can be easily performed. Moreover, these formation techniques can be acquired quickly.
The jaw model tooth is a substitute for the hardest natural tooth in the human body, and a normal material feels soft at the time of cutting, while a cutting feeling similar to that of a natural tooth can be obtained. A cutting experience similar to that of cutting using diamond abrasives (using an air turbine) rotating at a high speed of 400000 revolutions per minute in the oral cavity is possible.
本発明は顎歯模型用歯牙が天然歯牙とよく似た切削感を得ることができる。粉末焼成体のみでは十分な切削感を再現することができなかったが今回の発明で再現することができた。
更に、歯牙模型の歯冠の形状も重要であり、支台歯形成や窩洞形成の目標となり隆起部分や窩、咬頭などが正確に表現されていることが重要であり、CIMでの成形が適している。
本発明の歯牙は歯質と同じように白色、アイボリー色、乳白色、半透明色とすることができるため、よりリアルな切削体験をすることができる。好ましくは白色、アイボリー色、乳白色である。
歯牙切削時に飛散する粉塵を軽減する効果があり、模型などの粉塵による汚れを押さえることができた。勿論、練習している学生の粉塵の吸い込みも軽減することができた。
熱硬化性樹脂または架橋剤を含んだ樹脂を含浸させることで、含浸させない場合と比べ、天然歯牙に近い軟かい切削感となる。熱可塑性樹脂を含浸させることで含浸させない場合と比べ、天然歯牙に近い纏わり付く様な切削感となる。これらの樹脂は水を同時に用いる場合であっても溶け出すことなく、纏わり付く感じが再現できる。
本発明はデンチン部分、エナメル部分両方に用いることができるが、特にデンチン部分に用いることが好ましい。
In the present invention, the jaw model tooth can obtain a cutting feeling similar to that of a natural tooth. Although a sufficient cutting feeling could not be reproduced with the powder fired body alone, it could be reproduced with the present invention.
Furthermore, the shape of the crown of the tooth model is also important, and it is important that the ridges, fossa, and cusps are accurately expressed as the objective of abutment tooth formation and cavity formation. ing.
Since the tooth of the present invention can be white, ivory, milky white, and translucent, like a tooth, a more realistic cutting experience can be achieved. Preferred are white, ivory and milky white.
It has the effect of reducing dust scattered during tooth cutting, and it was possible to suppress dirt caused by dust from models and the like. Of course, we were able to reduce the inhalation of dust by the practicing students.
By impregnating a thermosetting resin or a resin containing a crosslinking agent, a soft cutting feeling close to that of a natural tooth is obtained as compared with a case where no impregnation is performed. Compared to the case where the thermoplastic resin is impregnated, the cutting feeling is close to that of a natural tooth. These resins can reproduce the feeling of clumping without dissolving even when water is used at the same time.
Although this invention can be used for both a dentin part and an enamel part, it is particularly preferable to use it for a dentin part.
顎歯模型用歯牙とは、大学などで顎歯模型を用いて口腔内の治療行為をシミュレーションや治療の練習をするために用いられる歯牙であって、本発明は歯牙を切削し、形成する為に用いられる場合に関する。特に天然歯牙と切削性が近似した歯牙であって、窩洞形成、支台歯形成の練習に用いられる歯牙に関する。 A tooth for a jaw and tooth model is a tooth used for simulating the practice of treatment in the oral cavity and practicing treatment using a jaw and tooth model in universities, etc., and the present invention cuts and forms teeth. It relates to the case used for In particular, the present invention relates to a tooth having cutting ability similar to that of a natural tooth and used for practicing cavity formation and abutment tooth formation.
