CN111000288A - Gel for cigarettes and tobacco products - Google Patents
Gel for cigarettes and tobacco products Download PDFInfo
- Publication number
- CN111000288A CN111000288A CN201911394392.3A CN201911394392A CN111000288A CN 111000288 A CN111000288 A CN 111000288A CN 201911394392 A CN201911394392 A CN 201911394392A CN 111000288 A CN111000288 A CN 111000288A
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- China
- Prior art keywords
- parts
- essence
- polyethylene glycol
- gel
- ice
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 69
- 235000019505 tobacco product Nutrition 0.000 title claims description 14
- 239000000203 mixture Substances 0.000 claims abstract description 46
- 239000011159 matrix material Substances 0.000 claims abstract description 31
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 24
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 23
- 239000000463 material Substances 0.000 claims abstract description 14
- 150000004676 glycans Chemical class 0.000 claims abstract description 8
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 8
- 239000005017 polysaccharide Substances 0.000 claims abstract description 8
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims abstract description 7
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000001630 malic acid Substances 0.000 claims abstract description 7
- 235000011090 malic acid Nutrition 0.000 claims abstract description 7
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 5
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 5
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000008117 stearic acid Substances 0.000 claims abstract description 5
- 239000000796 flavoring agent Substances 0.000 claims description 56
- 235000019634 flavors Nutrition 0.000 claims description 51
- 244000269722 Thea sinensis Species 0.000 claims description 30
- 235000013616 tea Nutrition 0.000 claims description 23
- 239000003205 fragrance Substances 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 13
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims description 10
- 235000009569 green tea Nutrition 0.000 claims description 9
- 239000000341 volatile oil Substances 0.000 claims description 9
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims description 8
- SIKJAQJRHWYJAI-UHFFFAOYSA-N Indole Chemical compound C1=CC=C2NC=CC2=C1 SIKJAQJRHWYJAI-UHFFFAOYSA-N 0.000 claims description 8
- 241000207840 Jasminum Species 0.000 claims description 8
- 235000010254 Jasminum officinale Nutrition 0.000 claims description 8
- 241000208125 Nicotiana Species 0.000 claims description 8
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 8
- JBFHTYHTHYHCDJ-UHFFFAOYSA-N gamma-caprolactone Chemical compound CCC1CCC(=O)O1 JBFHTYHTHYHCDJ-UHFFFAOYSA-N 0.000 claims description 8
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims description 8
- KVWWIYGFBYDJQC-UHFFFAOYSA-N methyl dihydrojasmonate Chemical compound CCCCCC1C(CC(=O)OC)CCC1=O KVWWIYGFBYDJQC-UHFFFAOYSA-N 0.000 claims description 8
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 7
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 7
- 229940041616 menthol Drugs 0.000 claims description 7
- 229940093430 polyethylene glycol 1500 Drugs 0.000 claims description 7
- 229940057838 polyethylene glycol 4000 Drugs 0.000 claims description 7
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims description 6
- -1 hexanoic acid leaf alcohol ester Chemical class 0.000 claims description 6
- NFLGAXVYCFJBMK-RKDXNWHRSA-N (+)-isomenthone Natural products CC(C)[C@H]1CC[C@@H](C)CC1=O NFLGAXVYCFJBMK-RKDXNWHRSA-N 0.000 claims description 5
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims description 5
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims description 5
- NFLGAXVYCFJBMK-UHFFFAOYSA-N Menthone Chemical compound CC(C)C1CCC(C)CC1=O NFLGAXVYCFJBMK-UHFFFAOYSA-N 0.000 claims description 5
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims description 5
- 229930007503 menthone Natural products 0.000 claims description 5
- 235000019477 peppermint oil Nutrition 0.000 claims description 5
- 229940113116 polyethylene glycol 1000 Drugs 0.000 claims description 5
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims description 4
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims description 4
- JGBBQKAJVHEQJM-FNORWQNLSA-N (e)-1-(2,6,6-trimethylcyclohexa-2,4-dien-1-yl)but-2-en-1-one Chemical compound C\C=C\C(=O)C1C(C)=CC=CC1(C)C JGBBQKAJVHEQJM-FNORWQNLSA-N 0.000 claims description 4
- WWZKQHOCKIZLMA-UHFFFAOYSA-N Caprylic acid Natural products CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 4
- IMKHDCBNRDRUEB-UHFFFAOYSA-N Dihydroactinidiolide Natural products C1CCC(C)(C)C2=CC(=O)OC21C IMKHDCBNRDRUEB-UHFFFAOYSA-N 0.000 claims description 4
- XMLSXPIVAXONDL-PLNGDYQASA-N Jasmone Chemical compound CC\C=C/CC1=C(C)CCC1=O XMLSXPIVAXONDL-PLNGDYQASA-N 0.000 claims description 4
- UZFLPKAIBPNNCA-BQYQJAHWSA-N alpha-ionone Chemical compound CC(=O)\C=C\C1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-BQYQJAHWSA-N 0.000 claims description 4
- UZFLPKAIBPNNCA-UHFFFAOYSA-N alpha-ionone Natural products CC(=O)C=CC1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-UHFFFAOYSA-N 0.000 claims description 4
- IVLCENBZDYVJPA-ARJAWSKDSA-N cis-Jasmone Natural products C\C=C/CC1=C(C)CCC1=O IVLCENBZDYVJPA-ARJAWSKDSA-N 0.000 claims description 4
- 239000001926 citrus aurantium l. subsp. bergamia wright et arn. oil Substances 0.000 claims description 4
- IMKHDCBNRDRUEB-LLVKDONJSA-N dihydroactinidiolide Chemical compound C1CCC(C)(C)C2=CC(=O)O[C@@]21C IMKHDCBNRDRUEB-LLVKDONJSA-N 0.000 claims description 4
- 239000010648 geranium oil Substances 0.000 claims description 4
- 235000019717 geranium oil Nutrition 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- PZOUSPYUWWUPPK-UHFFFAOYSA-N indole Natural products CC1=CC=CC2=C1C=CN2 PZOUSPYUWWUPPK-UHFFFAOYSA-N 0.000 claims description 4
- RKJUIXBNRJVNHR-UHFFFAOYSA-N indolenine Natural products C1=CC=C2CC=NC2=C1 RKJUIXBNRJVNHR-UHFFFAOYSA-N 0.000 claims description 4
- 150000002576 ketones Chemical class 0.000 claims description 4
- 229930007744 linalool Natural products 0.000 claims description 4
- FUZZWVXGSFPDMH-UHFFFAOYSA-N n-hexanoic acid Natural products CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- XMLSXPIVAXONDL-UHFFFAOYSA-N trans-jasmone Natural products CCC=CCC1=C(C)CCC1=O XMLSXPIVAXONDL-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000002304 perfume Substances 0.000 claims description 3
- 235000019445 benzyl alcohol Nutrition 0.000 claims description 2
- 235000015165 citric acid Nutrition 0.000 claims description 2
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims description 2
- 241001122767 Theaceae Species 0.000 abstract 1
- 239000000686 essence Substances 0.000 description 45
- 230000000052 comparative effect Effects 0.000 description 24
- 239000000243 solution Substances 0.000 description 23
- 238000002347 injection Methods 0.000 description 16
- 239000007924 injection Substances 0.000 description 16
- 239000000779 smoke Substances 0.000 description 16
- 230000000391 smoking effect Effects 0.000 description 10
- 238000009472 formulation Methods 0.000 description 8
- 230000000694 effects Effects 0.000 description 6
- 235000013355 food flavoring agent Nutrition 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 5
- 235000009508 confectionery Nutrition 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 235000019198 oils Nutrition 0.000 description 4
- 229920000747 poly(lactic acid) Polymers 0.000 description 4
- 239000004626 polylactic acid Substances 0.000 description 4
- 239000003571 electronic cigarette Substances 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 230000007794 irritation Effects 0.000 description 3
- 239000000049 pigment Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000005096 rolling process Methods 0.000 description 3
- 235000013599 spices Nutrition 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 206010013911 Dysgeusia Diseases 0.000 description 2
- 239000004743 Polypropylene Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229920001155 polypropylene Polymers 0.000 description 2
- 230000035807 sensation Effects 0.000 description 2
- 235000019615 sensations Nutrition 0.000 description 2
- 238000009210 therapy by ultrasound Methods 0.000 description 2
- 229920006221 acetate fiber Polymers 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 230000035597 cooling sensation Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 239000005454 flavour additive Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 230000001339 gustatory effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000036314 physical performance Effects 0.000 description 1
- 230000001902 propagating effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/022—Applying additives to filter materials with liquid additives, e.g. application of plasticisers
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
- A24D1/045—Cigars; Cigarettes with mouthpieces or filter-tips with smoke filter means
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Manufacture Of Tobacco Products (AREA)
- Fats And Perfumes (AREA)
Abstract
A gel composition for cigarettes comprises 50-97 wt% of gel matrix and 3-50 wt% of essence solution; the gel matrix comprises the following components: 36-81 parts of polyethylene glycol material; 24-48 parts of stearic acid; 2-9 parts of tea polysaccharide; 0.8-1 part by weight of malic acid; and 0.7-1.1 parts by weight of citric acid.
Description
Technical Field
The invention belongs to the field of essences, and particularly relates to a gel for cigarettes and a tobacco product.
Background
The essence and spice can cover the defects of the tobacco, improve the fragrance and the taste of the tobacco and improve the physical performance of the tobacco in the cigarette, and can endow the cigarette with unique taste and style and realize quality differentiation. The method has the advantages that the aroma quality of cigarette smoking is stabilized, the formation of cigarette style and quality is greatly influenced, and the method is also the key for highlighting and propagating the style characteristics of cigarette brands and expanding and developing the cigarette brands. At present, essence and spice are mainly added into tobacco shreds, the cigarette fragrance is increased by burning the essence and spice along with the tobacco shreds in the smoking process, or essence particles or essence capsules are directly added into cigarette filter sticks to increase the fragrance, but the cigarette fragrance increasing methods generally have the defects of uneven fragrance release, short storage time, poor compatibility with smoke, heavy miscellaneous gas and the like, and the fragrance improving effect is not ideal.
The gel is a good perfume-locking material, the melted glue solution is mixed with essence, and the gel can lock the essence after the normal temperature is recovered. The gel containing the essence is added into the cigarette filter stick, and when a consumer smokes the cigarette, the gel in the cigarette filter stick is melted into liquid under the influence of the smoke temperature, so that the aroma of the essence is released. However, researches find that the cigarette products added with the essence-containing gel in the existing cigarette filter stick generally have the problems of heavy oil smell, inconsistent cigarette fragrance, poor smoking taste and the like during smoking.
Therefore, there is a need for a gel composition for cigarettes for use in cigarette filter rods that improves the sensory quality of cigarette smoking.
Disclosure of Invention
The inventor finds that the addition of tea polysaccharide: malic acid: 2-9% of citric acid: 0.5-1.2: 0.7-1.2' of flavoring agent, wherein the flavoring additive has a coordinated sweet and sour feeling and can effectively eliminate the smell of oil in the gel for cigarettes. The cigarette gel containing the flavoring agent is used for tobacco products, and can reduce smoke irritation and make smoke have sweet and moist feeling.
Furthermore, the cigarette gel containing the flavoring agent preferably contains the ice-feeling matcha flavor, the cigarette gel with the coordinated sweet and sour feeling is matched with the ice-feeling matcha flavor, the layering sense of the ice-feeling matcha flavor is effectively enhanced and enriched, smoke has pleasant 'ice feeling' and obvious 'matcha flavor', and the excellent taste and smell enjoyment is brought to consumers.
The invention relates to a gel composition for cigarettes, which comprises 50-97 wt% (such as 60-80 wt%, such as 70-90 wt%, such as 55-97%) of a gel matrix and 3-50 wt% (such as 3-45%, such as 20-40 wt%, such as 10-30 wt%) of a essence solution;
the gel matrix comprises the following components:
in some embodiments, the gel matrix comprises the following components in percent by weight, based on the total weight of the gel matrix:
in some embodiments, the sum of the weight percentages of the components making up the gel matrix is 100 wt%.
In some embodiments, the gel matrix is a composition of:
in some embodiments, the gel matrix comprises the following components in percent by weight, based on the total weight of the gel matrix:
in some embodiments, the polyethylene glycol material is a polyethylene glycol having an average molecular weight in the range of 750 to 12000 (e.g., in the range of 1000 to 10000).
In some embodiments, the polyethylene glycol material is selected from one or more of polyethylene glycol 1000, polyethylene glycol 1500, polyethylene glycol 4000, polyethylene glycol 10000.
In some embodiments, the weight ratio of polyethylene glycol 1000, polyethylene glycol 1500, polyethylene glycol 4000 and polyethylene glycol 10000 in the polyethylene glycol material is 8-12: 8-12: 8-12: 8-12, for example 9-11: 9-11: 9-11: 9 to 11.
In some embodiments, the flavor solution is an ice-feel matcha flavor solution.
In some embodiments, the ice-sensitive matcha flavor solution comprises an ice-sensitive matcha flavor and a solvent.
Wherein the ice feeling matcha flavor essence contains the following aroma components in parts by weight:
4.59 to 5.61 parts of ice-feeling essence;
1.75-2.15 parts of jasmine essence;
0.49-0.61 part of flower fragrance essence;
0.32 to 0.40 portion of tea essence; and
0.08 to 0.11 portion of auxiliary essence;
wherein,
the ice essence is selected from one or more of peppermint oil, menthol, menthone and menthyl acetate;
the jasmine essence is selected from one or more of jasmine essential oil, methyl dihydrojasmonate, cis-jasmone and phenethyl alcohol;
the floral essence is selected from one or more of geranium oil, bergamot oil, hexanoic acid leaf alcohol ester, α -ionone, α -damascenone;
the tea essence is selected from one or more of linalool, tea scented ketone, indole, benzyl alcohol, tea scented spirane, and Tieguanyin tea leaf essential oil;
the auxiliary essence is one or more selected from dihydroactinidiolide, gamma-caprolactone and peru extract.
In some embodiments, the ice-feel matcha flavor essence contains the following ingredients in parts by weight:
0.675-0.825 parts of peppermint oil;
2.7-3.3 parts of menthol;
0.54-0.66 parts of menthone;
0.675 to 0.825 parts of menthyl acetate;
0.27-0.33 parts of jasmine essential oil;
0.54-0.66 parts of methyl dihydrojasmonate;
0.405-0.495 parts of cis-jasmone;
0.54-0.66 parts of phenethyl alcohol;
0.135-0.165 parts of geranium oil;
0.27-0.33 parts of bergamot oil;
0.0675-0.0825 parts of hexanoic acid leaf alcohol ester;
0.0135-0.0165 part of α -ionone;
0.00675-0.00825 parts of α -damascenone;
0.135-0.165 parts of linalool;
0.0675-0.0825 parts of tea scented ketone;
0.027-0.033 parts of indole;
0.0675-0.0825 parts of benzyl alcohol;
0.0135-0.0165 parts of tea-scented spirane;
0.0135-0.0165 parts of Tieguanyin essential oil;
0.054-0.066 parts of dihydroactinidiolide;
0.027-0.033 parts of gamma-caprolactone; and
0.00675-0.00825 parts of Peru extract.
In some embodiments, the concentration of ice-sensitive matcha flavor in the ice-sensitive matcha flavor solution is 5 to 15 wt%, such as 8 to 12 wt%, based on the total weight of the ice-sensitive matcha flavor solution.
In some embodiments, the balance of the ice-feel matcha flavor essence solution is solvent.
In some embodiments, the solvent is propylene glycol.
In some embodiments, the gel composition for cigarettes may also contain a pigment (e.g., a food pigment). Based on the method, a colorful gel product can be obtained, so that the appearance of the product is enriched. Therefore, the gel not only can be used as a storage carrying substance of essence, but also has the functions of beautifying the filter stick and preventing counterfeiting.
In some embodiments, the gel composition for cigarette contains 3 to 50 wt% of the ice-sensitive green tea flavor solution. If the proportion of the essence is too high, the coagulation performance of the flavored gel is poor, and if the proportion of the essence is too low, the content of effective aroma components added into the filter stick is low, and the aroma concentration required by the design cannot be achieved.
In some aspects, there is provided a method of preparing a gel comprising the steps of:
(1) heating and melting a polyethylene glycol material and stearic acid according to the formula of the gel composition for the cigarettes, and mixing to obtain a mixture;
optionally, propylene glycol is also added;
(2) citric acid, malic acid, tea polysaccharide and a perfume solution were added to the mixture.
In some embodiments, the flavor solution is an ice-feel matcha flavor solution.
In some aspects, there is provided a method of preparing the above ice-feeling matcha flavor gel, comprising the steps of:
1) according to the formula of the ice-feeling matcha essence, the menthol, the peru extract, the tea spirane and the Tieguanyin tea essential oil are put into a closed container, water is added, the container is placed on an ultrasonic oscillator, and ultrasonic treatment is carried out under the condition of water bath at 6-10 ℃ until all the components are uniformly mixed;
2) and adding the rest formula components in the formula into the product obtained in the last step, and stirring uniformly under the water bath condition of 5-10 ℃ to obtain the ice taste matcha flavor essence solution.
In some aspects, there is provided the use of the above-described gel composition for use in the preparation of a tobacco product (e.g., a filter portion of a cigarette).
In some aspects, a filter rod for tobacco products is provided, wherein the gel composition for the cigarette is arranged in the filter rod
In some embodiments, the gel composition for cigarettes is in the form of a strip, the strip of gel composition is located within the filter rod, and the length direction of the strip of gel composition is parallel to the length direction of the filter rod.
In some aspects, there is provided a method of making a filter rod as described above, comprising the steps of:
according to the composition formula of the gel matrix, mixing the raw materials, heating to melt, adding the ice-feeling matcha flavor to obtain a flowing gel composition for the cigarettes;
in the process of rolling the filter stick, injecting a flowing gel composition for cigarettes into the center of the filter stick, so that the flowing gel is solidified in the filter stick to form solid strip-shaped gel, wherein the length direction of the gel is parallel to the length direction of the filter stick.
In some embodiments, the method of making a filter rod comprises: heating the gel to 50-100 ℃, completely melting the gel, slowly adding the ice-feeling green tea essence, uniformly stirring under a sealed condition, connecting the gel with a horn mouth of a filter stick forming machine through gel fragrance injection equipment, and adding the flavored gel into the filter stick in the filter stick forming process.
In some embodiments, the flavor injection device can be directly connected with the filter stick machine, and gel is injected into the center of the filter stick by the flavor injection device during the rolling process of the filter stick, and the gel is solidified after being cooled.
In some practical applications, the injection holes of the fragrance injection equipment are circular, triangular, quadrilateral, pentagram-shaped, regular hexagon and the like, and the injection holes with different shapes can change the shape of the gel after being added into the filter stick, thereby enriching the appearance of the product.
In some embodiments, the solidified gel accounts for 5-10% of the total cross section of the filter stick, too low a proportion can result in too low injected gel aroma substances, and too high a proportion can result in too high suction resistance of the filter stick.
In some embodiments, the gel-containing filter rod has a diameter of 4.50 to 7.70mm and a pressure drop of 2550 and 4050 Pa.
In some embodiments, the effective amount of ice-sensitive green tea flavor added to a single filter rod is from 5mg to 30 mg.
In some embodiments, the material of the filter rod is selected from one or more of a cellulose acetate filter rod, a polylactic acid fiber (PLA) filter rod or a polypropylene filter rod. The filter stick material is a filter material used in the existing cigarette filter tip, and can be produced by using the existing filter stick equipment.
In some aspects, a tobacco product is provided, comprising a filter rod as described above.
In some embodiments, the smoking article may be a burning cigarette, a heat non-burning cigarette, as it were, or an electronic cigarette.
Description of terms:
the term "burning cigarette" refers to a type of tobacco product in which the cigarette remains lit during use.
The term "heated non-burning cigarette" refers to a type of tobacco product in which the cigarette remains heated but not lit during use.
The term "electronic cigarette" refers to a type of tobacco product that, when in use, generates an aerosol by atomizing an electronic cigarette liquid.
The term "perfume" refers to a pure substance or composition capable of having a fragrance.
The term polyethylene glycol 1000 refers to polyethylene glycol having an average molecular weight in the range of 850 to 1150.
The term polyethylene glycol 1500 refers to polyethylene glycols having an average molecular weight in the range of 1200 to 1600.
The term polyethylene glycol 4000 refers to polyethylene glycol having an average molecular weight in the range of 3500 to 4500.
The term polyethylene glycol 10000 refers to polyethylene glycol having an average molecular weight in the range of 8500 to 11500.
The term "ice feel" refers to the cooling sensation imparted to the flavor by peppermint oil, menthol, menthone, menthyl acetate, or a combination thereof, including a cooling olfactory sensation and/or a cooling gustatory sensation.
Advantageous effects
The essence or the cigarette has the following beneficial effects:
1) the cigarette gel added with the flavoring agent can effectively eliminate the smell of oil in the cigarette gel;
2) the cigarette gel added with the flavoring agent and the ice-feeling matcha flavor has pleasant ice feeling and obvious matcha flavor, and the flavor of the cigarette gel is coordinated with the smoke of the tobacco, so that the smoke has no smell of wood gas, earthy smell and the like, and has no stimulation to mouth, nose and throat and dry feeling;
3) the aroma loss of the gel for the cigarette is slow in the storage process, and the aroma release is fast in the smoking process;
4) can reduce the heat of smoke, enrich the appearance of the product, have the anti-counterfeiting function and ensure that the tobacco product has comfortable flavor of opening the package.
Detailed Description
The technical solution of the present invention is further described in detail by the following examples. The exemplary embodiments of the present invention and the description thereof are provided for the purpose of explanation and are not to be construed as limiting the invention.
The flavors and fragrances used in the examples were provided by the tobacco industry, llc in fujian.
Examples 1 to 3
The ice-feeling green tea flavor solutions of examples 1 to 3 were each No. a1 to A3, and the formulations are shown in table 3.
The preparation method of the essence solution comprises the following steps:
1) according to the formula of the ice-feeling matcha flavor essence solution, putting menthol, peru extract, tea spirane and Tieguanyin tea essence oil into a closed container, adding water, placing on an ultrasonic oscillator, and performing ultrasonic treatment under the condition of water bath at 8 ℃ until all the components are uniformly mixed;
3) adding the rest raw materials into the product of the last step, and stirring uniformly by using a spiral stirrer under the condition of water bath at 7 ℃ to obtain the ice taste matcha flavor;
4) storing at 5 ℃ for later use.
The formulations of the gel matrices of examples 1 to 3 are shown in Table 1. The preparation method of the ice-feeling matcha flavor gel filter stick of the embodiments 1 to 3 is as follows:
according to the formula of the gel matrix components in the table 1, the matrix raw materials are mixed and heated to be completely melted, the ice-feeling green tea flavor is added into the mixture, and the mixture is uniformly stirred under the sealed condition, so that the flowing state fragrant gel is obtained. And (3) connecting the gel fragrance injection equipment with a horn mouth of a filter stick forming machine, and adding the flowing gel into the filter stick in the filter stick forming process.
In example 1, the mass ratio of the essence solution to the gel matrix is 1: 30, of a nitrogen-containing gas; the essence content in a single filter stick is 5mg, an injection hole of the essence injection equipment is circular, the filter stick is made of acetate fiber, the diameter of the filter stick after gel injection is 4.50mm, and the pressure drop is 2550 Pa.
In example 2, the mass ratio of the essence solution to the gel matrix is 1: 2.5; the essence content in a single filter stick is 20mg, an injection hole of the essence injection equipment is circular, the filter stick is made of polypropylene fiber, the diameter of the filter stick after gel injection is 6.0mm, and the pressure drop is 3430 Pa.
