GB1183833A - Improvements in Chromatographic Processes and Apparatus. - Google Patents

Improvements in Chromatographic Processes and Apparatus.

Info

Publication number
GB1183833A
GB1183833A GB36538/67A GB3653867A GB1183833A GB 1183833 A GB1183833 A GB 1183833A GB 36538/67 A GB36538/67 A GB 36538/67A GB 3653867 A GB3653867 A GB 3653867A GB 1183833 A GB1183833 A GB 1183833A
Authority
GB
United Kingdom
Prior art keywords
velocity
relative overall
carried out
point
aug
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB36538/67A
Inventor
Victor Pretorious
Hans Helmut Hahn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of GB1183833A publication Critical patent/GB1183833A/en
Expired legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6052—Construction of the column body
    • G01N30/6069—Construction of the column body with compartments or bed substructure
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/28—Control of physical parameters of the fluid carrier
    • G01N30/32—Control of physical parameters of the fluid carrier of pressure or speed
    • G01N2030/324—Control of physical parameters of the fluid carrier of pressure or speed speed, flow rate
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N2030/387—Turbulent flow of mobile phase
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/52—Physical parameters
    • G01N2030/521—Physical parameters form

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,183,833. Gas and liquid chromatography. V. PRETORIUS and H. H. HAHN. 9 Aug., 1967 [11 Aug., 1966], No. 36538/67. Addition to 1148661. Headings B1L and B1X. A gas or liquid chromatographic separating process is carried out in a tubular column in which movement of the retarding phase is stationary or restrained and the relative overall flow velocity between the phases is adjusted to a value in excess of the velocity corresponding to the onset in the forwarding phase of convective flow phenomena apparent by a point of downward inflection in a graphical representation of plate height against the said relative overall velocity, and the chromatographic separation is carried out at this adjusted velocity. In Fig 1, the ordinate h is proportional to the plate height, the abscissa Re is proportional to the relative overall velocity, and the point of downward inflection is at c. The separation may be carried out at or beyond a relative overall velocity corresponding to point d. Columns described may be of copper internally covered with whiskers or fur formed by oxidation with sodium chlorite in the presence of cyanide ion and strong alkali (Fig. 2); have an internal spiral groove for countercurrent chromatography (Fig. 6); have inclined perforated plates (Fig. 8); comprise bonded beads coated with retarding phase (Fig. 11) or Raschig rings (Fig. 12).
GB36538/67A 1966-08-11 1967-08-09 Improvements in Chromatographic Processes and Apparatus. Expired GB1183833A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ZA664773 1966-08-11

Publications (1)

Publication Number Publication Date
GB1183833A true GB1183833A (en) 1970-03-11

Family

ID=25561010

Family Applications (1)

Application Number Title Priority Date Filing Date
GB36538/67A Expired GB1183833A (en) 1966-08-11 1967-08-09 Improvements in Chromatographic Processes and Apparatus.

Country Status (3)

Country Link
US (1) US3522172A (en)
DE (1) DE1673011C3 (en)
GB (1) GB1183833A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1244507A1 (en) * 2000-01-04 2002-10-02 Waters Investments Limited Capillary columns employing monodispersed particles

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US3953569A (en) * 1971-07-22 1976-04-27 Maomi Seko Concentration of uranium 235 in mixtures with uranium 238 using ion exchange resins
US3768300A (en) * 1971-09-24 1973-10-30 Vacuum Inst Corp Differential sorption chromatograhy
AU476229B2 (en) * 1971-10-01 1976-09-16 Suomen Sokeri Osakeyhtio Liquid control apparatus for chromatography columns
US4175037A (en) * 1978-04-10 1979-11-20 Whatman Inc. Process for packing chromatographic columns
JPS59199032A (en) * 1983-04-26 1984-11-12 Asahi Chem Ind Co Ltd Pressure absorbing mechanism
US4486312A (en) * 1983-08-12 1984-12-04 Dionex Corporation Analysis of liquid streams using tubing with protuberances on its inner wall
US4551251A (en) * 1984-03-06 1985-11-05 The United States Of America As Represented By The Department Of Health And Human Services Monolithic integrated flow circuit
FR2575666B1 (en) * 1985-01-04 1989-08-18 Centre Nat Rech Scient METHOD AND DEVICE FOR CHROMATOGRAPHIC SEPARATION OF BIOLOGICAL MACROMOLECULES
US4587834A (en) * 1985-03-07 1986-05-13 General Electric Company Method and apparatus for analyzing gases dissolved in a liquid sample
FI97277C (en) * 1993-01-25 1996-11-25 Suomen Sokeri Oy Chromatographic separation column, constructs in the same and chromatographic separation procedure
FI96225C (en) 1993-01-26 1996-05-27 Cultor Oy Process for fractionation of molasses
US6663780B2 (en) 1993-01-26 2003-12-16 Danisco Finland Oy Method for the fractionation of molasses
FR2708480B1 (en) * 1993-08-02 1996-05-24 Inst Francais Du Petrole Single-phase fluid distributor-mixer-extractor for granular solids beds.
US5795398A (en) 1994-09-30 1998-08-18 Cultor Ltd. Fractionation method of sucrose-containing solutions
DE69625769T2 (en) * 1995-10-20 2003-08-07 Institut Francais Du Petrole, Rueil Malmaison Distributor for the independent introduction and / or discharge of fluids
US6224776B1 (en) * 1996-05-24 2001-05-01 Cultor Corporation Method for fractionating a solution
US6406632B1 (en) 1998-04-03 2002-06-18 Symyx Technologies, Inc. Rapid characterization of polymers
US6416663B1 (en) 1998-04-03 2002-07-09 Symyx Technologies, Inc. Chromatographic column for rapid characterizations of polymers
US6866786B2 (en) * 1998-04-03 2005-03-15 Symyx Technologies, Inc. Rapid characterization of polymers
US6855258B2 (en) * 1999-04-02 2005-02-15 Symyx Technologies, Inc. Methods for characterization of polymers using multi-dimensional liquid chromatography with parallel second-dimension sampling
DE10100921A1 (en) * 2001-01-10 2002-07-11 Abb Research Ltd Separating column used for determining calorific value of natural gas comprises capillary filled with separating material in form of balls having same diameter
FI20010977A (en) * 2001-05-09 2002-11-10 Danisco Sweeteners Oy Chromatographic separation method
KR20040032884A (en) * 2001-08-03 2004-04-17 닛본 덴끼 가부시끼가이샤 Separation Apparatus and Process for Fabricating Separation Apparatus
US6730228B2 (en) * 2001-08-28 2004-05-04 Symyx Technologies, Inc. Methods and apparatus for characterization of polymers using multi-dimensional liquid chromatography with regular second-dimension sampling
AU2003299566A1 (en) * 2002-11-26 2004-06-18 Prime Separations Incorporated Chromatographic separation process
JP4920674B2 (en) * 2005-03-18 2012-04-18 キヤノン株式会社 Structure, separation element, separation device, capture element, detection device, method for producing the same, and method for separating and detecting target substance
ATE519723T1 (en) * 2006-06-02 2011-08-15 Albemarle Corp SEPARATION AND/OR RECOVERY OF PROPYL BROMIDE
US8293111B2 (en) * 2010-05-17 2012-10-23 Uti Limited Partnership Apparatus, system, and method for chromatography using a water stationary phase
US9308470B2 (en) 2013-03-12 2016-04-12 The Chem-Pro Group Llc Liquid-liquid extractor
US10073068B2 (en) * 2013-09-18 2018-09-11 Agilent Technologies, Inc. Liquid chromatography columns with structured walls
EP3266047A1 (en) * 2015-03-04 2018-01-10 OSRAM Opto Semiconductors GmbH Bin insert for binning of light emitting devices, binning arrangement for binning of light emitting devices, and use of a binning arrangement for binning of light emitting devices
US9981218B2 (en) * 2015-12-01 2018-05-29 Ma'an Nassar Raja Al-Ani Nanoparticle purifying system
CN115469047B (en) * 2022-09-21 2023-08-15 四川大学华西医院 Countercurrent chromatographic separation column without adapter

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA703044A (en) * 1965-02-02 J. E. Golay Marcel Gas chromatographic apparatus
US2893955A (en) * 1956-05-11 1959-07-07 Gulf Research Development Co Continuous separation process
US3005514A (en) * 1959-04-20 1961-10-24 Cons Electrodynamics Corp Fluid treating columns
DE1258631B (en) * 1962-05-04 1968-01-11 Erwin Heine Dipl Chem Dr Separating column for performing gas chromatographic analyzes
US3250059A (en) * 1963-05-15 1966-05-10 Nat Lead Co Method and means for conditioning gases
US3374606A (en) * 1965-09-10 1968-03-26 Abcor Inc Method of and apparatus for chromatographic separations
US3298527A (en) * 1965-05-17 1967-01-17 Wright John Lemon Chromatographic flow column

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1244507A1 (en) * 2000-01-04 2002-10-02 Waters Investments Limited Capillary columns employing monodispersed particles
EP1244507A4 (en) * 2000-01-04 2008-02-13 Waters Investments Ltd Capillary columns employing monodispersed particles

Also Published As

Publication number Publication date
DE1673011B2 (en) 1974-12-12
DE1673011A1 (en) 1972-08-10
DE1673011C3 (en) 1975-07-31
US3522172A (en) 1970-07-28

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee