DE575859C - Process for the preparation of salts of tertiary aliphatic bases - Google Patents
Process for the preparation of salts of tertiary aliphatic basesInfo
- Publication number
- DE575859C DE575859C DEC44044D DEC0044044D DE575859C DE 575859 C DE575859 C DE 575859C DE C44044 D DEC44044 D DE C44044D DE C0044044 D DEC0044044 D DE C0044044D DE 575859 C DE575859 C DE 575859C
- Authority
- DE
- Germany
- Prior art keywords
- salts
- preparation
- tertiary aliphatic
- bases
- aliphatic bases
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
Description
Verfahren zur Herstellung von Salzen tertiärer aliphatischer Basen Es wurde gefunden, daß. eine große Zahl von Salzen aliphatischer, insbesondere tertiärer Basen die bisher-noch nicht bekannte Eigenschaft besitzen, appetitanregend zu wirken. Sie sind jedoch einerseits stark hygroskopisch, so daß ihre Dosierbarkeit und die Herstellung von Tablettenerschwert ist, andererseits besitzen sie .auch noch den durchdringenden Geruch der freien Basen, der nur schwierig zu entfernen ist, schließlich läßt ihr Geschmack und ihre Verträglichkeit zu wünscheai übrig.Process for the preparation of salts of tertiary aliphatic bases It was found that. a large number of salts of aliphatic, especially tertiary Bases have the previously unknown property of stimulating the appetite. However, they are on the one hand very hygroscopic, so that their meterability and the Manufacture of tablet sword is, on the other hand, they also have the pervasive odor of free bases that is difficult to remove after all leaves their taste and tolerance to be desiredeai.
Es zeigte sich nun, daß die bisher noch nicht beschriebenen Tannate dieser Verbindungen für den oben angegebenen Zweck vorzüglich geeignet sind; sie sind unlöslich, also nicht hygroskopisch. Durch Säuren und Alkalien werden sie leicht gespalten, so daß sie im Organismus in die gewünschte resorbierbare Form übergeführt werden können. Außerdem lassen sie sich durch zweckmäßiges Reinigen mittels gründlichen Auswaschens so weit geschmack- und geruchlos darstellen, daß ihrer praktischen therapeutischen Anwendung nichts im Wiege steht.It has now been shown that the tannates that have not yet been described these compounds are eminently suitable for the purpose indicated above; she are insoluble, i.e. not hygroscopic. Acids and alkalis make them light split so that they are converted into the desired absorbable form in the organism can be. In addition, they can be cleaned properly by means of thorough The wash-out is so tasteless and odorless that its practical therapeutic Application is not in the cradle.
Beispiel z 5o Teile Tannin werden in der 13fachen Menge Alkohol in der Kälte gelöst und unter stetem Rühren 4.o Teile einer 33%igen Äthyldimethylaminlösung zulaufen .gelassen. Das Tannat fällt hierbei als unlöslicher Niederschlag aus, welcher schnell abgesaugt, mit Alkohol abgedeckt und im Vakuum über Schwefelsäure getrocknet wird. Das so erhaltene Produkt enthält -etwa 12,5 % Äthyldimethylamiri.Example z 50 parts of tannin are in 13 times the amount of alcohol in the cold and with constant stirring 4.o parts of a 33% ethyldimethylamine solution allowed to run. The tannate precipitates out as an insoluble precipitate, which quickly sucked off, covered with alcohol and dried in vacuo over sulfuric acid will. The product obtained in this way contains about 12.5% ethyldimethylamine.
Beispiel 2 5o Teile Tannin werden in 750 Teilen Alkohol gelöst und allmählich mit 23 Teilen Triäthylamiii versetzt. Der ausfallende Niederschlag wird, wie in Beispiel i angegeben, aufgearbeitet und ergibt ein Produkt von analogen Eigenschaften.Example 2 50 parts of tannin are dissolved in 750 parts of alcohol and 23 parts of triethylamine are gradually added. The precipitate which separates out is worked up as indicated in Example i and gives a product with analogous properties.
Beispiel 3 In gleicher Weise wie in Beispiel I und 2 werden 5o g Tannin, in Methylalkohol gelöst, mit 40 g einer 33%igen Trimethylaminlösung behandelt. Das ausfallende Produkt wird, wie in Beispiel i angegeben, aufgearbeitet.Example 3 In the same way as in Example I and 2, 50 g of tannin, dissolved in methyl alcohol, treated with 40 g of a 33% trimethylamine solution. That precipitating product is worked up as indicated in Example i.
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEC44044D DE575859C (en) | 1929-11-28 | 1929-11-28 | Process for the preparation of salts of tertiary aliphatic bases |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEC44044D DE575859C (en) | 1929-11-28 | 1929-11-28 | Process for the preparation of salts of tertiary aliphatic bases |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE575859C true DE575859C (en) | 1933-05-04 |
Family
ID=7025644
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEC44044D Expired DE575859C (en) | 1929-11-28 | 1929-11-28 | Process for the preparation of salts of tertiary aliphatic bases |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE575859C (en) |
-
1929
- 1929-11-28 DE DEC44044D patent/DE575859C/en not_active Expired
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE575859C (en) | Process for the preparation of salts of tertiary aliphatic bases | |
| DE625077C (en) | Process for the preparation of mixed silicic acid esters | |
| DE733317C (en) | Process for the production of synthetic resins from methacrylic acid amide | |
| DE709652C (en) | Process for the production of a starch product from potato starch | |
| DE430684C (en) | Process for the preparation of a basic triiodophenol bismuth compound | |
| DE479229C (en) | Process for the production of copper, zinc and magnesium salts of tannin | |
| DE741340C (en) | Process for the production of dry protein | |
| DE514399C (en) | Preparations for greasing leather | |
| DE682642C (en) | Process for the preparation of water-soluble compounds of the aromatic series | |
| DE565065C (en) | Process for the separate recovery of a hypertensive substance and a uterine muscle contracting substance from the posterior lobe of the pituitary gland | |
| DE713471C (en) | Process for the preparation of a water-soluble acetylsalicylic acid salt | |
| DE556716C (en) | Process for the production of stable colloidal aqueous solutions of the irradiated ergosterol | |
| DE597414C (en) | Process for the production of soluble derivatives of polyaminoarsenostibio compounds | |
| DE549726C (en) | Process for the preparation of silver, tannin or products containing acyl derivatives and proteins in solid form or in solution | |
| DE643979C (en) | Process for the preparation of therapeutically valuable gynecological hormone preparations | |
| DE527715C (en) | Process for the preparation of easily soluble salts of 3-acetylamino-4-oxybenzene-1-arsic acid | |
| AT203633B (en) | Process for the preparation of injectable solutions from royal jelly | |
| DE540700C (en) | Process for the preparation of an organic arsenic compound of the pyrazolone series | |
| DE494778C (en) | Process for the preparation of condensation products from the compounds obtainable by the action of aliphatic or mixed ketones on phenols | |
| DE494371C (en) | Process for the preservation of technical and pharmaceutical preparations | |
| DE616884C (en) | Method for the preparation of a tuberculosis antigen | |
| DE537698C (en) | Process for the preparation of mercury diarylarsine oxides | |
| DE963183C (en) | Process for obtaining genins from glycosides | |
| DE665513C (en) | Process for the preparation of 3,5-diiodo-4-oxyacetophenone | |
| DE426223C (en) | Process for the production of bismuth-containing adsorption compounds with a high degree of dispersion |