CN214199384U - Cooling device for production and use of high-viscosity silicone oil - Google Patents

Cooling device for production and use of high-viscosity silicone oil Download PDF

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Publication number
CN214199384U
CN214199384U CN202022602284.5U CN202022602284U CN214199384U CN 214199384 U CN214199384 U CN 214199384U CN 202022602284 U CN202022602284 U CN 202022602284U CN 214199384 U CN214199384 U CN 214199384U
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reaction kettle
silicone oil
wall surface
cooling tank
pipe
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CN202022602284.5U
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Chinese (zh)
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李俊
陈阿勤
杨清彪
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Yizheng Xinyuan New Material Technology Co ltd
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Yizheng Xinyuan New Material Technology Co ltd
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Abstract

The utility model relates to the technical field of water-soluble silicone oil production, and discloses a cooling device for high-viscosity silicone oil production, which comprises a reaction kettle, wherein the interior of the reaction kettle is hollow, a cooling tank is arranged outside the reaction kettle, in the utility model, after a pressure pump on a feeding pipe is started, the pressure pump can suck the silicone oil in the reaction kettle into the cooling tank through the feeding pipe, cooling liquid is arranged in the cooling tank, and when the silicone oil flows in the curved pipe, the silicone oil can continuously enter the reaction kettle and the cooling tank to carry out multiple times of backflow exchange, the cooled silicone oil can flow back into the reaction kettle through the curved pipe, then the silicone oil can take high temperature out to flow back into the cooling tank again when flowing back into the reaction kettle, thus the silicone oil in the curved pipe can absorb and offset the high temperature in the reaction kettle after the cold and heat exchange is carried out through the reaction kettle and the cooling tank for multiple times, thereby achieving the effects of quickly cooling the silicone oil and improving the production efficiency.

