GB1346701A - Process for the manufacture of aceto-acetic acid - Google Patents
Process for the manufacture of aceto-acetic acidInfo
- Publication number
- GB1346701A GB1346701A GB3999072A GB3999072A GB1346701A GB 1346701 A GB1346701 A GB 1346701A GB 3999072 A GB3999072 A GB 3999072A GB 3999072 A GB3999072 A GB 3999072A GB 1346701 A GB1346701 A GB 1346701A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydrogen chloride
- aceto
- manufacture
- acetic acid
- diketene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1346701 Acetoacetic acid WACKERCHEMIE GmbH 29 Aug 1972 [4 Nov 1971] 39990/72 Heading C2C Acetoacetic acid ester is prepared by hydrolysing diketene at from 0 to 30‹ C. with the stoichiometric amount of water in the presence of 10 to 60 mol. per cent of hydrogen chloride, relative to the diketene, and crystallizing the acid at - 40 to 0‹ C. An inert solvent such as an aliphatic hydrocarbon may be used and the hydrogen chloride added as free hydrogen chloride or hydrochloric acid.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19712154875 DE2154875C3 (en) | 1971-11-04 | Process for the preparation of crystalline acetoacetic acid |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1346701A true GB1346701A (en) | 1974-02-13 |
Family
ID=5824207
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3999072A Expired GB1346701A (en) | 1971-11-04 | 1972-08-29 | Process for the manufacture of aceto-acetic acid |
Country Status (6)
Country | Link |
---|---|
JP (1) | JPS5024292B2 (en) |
BE (1) | BE790793A (en) |
CH (1) | CH568954A5 (en) |
FR (1) | FR2158480B1 (en) |
GB (1) | GB1346701A (en) |
IT (1) | IT966777B (en) |
-
0
- BE BE790793D patent/BE790793A/en unknown
-
1972
- 1972-08-29 GB GB3999072A patent/GB1346701A/en not_active Expired
- 1972-10-26 IT IT5362072A patent/IT966777B/en active
- 1972-11-02 JP JP11017772A patent/JPS5024292B2/ja not_active Expired
- 1972-11-03 FR FR7238925A patent/FR2158480B1/fr not_active Expired
- 1972-11-03 CH CH1605772A patent/CH568954A5/xx not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE2154875B2 (en) | 1976-04-22 |
DE2154875A1 (en) | 1973-05-10 |
JPS4854026A (en) | 1973-07-30 |
JPS5024292B2 (en) | 1975-08-14 |
CH568954A5 (en) | 1975-11-14 |
BE790793A (en) | 1973-04-30 |
FR2158480A1 (en) | 1973-06-15 |
IT966777B (en) | 1974-02-20 |
FR2158480B1 (en) | 1975-03-28 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |