DE102004023249A1 - Verfahren zur strukturierten Befüllung von Kontaktrohren eines Kontaktrohrbündels - Google Patents

Verfahren zur strukturierten Befüllung von Kontaktrohren eines Kontaktrohrbündels Download PDF

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Publication number
DE102004023249A1
DE102004023249A1 DE102004023249A DE102004023249A DE102004023249A1 DE 102004023249 A1 DE102004023249 A1 DE 102004023249A1 DE 102004023249 A DE102004023249 A DE 102004023249A DE 102004023249 A DE102004023249 A DE 102004023249A DE 102004023249 A1 DE102004023249 A1 DE 102004023249A1
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DE
Germany
Prior art keywords
rings
battery
reactor tubes
manual removal
tubes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE102004023249A
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English (en)
Inventor
Martin Dieterle
Knut Eger
Klaus Joachim Mueller-Engel
Ulrich Hammon
Volker Schliephake
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BASF SE
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BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to DE102004023249A priority Critical patent/DE102004023249A1/de
Publication of DE102004023249A1 publication Critical patent/DE102004023249A1/de
Priority to KR1020067025734A priority patent/KR101237662B1/ko
Priority to KR1020127028080A priority patent/KR101431365B1/ko
Priority to CN201410148505.2A priority patent/CN103894117A/zh
Priority to CNA2005800146017A priority patent/CN1956773A/zh
Priority to RU2006143086/15A priority patent/RU2393915C2/ru
Priority to BRPI0509632A priority patent/BRPI0509632B1/pt
Priority to JP2007511930A priority patent/JP4768726B2/ja
Priority to CN201410148068.4A priority patent/CN103908927A/zh
Priority to PCT/EP2005/004351 priority patent/WO2005113123A1/de
Priority to EP05737721.0A priority patent/EP1748839B1/de
Priority to US11/118,433 priority patent/US7731916B2/en
Priority to MYPI20052014A priority patent/MY139283A/en
Priority to TW094114787A priority patent/TWI360436B/zh
Priority to ZA200610181A priority patent/ZA200610181B/en
Priority to US12/756,424 priority patent/US20100197489A1/en
Withdrawn legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/003—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00752—Feeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00769—Details of feeding or discharging
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00805—Details of the particulate material
    • B01J2208/00814—Details of the particulate material the particulate material being provides in prefilled containers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023—Details
    • B01J2208/024—Particulate material
    • B01J2208/025—Two or more types of catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/30—Details relating to random packing elements
    • B01J2219/308—Details relating to random packing elements filling or discharging the elements into or from packed columns
    • B01J2219/3086—Filling of the packing elements into the column or vessel, e.g. using a tube
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/888—Tungsten
    • B01J23/8885—Tungsten containing also molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/55—Cylinders or rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Ein Verfahren der strukturierten Befüllung von Kontaktrohren eines Kontaktrohrbündels, bei dem zur Erzeugung eines Befüllungsabschnitts einheitlich vorportionierte Zusammenstellungen von Katalysatorformkörpern verwendet werden.
DE102004023249A 2004-05-07 2004-05-07 Verfahren zur strukturierten Befüllung von Kontaktrohren eines Kontaktrohrbündels Withdrawn DE102004023249A1 (de)

Priority Applications (16)

Application Number Priority Date Filing Date Title
DE102004023249A DE102004023249A1 (de) 2004-05-07 2004-05-07 Verfahren zur strukturierten Befüllung von Kontaktrohren eines Kontaktrohrbündels
EP05737721.0A EP1748839B1 (de) 2004-05-07 2005-04-22 Verfahren zur strukturierten befüllung von kontaktrohren eines kontaktrohrbündels
BRPI0509632A BRPI0509632B1 (pt) 2004-05-07 2005-04-22 processo para carregamento de tubos de contato de um feixe de tubos de contato de uma maneira estruturada
CN201410148068.4A CN103908927A (zh) 2004-05-07 2005-04-22 以结构化方式装填催化剂管束中的催化剂管的方法
CN201410148505.2A CN103894117A (zh) 2004-05-07 2005-04-22 将催化剂成形体份封装于包装材料中而生产的包裹
CNA2005800146017A CN1956773A (zh) 2004-05-07 2005-04-22 以结构化方式装填催化剂管束中的催化剂管的方法
RU2006143086/15A RU2393915C2 (ru) 2004-05-07 2005-04-22 Способ структурированного заполнения контактных труб пучка контактных труб и упаковка, полученная обертыванием упаковочным средством количественной порции состава катализаторных формованных изделий
KR1020067025734A KR101237662B1 (ko) 2004-05-07 2005-04-22 촉매 튜브 다발의 촉매 튜브를 구조화된 방식으로 충진하는방법
JP2007511930A JP4768726B2 (ja) 2004-05-07 2005-04-22 接触管束の接触管を構造的に充填する方法
KR1020127028080A KR101431365B1 (ko) 2004-05-07 2005-04-22 촉매 튜브 다발의 촉매 튜브를 구조화된 방식으로 충진하는 방법
PCT/EP2005/004351 WO2005113123A1 (de) 2004-05-07 2005-04-22 Verfahren zur strukturierten befüllung von kontaktrohren eines kontaktrohrbündels
US11/118,433 US7731916B2 (en) 2004-05-07 2005-05-02 Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion
MYPI20052014A MY139283A (en) 2004-05-07 2005-05-05 Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion
TW094114787A TWI360436B (en) 2004-05-07 2005-05-06 Method of charging catalyst tubes of a bundle of c
ZA200610181A ZA200610181B (en) 2004-05-07 2006-12-05 Method for structurally filing contact tubes of a bank of contact tubes
US12/756,424 US20100197489A1 (en) 2004-05-07 2010-04-08 Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102004023249A DE102004023249A1 (de) 2004-05-07 2004-05-07 Verfahren zur strukturierten Befüllung von Kontaktrohren eines Kontaktrohrbündels

Publications (1)

Publication Number Publication Date
DE102004023249A1 true DE102004023249A1 (de) 2005-03-10

Family

ID=34178117

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102004023249A Withdrawn DE102004023249A1 (de) 2004-05-07 2004-05-07 Verfahren zur strukturierten Befüllung von Kontaktrohren eines Kontaktrohrbündels

Country Status (6)

Country Link
JP (1) JP4768726B2 (de)
KR (1) KR101431365B1 (de)
CN (3) CN1956773A (de)
DE (1) DE102004023249A1 (de)
RU (1) RU2393915C2 (de)
ZA (1) ZA200610181B (de)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007028332A1 (de) 2007-06-15 2008-12-18 Basf Se Verfahren zum Beschicken eines Reaktors mit einem Katalysatorfestbett, das wenigstens ringförmige Katalysatorformkörper K umfasst
DE102007028333A1 (de) 2007-06-15 2008-12-18 Basf Se Verfahren zum Einbringen einer wenigstens einer Produktionscharge von ringförmigen Schalenkatalysatoren K entnommenen Teilmenge in ein Reaktionsrohr eines Rohrbündelreaktors
DE202008004922U1 (de) 2008-04-10 2009-08-20 Süd-Chemie AG Beschickungssystem für Rohrbündelreaktoren
DE102014016203A1 (de) 2014-11-03 2016-05-19 Clariant International Ltd. Beschickungssystem zur Beschickung eines Rohrbündelreaktors
EP3112014A1 (de) * 2015-06-30 2017-01-04 Shell Internationale Research Maatschappij B.V. Verfahren zum laden eines teilchenförmigen materials in einem reaktor
WO2021048373A1 (de) * 2019-09-13 2021-03-18 Hte Gmbh The High Throughput Experimentation Company Verfahren zur befüllung von reaktoren und zur untersuchung von katalysatoren

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007017080A1 (de) * 2007-04-10 2008-10-16 Basf Se Verfahren zur Beschickung eines Längsabschnitts eines Kontaktrohres

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NL62754C (de) * 1941-01-27
IT955185B (it) * 1972-04-29 1973-09-29 Saes Getter Spa Cartuccia catalitica
KR830000312B1 (ko) * 1978-03-13 1983-03-02 유씨비, 에스. 에이. 가압처리 탄산음료용 플라스틱용기 몸체
US4402643A (en) * 1981-02-18 1983-09-06 Ppg Industries, Inc. Catalyst loader
JPS63197533A (ja) * 1987-12-28 1988-08-16 ケミカル・リサーチ・アンド・ライセンシング・カンパニー 接触蒸留用触媒構造物
US5417938A (en) * 1988-09-02 1995-05-23 Sulzer Brothers Limited Device for carrying out catalyzed reactions
US5266546A (en) * 1992-06-22 1993-11-30 Chemical Research & Licensing Company Catalytic distillation machine
EP0631813B1 (de) * 1993-06-30 1998-01-07 Sulzer Chemtech AG Katalysierender Festbettreaktor
DE4442346A1 (de) * 1994-11-29 1996-05-30 Basf Ag Verfahren zur Herstellung eines Katalysators, bestehend aus einem Trägerkörper und einer auf der Oberfläche des Trägerkörpers aufgebrachten katalytisch aktiven Oxidmasse
AU7476496A (en) * 1996-10-22 1998-04-24 Mathis P. Comardo Catalytic reactor charging system and method
JP3891726B2 (ja) * 1999-04-12 2007-03-14 三井化学株式会社 有機高分子シロキサン触媒の充填方法
DE19934324A1 (de) * 1999-07-21 2000-09-07 Basf Ag Vorrichtung zum Befüllen von Rohren mit Schüttgut
AU2001265326A1 (en) * 2000-06-07 2001-12-17 Abb Lummus Global Inc. Heat exchanger/reactor apparatus
CN1172823C (zh) * 2001-05-30 2004-10-27 中国石油化工股份有限公司 一种包装袋及其在催化剂包装中的应用
JP4092090B2 (ja) * 2001-06-26 2008-05-28 株式会社日本触媒 固体粒子充填反応器およびその反応器を用いた接触気相酸化方法
US7182778B2 (en) * 2001-11-01 2007-02-27 Gel Tech Solutions, Inc. Conforming thermal pack

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007028332A1 (de) 2007-06-15 2008-12-18 Basf Se Verfahren zum Beschicken eines Reaktors mit einem Katalysatorfestbett, das wenigstens ringförmige Katalysatorformkörper K umfasst
DE102007028333A1 (de) 2007-06-15 2008-12-18 Basf Se Verfahren zum Einbringen einer wenigstens einer Produktionscharge von ringförmigen Schalenkatalysatoren K entnommenen Teilmenge in ein Reaktionsrohr eines Rohrbündelreaktors
DE202008004922U1 (de) 2008-04-10 2009-08-20 Süd-Chemie AG Beschickungssystem für Rohrbündelreaktoren
DE102014016203A1 (de) 2014-11-03 2016-05-19 Clariant International Ltd. Beschickungssystem zur Beschickung eines Rohrbündelreaktors
EP3112014A1 (de) * 2015-06-30 2017-01-04 Shell Internationale Research Maatschappij B.V. Verfahren zum laden eines teilchenförmigen materials in einem reaktor
WO2021048373A1 (de) * 2019-09-13 2021-03-18 Hte Gmbh The High Throughput Experimentation Company Verfahren zur befüllung von reaktoren und zur untersuchung von katalysatoren
US11738316B2 (en) 2019-09-13 2023-08-29 Hte Gmbh The High Throughput Experimentation Method for filling reactors and for examining catalytic reactors

Also Published As

Publication number Publication date
RU2393915C2 (ru) 2010-07-10
ZA200610181B (en) 2008-05-28
KR20120134146A (ko) 2012-12-11
CN1956773A (zh) 2007-05-02
CN103908927A (zh) 2014-07-09
KR101431365B1 (ko) 2014-08-18
CN103894117A (zh) 2014-07-02
JP2007536078A (ja) 2007-12-13
RU2006143086A (ru) 2008-06-20
JP4768726B2 (ja) 2011-09-07

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