Description

Cooling device for production and use of high-viscosity silicone oil
Technical Field
The utility model relates to a water-soluble silicon oil production technical field especially relates to a cooling device of high viscosity silicon oil plant use.
Background
The silicone oil is generally a linear polysiloxane product which is kept in a liquid state at room temperature, and is generally divided into two types of methyl silicone oil and modified silicone oil, the most commonly used silicone oil, namely methyl silicone oil, is also called common silicone oil, all organic groups of the silicone oil are methyl, the methyl silicone oil has good chemical stability, insulativity and good hydrophobic property, and is prepared by adding water into dimethyldichlorosilane to hydrolyze to prepare a primary condensed ring body, cracking and rectifying the ring body to prepare a low ring body, then putting the ring body, a sealing agent and a catalyst together to perform telomerization to obtain a mixture with various polymerization degrees, and removing low-boiling-point substances through reduced pressure distillation to prepare the silicone oil.
The existing silicon oil needs to be heated to 600 ℃ plus 300 ℃ in a reaction kettle for reaction during production, and the temperature needs to be reduced for filling after the reaction is completed.
SUMMERY OF THE UTILITY MODEL
Technical problem to be solved
The utility model mainly solves the technical problem existing in the prior art and provides a cooling device for producing and using high-viscosity silicone oil.
(II) technical scheme
In order to achieve the above purpose, the present invention adopts the following technical scheme, a cooling device for producing and using high viscosity silicone oil, comprising a reaction kettle, wherein the interior of the reaction kettle is hollow, a cooling tank is arranged outside the reaction kettle, the cooling tank is in a circular tank shape, the interior of the cooling tank is hollow, a cooling liquid is arranged inside the cooling tank, a feed pipe is arranged between the reaction kettle and the cooling tank, the feed pipe is in a circular tubular shape, the interior of the feed pipe is hollow, the left end and the right end of the feed pipe respectively penetrate through the outer wall surfaces of the reaction kettle and the cooling tank, a curved pipe penetrates through the interior of the reaction kettle and the cooling tank, the curved pipe is in a curved tubular shape, the interior of the curved pipe is hollow, the right end of the feed pipe is fixedly connected with the left end of the curved pipe, a pressure pump is arranged inside the feed pipe, a long shaft is arranged inside the reaction kettle, the outer wall fixed mounting of major axis has the ring piece, and the ring piece is circular cyclic annular, reation kettle's inside is provided with two mirror symmetry's supporting rod, and the supporting rod is circular shaft-like, two the one end that the supporting rod deviates from each other respectively with reation kettle's internal face fixed connection, two the one end that the supporting rod is close to each other respectively with the outer wall fixed connection of ring piece, the outer wall fixed mounting of major axis has the fixed block that three equidistance was arranged, and the fixed block is rectangular block-shaped, three a side wall fixed mounting respectively that the fixed block deviates from each other has the stirring leaf, the outer wall of bent pipe runs through there is the pivot, the outer wall of major axis with the outer wall of pivot is fixed mounting respectively has the interlinkage gear.
Preferably, the two link gears are movably linked together, a round block is fixedly mounted on the outer wall surface of the rotating shaft, two mirror-symmetric driving plates are fixedly mounted on the outer wall surface of the round block on the rotating shaft, each driving plate is rectangular plate-shaped, a discharge pipe is arranged between the reaction kettle and the cooling tank, the left end and the right end of the discharge pipe respectively penetrate through the reaction kettle and the cooling tank, and a pressure pump is arranged inside the discharge pipe.
Preferably, a fixed plug is arranged in the discharge pipe, the fixed plug is circular in appearance, the outer wall surface of the fixed plug is fixedly connected with the inner wall surface of the discharge pipe, a movable plug is arranged in the discharge pipe, the outer wall surface of the movable plug is movably attached to the inner wall surface of the discharge pipe, a feed chute is formed in the right end of the movable plug, and the feed chute is in the shape of an oval chute.
Preferably, the left end of the fixed plug is provided with two circular grooves which are in mirror symmetry, the two circular grooves are internally provided with springs respectively, the right ends of the two springs are fixedly connected with the right wall surfaces of the two circular grooves respectively, and the left ends of the two springs are fixedly connected with the right end of the movable plug respectively.
Preferably, the left end of the fixed plug is provided with two mirror symmetry through holes, the through holes are circular holes, the right end of the movable plug is fixedly provided with two sealing blocks corresponding to the two through holes, and the outer wall surfaces of the two sealing blocks are respectively in sealing fit with the inner wall surfaces of the two through holes.
Advantageous effects
The utility model provides a cooling device of high viscosity silicone oil plant use. The method has the following beneficial effects:
(1) the cooling device for producing the high-viscosity silicone oil is characterized in that after a pressure pump on a feeding pipe is started, the pressure pump can suck the silicone oil in a reaction kettle into a cooling tank through the feeding pipe, cooling liquid is arranged in the cooling tank, and the silicone oil flows in the curved pipe, the silicone oil can continuously enter the reaction kettle and the cooling tank to carry out backflow exchange for many times, when the high-temperature silicone oil enters the cooling tank, the high-temperature silicone oil can be cooled by the cooling liquid in the cooling tank, the cooled silicone oil can flow back into the reaction kettle through the curved pipe, at the moment, the high temperature is taken out and flows back into the cooling tank again when the cooled silicone oil flows back into the reaction kettle, so that the high temperature in the reaction kettle can be absorbed and offset after the silicone oil passes through the reaction kettle and the cooling tank for many times to realize quick cooling of the silicone oil, the production efficiency is improved.
(2) This cooling device that high viscosity silicon oil plant use will contact with the drive board when silicon oil flows at bent shape inside round trip, two drive boards will rotate under the extrusion of bent shape inside silicon oil, and the epaxial linking gear of pivot and the epaxial movable joint of linking gear of major axis, at this moment the pivot just can drive the major axis and rotate, at this moment the stirring leaf just can stir inside reation kettle under the drive of major axis to reach the effect that reduces silicon oil self temperature with higher speed.
(3) This cooling device that high viscosity silicon oil plant use, silicon oil when the inside of discharging pipe is when flowing, at this moment the discharging pipe can be through-hole extrusion activity stopper, at this moment silicon oil can get into inside the reation kettle through the feed chute on the activity stopper, after the inside silicon oil temperature of reation kettle reduces, force pump on the inlet pipe just can seal to the inlet pipe is inside, prevent that inside silicon oil of reation kettle from getting into the cooling can inside here, after the inside whole reation kettle that flows in of silicon oil of bent shape intraduct, at this moment force pump on the discharging pipe just can stop, silicon oil when the discharging pipe is inside will flow back under no bulldozing force, at this moment the activity is pushed down to fixed stopper under the extrusion of silicon oil backward flow, sealed piece just can with the sealed laminating of through-hole, thereby reach and prevent that the discharging pipe is inside to leave the incomplete material, make things convenient next time use's effect.
Drawings
FIG. 1 is an overall structure diagram of the present invention;
FIG. 2 is an enlarged view of A in FIG. 1 according to the present invention;
FIG. 3 is a partial schematic view of the discharge tube of the present invention.
Illustration of the drawings:
1. a reaction kettle; 2. a cooling tank; 3. a feed pipe; 4. a curved tube; 5. a pressure pump; 6. a long axis; 7. a ring block; 8. a clamping rod; 9. a fixed block; 10. stirring blades; 11. a rotating shaft; 12. a link gear; 13. driving the plate; 14. a discharge pipe; 15. a fixed plug; 16. a movable plug; 17. a feed chute; 18. a circular groove; 19. a spring; 20. a through hole; 21. and (6) sealing the block.
Detailed Description
The technical solution of the present invention is further described in detail by the following embodiments with reference to the accompanying drawings.
Example (b): a cooling device for producing high-viscosity silicone oil is shown in figures 1-3, and comprises a reaction kettle 1, wherein the reaction kettle 1 is of an existing structure, details are not described herein, the interior of the reaction kettle 1 is hollow, a cooling tank 2 is arranged outside the reaction kettle 1, the cooling tank 2 is in a round tank shape, the interior of the cooling tank 2 is hollow, cooling liquid is arranged inside the cooling tank 2, a feeding pipe 3 is arranged between the reaction kettle 1 and the cooling tank 2, the feeding pipe 3 is in a round tubular shape, the interior of the feeding pipe 3 is hollow, the left end and the right end of the feeding pipe 3 respectively penetrate through the outer wall surfaces of the reaction kettle 1 and the cooling tank 2, a curved pipe 4 penetrates through the interior of the reaction kettle 1 and the cooling tank 2, the curved pipe 4 is in a curved tubular shape, the interior of the curved pipe 4 is hollow, the right end of the feeding pipe 3 is fixedly connected with the left end of the curved pipe 4, a pressure pump 5 is arranged inside the feeding pipe 3, the pressure pump 5 is of a conventional structure, which is not described herein, a long shaft 6 is arranged inside the reaction kettle 1, a ring block 7 is fixedly arranged on the outer wall surface of the long shaft 6, the ring block 7 is circular ring-shaped, two clamping rods 8 which are mirror-symmetrical are arranged inside the reaction kettle 1, the clamping rods 8 are circular rod-shaped, the ends of the two clamping rods 8 which are away from each other are fixedly connected with the inner wall surface of the reaction kettle 1 respectively, the ends of the two clamping rods 8 which are close to each other are fixedly connected with the outer wall surface of the ring block 7 respectively, three fixed blocks 9 which are arranged at equal intervals are fixedly arranged on the outer wall surface of the long shaft 6, the fixed blocks 9 are rectangular block-shaped, stirring blades 10 are fixedly arranged on the side wall surfaces of the three fixed blocks 9 which are away from each other respectively, a rotating shaft 11 penetrates through the outer wall surface of the curved pipe 4, linking gears 12 are fixedly arranged on the outer wall surfaces of the long shaft 6 and the rotating shaft 11 respectively, and the two linking gears 12 are movably linked together, the outer wall surface of the rotating shaft 11 is fixedly provided with a round block, the outer wall surface of the round block on the rotating shaft 11 is fixedly provided with two mirror symmetry driving plates 13, the driving plates 13 are rectangular plate-shaped, a discharge pipe 14 is arranged between the reaction kettle 1 and the cooling tank 2, the left end and the right end of the discharge pipe 14 respectively penetrate through the reaction kettle 1 and the cooling tank 2, a pressure pump 5 is arranged inside the discharge pipe 14, a fixed plug 15 is arranged inside the discharge pipe 14, the fixed plug 15 is circular in appearance, the outer wall surface of the fixed plug 15 is fixedly connected with the inner wall surface of the discharge pipe 14, a movable plug 16 is arranged inside the discharge pipe 14, the outer wall surface of the movable plug 16 is movably attached to the inner wall surface of the discharge pipe 14, the right end of the movable plug 16 is provided with a feed groove 17, the feed groove 17 is in the shape of an oval groove, the left end of the fixed plug 15 is provided with two mirror symmetry round grooves 18, springs 19 are respectively arranged inside the two round grooves 18, and the right ends of the two springs 19 are respectively fixedly connected with the inner right wall surface of the two round grooves 18, the left ends of the two springs 19 are fixedly connected with the right end of the movable plug 16, the left end of the fixed plug 15 is provided with two mirror symmetry through holes 20, the through holes 20 are circular holes, the right end of the movable plug 16 is fixedly provided with two sealing blocks 21 corresponding to the two through holes 20, and the outer wall surfaces of the two sealing blocks 21 are in sealing fit with the inner wall surfaces of the two through holes 20 respectively.
The utility model discloses a theory of operation: when in use, after the silicon oil in the reaction kettle 1 is heated at high temperature for reaction, at this time, the pressure pump 5 is started to enable the high-temperature silicon oil in the reaction kettle 1 to be sucked into the curved pipe 4, at this time, the silicon oil in the reaction kettle 1 flows between the reaction kettle 1 and the cooling tank 2 through the curved pipe 4, when the silicon oil in the curved pipe 4 enters the cooling tank 2, the silicon oil in the cooling tank 2 can cool the silicon oil in the curved pipe 4, when the silicon oil flows in the curved pipe 4, the silicon oil flows into contact with the driving plates 13, the two driving plates 13 rotate under the extrusion of the silicon oil in the curved pipe 4, at this time, the linking gear 12 on the rotating shaft 11 can drive the linking gear 12 outside the long shaft 6 to rotate, at this time, the stirring blades 10 can stir in the reaction kettle 1 under the drive of the long shaft 6, so as to enable the silicon oil in the reaction kettle 1 to dissipate heat and cool rapidly, after the temperature of the silicone oil in the reaction kettle 1 is reduced, at this time, when the silicone oil in the curved pipe 4 completely flows into the reaction kettle 1 through the discharge pipe 14, the movable plug 16 in the discharge pipe 14 moves leftwards under the extrusion of the silicone oil, at this time, the silicone oil can enter the reaction kettle 1 through the through hole 20 and the feed chute 17, the pressure pump 5 on the discharge pipe 14 stops, at this time, when the silicone oil presses the movable plug 16 in a backflow manner, the movable plug 16 moves rightwards under the extrusion of the silicone oil and the elasticity of the spring 19 to be attached to the fixed plug 15, and the through hole 20 is sealed by the two sealing blocks 21.
The basic principles and main features of the present invention, i.e. the advantages of the present invention, have been shown and described above. It will be understood by those skilled in the art that the present invention is not limited to the above embodiments, and that the foregoing embodiments and descriptions are provided only to illustrate the principles of the present invention without departing from the spirit and scope of the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (6)

1. The utility model provides a cooling device that high viscosity silicone oil production was used, includes reation kettle (1), its characterized in that: the cooling tank (2) is arranged outside the reaction kettle (1), cooling liquid is arranged inside the cooling tank (2), an inlet pipe (3) is arranged between the reaction kettle (1) and the cooling tank (2), a curved pipe (4) penetrates through the reaction kettle (1) and the cooling tank (2), a pressure pump (5) is arranged inside the inlet pipe (3), a long shaft (6) is arranged inside the reaction kettle (1), a ring block (7) is fixedly arranged on the outer wall surface of the long shaft (6), two clamping rods (8) with mirror symmetry are arranged inside the reaction kettle (1), three fixing blocks (9) which are arranged at equal intervals are fixedly arranged on the outer wall surface of the long shaft (6), stirring blades (10) are fixedly arranged on one side wall surface of the fixing blocks (9) which deviate from each other respectively, and a rotating shaft (11) penetrates through the outer wall surface of the curved pipe (4), outer wall fixed mounting of pivot (11) has the disk, disk outer wall fixed mounting in pivot (11) has driving plate (13) of two mirror symmetry, be provided with discharging pipe (14) between reation kettle (1) and cooling tank (2), inside pressure pump (5) that is provided with of discharging pipe (14), discharging pipe (14) inside is provided with fixed stopper (15), and feed chute (17) have been seted up to the right-hand member of movable stopper (16), circular slot (18) of two mirror symmetry are seted up to the left end of fixed stopper (15), two the inside of circular slot (18) is provided with spring (19) respectively, through-hole (20) of two mirror symmetry are seted up to the left end of fixed stopper (15), the right-hand member fixed mounting of movable stopper (16) has two and two sealed piece (21) that through-hole (20) correspond to each other.
2. The cooling device for producing high-viscosity silicone oil according to claim 1, wherein: the left end and the right end of the inlet pipe (3) penetrate through the outer wall surface of the reaction kettle (1) and the outer wall surface of the cooling tank (2) respectively, and the right end of the inlet pipe (3) is fixedly connected with the left end of the curved pipe (4).
3. The cooling device for producing high-viscosity silicone oil according to claim 1, wherein: one ends of the two clamping rods (8) which deviate from each other are fixedly connected with the inner wall surface of the reaction kettle (1) respectively, and one ends of the two clamping rods (8) which are close to each other are fixedly connected with the outer wall surface of the ring block (7) respectively.
4. The cooling device for producing high-viscosity silicone oil according to claim 1, wherein: the outer wall surface of major axis (6) with the outer wall surface of pivot (11) is fixed mounting respectively has linking gear (12), two linking gear (12) active link is in the same place, both ends run through respectively about discharging pipe (14) reation kettle (1) and cooling tank (2).
5. The cooling device for producing high-viscosity silicone oil according to claim 1, wherein: the outer wall surface of the fixed plug (15) is fixedly connected with the inner wall surface of the discharge pipe (14), a movable plug (16) is arranged inside the discharge pipe (14), and the outer wall surface of the movable plug (16) is movably attached to the inner wall surface of the discharge pipe (14).
6. The cooling device for producing high-viscosity silicone oil according to claim 1, wherein: the right ends of the two springs (19) are fixedly connected with the right wall surfaces of the inner parts of the two circular grooves (18) respectively, the left ends of the two springs (19) are fixedly connected with the right end of the movable plug (16) respectively, and the outer wall surfaces of the two sealing blocks (21) are in sealing fit with the inner wall surfaces of the two through holes (20) respectively.
CN202022602284.5U 2020-11-11 2020-11-11 Cooling device for production and use of high-viscosity silicone oil Active CN214199384U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202022602284.5U CN214199384U (en) 2020-11-11 2020-11-11 Cooling device for production and use of high-viscosity silicone oil

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Application Number Priority Date Filing Date Title
CN202022602284.5U CN214199384U (en) 2020-11-11 2020-11-11 Cooling device for production and use of high-viscosity silicone oil

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118615989A (en) * 2024-08-09 2024-09-10 福建瑞森新材料股份有限公司 Reaction kettle for preparing zirconium phosphate modified compound and preparation method based on reaction kettle

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118615989A (en) * 2024-08-09 2024-09-10 福建瑞森新材料股份有限公司 Reaction kettle for preparing zirconium phosphate modified compound and preparation method based on reaction kettle
CN118615989B (en) * 2024-08-09 2024-10-29 福建瑞森新材料股份有限公司 Reaction kettle for preparing zirconium phosphate modified compound and preparation method based on reaction kettle

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