本発明の歯牙の組成はセラミックスから作製されることが好ましい。本発明の歯牙の組成はアルミナ系、ジルコニア系、シリカ系、窒化アルミ、窒化ケイ素などのセラミックスまたはガラスから作製される。また、アルミナ系、ジルコニア系で作製されることは好ましい。アルミナ系、ジルコニア系とはアルミナまたはジルコニアが焼成体組成の60%〜100%、好ましくは80%〜100%、更に好ましくは95%〜100%であることである。特にアルミナの組成が50%〜100%、好ましくは70%〜100%、更に好ましくは90%〜100%であることである。歯牙の組成がアルミナ粉末から成形されることが好ましい。
エナメル部分とデンチン部分の硬さの調整には、粒度を荒くする、空隙を多くする、材質を変えるなどの方法、焼成温度を変える、係留時間を変える等々の方法があるが、最も適した方法は、同一組成で粒度を変えることである。
エナメル部分の平均粒子径に対して、デンチン部分の平均粒子径を10倍以上にすることが好ましい。エナメル部分の平均粒子径が0.1〜0.5μmである場合は、デンチン部分の平均粒子径は1.0〜10.0μmに設定することが好ましい。
焼成温度に関しては組成によって異なるが、シリカ等のガラス成分が多い場合は焼成温度が800〜1200℃、アルミナの場合は1200〜1600℃の焼成温度、好ましくは1400〜1550℃の焼成温度となる。
The tooth composition of the present invention is preferably produced from ceramics. The composition of the tooth of the present invention is produced from ceramics or glass such as alumina, zirconia, silica, aluminum nitride, and silicon nitride. Moreover, it is preferable to produce by an alumina type and a zirconia type. Alumina-based and zirconia-based are that alumina or zirconia is 60% to 100%, preferably 80% to 100%, more preferably 95% to 100% of the fired body composition. In particular, the composition of alumina is 50% to 100%, preferably 70% to 100%, and more preferably 90% to 100%. The tooth composition is preferably molded from alumina powder.
To adjust the hardness of the enamel part and dentin part, there are methods such as roughening the grain size, increasing the voids, changing the material, changing the firing temperature, changing the mooring time, etc., but the most suitable method Is to change the particle size with the same composition.
The average particle size of the dentin portion is preferably 10 times or more than the average particle size of the enamel portion. When the average particle size of the enamel portion is 0.1 to 0.5 μm, the average particle size of the dentin portion is preferably set to 1.0 to 10.0 μm.
Although the firing temperature varies depending on the composition, when there are many glass components such as silica, the firing temperature is 800 to 1200 ° C., and when alumina is 1200 to 1600 ° C., preferably 1400 to 1550 ° C.
エナメル部分とデンチン部分の成形はセラミックスの成形方法でCIM技術を用いることは好ましい。
CIM技術を用いて、エナメル部分とデンチン部分とを射出成形し、脱脂、焼成の工程を経て、焼成されたエナメル部分とデンチン部分の界面を熱硬化性樹脂や化学重合性樹脂の接着剤を用いて接着することも好ましい。
For forming the enamel part and the dentin part, it is preferable to use the CIM technique as a ceramic forming method.
Using CIM technology, the enamel part and the dentin part are injection-molded, degreased and fired, and the interface between the fired enamel part and the dentin part is used with an adhesive of thermosetting resin or chemically polymerizable resin. It is also preferable to bond them together.
本発明は、顎歯模型用歯牙のセラミックス焼成体中の空間部分に有機系材料を含浸させることに特徴がある。
本発明の空間部分に含浸させる有機系材料は、熱硬化性樹脂や熱可塑性樹脂、架橋剤を含んだ樹脂の内少なくとも一つ以上である事が好ましい。
The present invention is characterized in that an organic material is impregnated in a space portion in a ceramic fired body of a jaw tooth model tooth.
The organic material impregnated in the space portion of the present invention is preferably at least one of a thermosetting resin, a thermoplastic resin, and a resin containing a crosslinking agent.
本発明に用いられる含浸させる樹脂は熱硬化性樹脂や熱可塑性樹脂を用いることができる。熱硬化性樹脂または架橋剤を含んだ樹脂が好ましい。更に、エポキシ樹脂が好ましい。熱可塑性樹脂とは、熱を加えることにより成形できる程度の熱可塑性を得ることの出来る樹脂のことを指し、熱硬化性樹脂とは熱を加えることにより架橋が進み硬化する樹脂を指します。具体的にはアクリル系、スチレン系、オレフィン系、塩ビ系、ウレタン系、ポリアミド系、ポリブタジエン系、ポリアセタール系、飽和ポリエステル系、ポリカーボネート、ポリフェニレンエーテルなど適宜使用できる。
特に、アクリル系、スチレン系、ウレタン系、ポリアミド系樹脂が好ましい。
As the resin to be impregnated used in the present invention, a thermosetting resin or a thermoplastic resin can be used. A thermosetting resin or a resin containing a crosslinking agent is preferred. Furthermore, an epoxy resin is preferable. Thermoplastic resin refers to a resin that can be molded to a degree of thermoplasticity by applying heat, and thermosetting resin refers to a resin that crosslinks and cures when heated. Specifically, acrylic, styrene, olefin, vinyl chloride, urethane, polyamide, polybutadiene, polyacetal, saturated polyester, polycarbonate, polyphenylene ether and the like can be used as appropriate.
In particular, acrylic, styrene, urethane, and polyamide resins are preferable.
熱可塑性樹脂よりも熱硬化性樹脂の方が好ましい。熱硬化性樹脂とは、加工後は溶媒に溶けず再加熱しても軟化しない。尿素樹脂・メラミン樹脂・フェノール樹脂、エポキシ樹脂などが代表的に使用でき、メラミン樹脂及びエポキシ樹脂が好ましい。最も好ましいのはエポキシ樹脂である。
化学重合性樹脂であることが好ましい。焼成体の空隙部分に樹脂が含浸し容易に硬化できるためである。
A thermosetting resin is preferred to a thermoplastic resin. A thermosetting resin does not dissolve in a solvent after processing and does not soften even when reheated. A urea resin, a melamine resin, a phenol resin, an epoxy resin, and the like can be typically used, and a melamine resin and an epoxy resin are preferable. Most preferred is an epoxy resin.
It is preferably a chemically polymerizable resin. This is because the resin is impregnated into the voids of the fired body and can be easily cured.
化学重合性樹脂とは、本来熱硬化性樹脂や熱可塑性樹脂に含まれる樹脂であっても、化学触媒を用いて、重合する樹脂のことである。特に架橋材を含み熱可塑性がないものが好ましい。
接着剤に用いる樹脂は熱硬化性樹脂や熱可塑性樹脂、化学重合性樹脂の中で、熱硬化性樹脂、化学重合性樹脂が好ましい。
The chemically polymerizable resin is a resin that is polymerized using a chemical catalyst even if it is originally contained in a thermosetting resin or a thermoplastic resin. Particularly preferred are those containing a cross-linking material and having no thermoplasticity.
The resin used for the adhesive is preferably a thermosetting resin or a chemically polymerizable resin among thermosetting resins, thermoplastic resins, and chemically polymerizable resins.
(歯牙の焼成体作製)
歯牙形体の形状を射出成形できる金型を作製した。歯牙の原料としてのCIM用アルミナ
ペレット(Al2O3が26%、SiO2が44%、平均粒径3.0μm、ステアリン酸30%)1kgを用いて、歯牙形体の金型に、射出成形し射出体を得た。
作製された歯牙の形をした射出体を、脱脂、焼成(1300℃、係留時間10分)として焼成体1を得た。
(エナメル部分とデンチン部分の焼成体作製)
歯牙形体のエナメル部分とデンチン部分の目的形状を射出成形できる金型を作製した。エナメル部分もデンチン部分も成型後、脱脂、焼成により収縮が発生する為、その部分を事前に大きく計算して金型を作製した。材料ごとに金型を調整して実施した。
エナメル部分の原料としてのCIM用アルミナ
ペレット(Al2O3が68%、SiO2が2%、平均粒径0.3μm、ステアリン酸30%)1kgを用いて、歯牙形体の金型に、射出成形し射出体を得た。
作製されたエナメル部分の形をした射出体を、脱脂、焼成(1550℃、係留時間10分)として焼成体2−1を得た。
デンチン部分の原料としてのCIM用アルミナ
ペレット(Al2O3が68%、SiO2が2%、平均粒径5.0μm、ステアリン酸30%)1kgを用いて、歯牙形体の金型に、射出成形し射出体を得た。
作製されたデンチン部分の形をした射出体を、脱脂、焼成(1400℃、係留時間15分)として焼成体2−2を得た。
(Manufacture of fired teeth)
A mold capable of injection molding the shape of the tooth form was produced. Using 1 kg of alumina pellets for CIM (26% Al 2 O 3 , 44% SiO 2 , average particle size 3.0 μm, 30% stearic acid) as a raw material for teeth, injection molding into a mold of tooth shape A projectile was obtained.
The produced tooth-shaped injection body was degreased and fired (1300 ° C., mooring time 10 minutes) to obtain fired body 1.
(Production of fired body of enamel part and dentin part)
A mold capable of injection molding the target shapes of the enamel part and dentin part of the tooth form was produced. Since both the enamel part and the dentin part are shrunk by degreasing and firing after molding, the part was largely calculated in advance to prepare a mold. The mold was adjusted for each material.
Using 1 kg of alumina pellets for CIM (68% Al 2 O 3 , 2% SiO 2 , average particle size 0.3 μm, 30% stearic acid) as a raw material for the enamel part, it is injected into a dental mold Molded to obtain an injection body.
A fired body 2-1 was obtained by degreasing and firing (1550 ° C., mooring time 10 minutes) of the produced injection body in the form of the enamel portion.
Using 1 kg of alumina pellets for CIM (68% Al 2 O 3 , 2% SiO 2 , average particle size 5.0 μm, 30% stearic acid) as a raw material for dentin, injection into a dental mold Molded to obtain an injection body.
The produced injection body in the form of the dentin portion was degreased and fired (1400 ° C., mooring time 15 minutes) to obtain a fired body 2-2.
(樹脂の含浸)
得られた焼成体1、2−1、2−2を以下の各材料中に包埋し、真空容器に入れ、真空にすることで焼成体の空隙部分に十分に含浸したことを確認し、焼成体2−1、2−2は接合し、樹脂を硬化させた。
作製された歯牙の切削感を確認した。焼成体はそれぞれ30個作製し試験を行なった。
(試験を行なった樹脂)
エポキシ樹脂(低粘度エポキシレジン Z-2/H-07):触媒を添加したエポキシ樹脂を用いた。72時間放置後、ダイヤモンドバーで切削感を確認した。
アクリル樹脂(クラレ製、MMAモノマー):化学重合触媒を添加したアクリル樹脂を用いた。72時間放置後、ダイヤモンドバーで切削感を確認した。
シリコン樹脂(RTVシリコン樹脂 M8017:旭化成):触媒を添加したシリコン樹脂を用いた。72時間放置後、ダイヤモンドバーで切削感を確認した。
比較例:比較例として含浸させていない焼成体を用いた。
(Resin impregnation)
The obtained fired bodies 1, 2-1, 2-2 were embedded in the following materials, placed in a vacuum container, and confirmed to be sufficiently impregnated in the voids of the fired body by making a vacuum, The fired bodies 2-1 and 2-2 were joined to cure the resin.
The cutting feeling of the produced tooth was confirmed. 30 fired bodies were prepared and tested.
(Resin tested)
Epoxy resin (low viscosity epoxy resin Z-2 / H-07): An epoxy resin to which a catalyst was added was used. After leaving for 72 hours, the cutting feeling was confirmed with a diamond bar.
Acrylic resin (manufactured by Kuraray, MMA monomer): An acrylic resin to which a chemical polymerization catalyst was added was used. After leaving for 72 hours, the cutting feeling was confirmed with a diamond bar.
Silicon resin (RTV silicone resin M8017: Asahi Kasei): A silicone resin to which a catalyst was added was used. After leaving for 72 hours, the cutting feeling was confirmed with a diamond bar.
Comparative Example: A fired body not impregnated was used as a comparative example.
○(切削感):デンチンとエナメルとが十分に表現できていなかった。
○(切削ネバさ):粘りけというより、若干の弾性感があった。
×:切削時の粘りが感じられず、粉塵が大きく飛散した。
◎(切削粉砕感):切削時における粉砕感がほとんど無く、生体歯牙を削る感覚であった。
○(切削粉砕感):切削時における粉砕感が感じられ、若干異なるものの生体歯牙を削る感覚であった。
×:切削時の粘りが感じられず、粉塵が大きく飛散した。
○ (cutting feeling): Dentin and enamel could not be expressed sufficiently.
○ (cutting): There was a slight elasticity rather than stickiness.
X: Stickiness at the time of cutting was not felt, and dust was scattered greatly.
A (cutting pulverization feeling): There was almost no pulverization feeling at the time of cutting, and it was a feeling of cutting a living tooth.
○ (cutting pulverization feeling): A feeling of pulverization at the time of cutting was felt.
X: Stickiness at the time of cutting was not felt, and dust was scattered greatly.
実施例1.2は比較例1と比べて粘りが感じられ天然歯牙と同様な切削感が得られた。切削された粉塵も比較例1と比べて少なく、飛散も少なかった。切削時におけるセラミックス独特の粉砕感がほとんど無く、生体歯牙を削る感覚に近かった。
実施例3は比較例1と比べて粘りが感じられ天然歯牙と同様な切削感が得られた。切削された粉塵も比較例1と比べて少なく、飛散も少なかった。実施例1.2に比べると飛散量が多かった。切削感も天然歯に近似している。実施例1.2に比べると天然歯が持つ切削時の抵抗の感じが若干劣るように思われる。実施例1、2よりは劣るものの、天然歯牙の状態が再現できていた。
実施例4.5は比較例2と比べて粘りが感じられ天然歯牙と同様な切削感が得られた。切削された粉塵も比較例2と比べて少なく、飛散も少なかった。エナメル部分からデンチン部分へ移層時においても、粘りけを感じる天然歯同様の切削感であった。切削時におけるセラミックス独特の粉砕感がほとんど無く、生体歯牙を削る感覚に近かった。
実施例6は比較例2と比べて粘りが感じられ天然歯牙と同様な切削感が得られた。切削された粉塵も比較例2と比べて少なく、飛散も少なかった。実施例4.5に比べると飛散量が多かった。切削感も天然歯に近似している。
エナメル部分からデンチン部分へ移層時においても、粘りけを感じる天然歯同様の切削感であったが、実施例4.5に比べると天然歯と異なる抵抗の感じが若干劣るように思われる。実施例4.5よりは劣るものの、天然歯牙の状態が再現できていた。
In Example 1.2, stickiness was felt as compared with Comparative Example 1, and a cutting feeling similar to that of natural teeth was obtained. The cut dust was less than that of Comparative Example 1, and the scattering was less. There was almost no crushing feeling peculiar to ceramics at the time of cutting, and it was close to the sense of cutting living teeth.
In Example 3, stickiness was felt as compared with Comparative Example 1, and a cutting feeling similar to that of natural teeth was obtained. The cut dust was less than that of Comparative Example 1, and the scattering was less. Compared with Example 1.2, there was much scattering amount. The cutting feeling is similar to natural teeth. Compared to Example 1.2, it seems that the feeling of resistance of natural teeth when cutting is slightly inferior. Although inferior to Examples 1 and 2, the state of natural teeth could be reproduced.
In Example 4.5, stickiness was felt as compared with Comparative Example 2, and a cutting feeling similar to that of natural teeth was obtained. The cut dust was less than that of Comparative Example 2, and the scattering was also small. Even when the layer was transferred from the enamel part to the dentin part, it had a cutting feel similar to that of natural teeth that felt sticky. There was almost no crushing feeling peculiar to ceramics at the time of cutting, and it was close to the sense of cutting living teeth.
In Example 6, stickiness was felt as compared with Comparative Example 2, and a cutting feeling similar to that of natural teeth was obtained. The cut dust was less than that of Comparative Example 2, and the scattering was also small. Compared with Example 4.5, there was much scattering amount. The cutting feeling is similar to natural teeth.
Even when the layer was transferred from the enamel portion to the dentin portion, the cutting feeling was the same as that of natural teeth that felt stickiness, but the resistance feeling different from that of natural teeth seems to be slightly inferior to Example 4.5. Although inferior to Example 4.5, the state of natural teeth could be reproduced.
Claims (5)
歯牙がセラミックスス焼成体から作製されており、セラミックス焼成体の空隙部分に樹脂またはシリコンの内何れかを含浸していることを特徴とする顎歯模型用歯牙。 Teeth for a jaw and tooth model for treatment practice,
A tooth for a jaw and tooth model, wherein the tooth is made of a ceramic fired body, and a void portion of the ceramic fired body is impregnated with either resin or silicon.
歯牙がセラミックス焼成体から作製されており、セラミックス焼成体の空隙部分に熱硬化性樹脂または熱可塑性樹脂が含浸していることを特徴とする顎歯模型用歯牙。 Teeth for a jaw and tooth model for treatment practice,
A tooth for a jaw and tooth model, wherein the tooth is made of a ceramic fired body, and a void portion of the ceramic fired body is impregnated with a thermosetting resin or a thermoplastic resin.
デンチン部分およびエナメル部分が無機粉末焼成体からなることを特徴とする請求項1〜4記載の顎歯模型用歯牙。 Teeth for a jaw and tooth model for treatment practice,
The dentine part and the enamel part are made of an inorganic powder fired body.
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EP2011450A1 (en) * | 2006-04-17 | 2009-01-07 | Kabushiki Kaisha Shofu | Tooth for dental arch model and method of producing the same |
EP2020653A3 (en) * | 2007-08-01 | 2010-01-06 | Kabushiki Kaisha Shofu | Tooth for tooth model, comprising enamel portion impregnated with resin or low melting point glass, and method for producing the same |
JPWO2014021343A1 (en) * | 2012-07-31 | 2016-07-21 | クラレノリタケデンタル株式会社 | Manufacturing method of dental mill blank |
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EP2011451A1 (en) * | 2006-04-17 | 2009-01-07 | Kabushiki Kaisha Shofu | Tooth for dental arch model and method of producing the same |
EP2011451A4 (en) * | 2006-04-17 | 2010-11-24 | Shofu Kk | Tooth for dental arch model and method of producing the same |
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US8784112B2 (en) | 2006-04-17 | 2014-07-22 | Kabushiki Kaisha Shofu | Tooth for dental arch model and method for producing the same |
EP2020653A3 (en) * | 2007-08-01 | 2010-01-06 | Kabushiki Kaisha Shofu | Tooth for tooth model, comprising enamel portion impregnated with resin or low melting point glass, and method for producing the same |
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