In example 3, the mass ratio of the essence solution to the gel matrix is 1: 1; the essence content in a single filter stick is 35mg, the injection hole of the essence injection equipment is circular, the filter stick material is polylactic acid fiber, the diameter of the filter stick after gel injection is 7.70mm, and the pressure drop is 4050 Pa.
TABLE 1 gel base formulation
| Matrix material | Example 1 | Example 2 | Example 3 |
| Stearic acid | 47.62％ | 30.49％ | 24.60％ |
| 1000 of polyethylene glycol | 11.90％ | 15.24％ | 16.39％ |
| Polyethylene glycol 1500 | 11.90％ | 15.24％ | 16.39％ |
| Polyethylene glycol 4000 | 11.90％ | 15.24％ | 16.39％ |
| Polyethylene glycol 10000 | 11.90％ | 15.24％ | 16.39％ |
| Tea polysaccharide | 2.38％ | 6.71％ | 8.20％ |
| Malic acid | 1.20％ | 0.92％ | 0.82％ |
| Citric acid | 1.20％ | 0.92％ | 0.82％ |
Comparative examples 1 to 3
The ice-feeling green tea flavor solutions of comparative examples 1 to 3 were numbered B1 to B3.
The formulations of the ice-sensitive green tea flavor solutions of comparative examples 1 to 3 are shown in table 3.
Comparative example 1 differs from example 1 only in the ice taste matcha flavor, and the ice taste matcha flavor of comparative example 1 is numbered B1. Comparative example 1 is the same gel matrix as example 1.
Comparative example 2 differs from example 2 only in the ice taste matcha flavor, and the ice taste matcha flavor of comparative example 2 is numbered B2. Comparative example 2 is the same gel matrix as example 2.
Comparative example 3 differs from example 3 only in the ice taste spatula flavour, which is the ice taste spatula flavour of comparative example 3 with the code B3. Comparative example 3 is the same gel matrix as example 3.
Comparative examples 4 to 6
Comparative example 4 differs from example 2 only in the formulation of the gel matrix, which does not contain tea polysaccharide, malic acid and citric acid in the gel matrix of comparative example 4.
Comparative example 5 differs from example 2 only in the formulation of the gel matrix, which does not contain citric acid in the gel matrix of comparative example 5.
Comparative example 6 differs from example 2 only in the formulation of the gel matrix, which does not contain tea polysaccharide.
The formulation of the gel matrix of comparative examples 4-6 is shown in table 2 below:
TABLE 2
| Matrix material | Comparative example 4 | Comparative example 5 | Comparative example 6 |
| Stearic acid | 32.8％ | 30.49％ | 32.8％ |
| 1000 of polyethylene glycol | 20.2％ | 15.24％ | 20.2％ |
| Polyethylene glycol 1500 | 10.1％ | 15.24％ | 10.1％ |
| Polyethylene glycol 4000 | 18.9％ | 15.24％ | 18.9％ |
| Polyethylene glycol 10000 | 11.3％ | 15.24％ | 11.3％ |
| Tea polysaccharide | / | 7.60％ | / |
| Malic acid | / | 0.95％ | 0.92％ |
| Citric acid | / | / | 0.92％ |
| Propylene glycol | 6.7％ | / | 4.86％ |
| Edible pigment | Blue color | Blue color | Blue color |
Cigarette aroma/smoking evaluation test:
and (3) rolling the filter stick product of the embodiment into a finished cigarette by using a cigarette making machine, and adding a blank control, wherein the blank control uses a polylactic acid filter stick with the diameter of 7.70mm and does not contain the gel composition for cigarettes. Smoke evaluation is carried out respectively, the smoke evaluation results are listed in a table 4, and then grading is carried out according to GB 5606.4-2005 and is listed in a table 5.
TABLE 4 sensory Smoke evaluation
TABLE 5 sensory Smoke score
As can be seen from the data in tables 3 and 4, compared with the blank control sample, the ice-feeling matcha flavor gel of examples 1 to 3 is used for cigarettes, so that the smoking flavor effect of the cigarettes is better improved, the irritation of smoke can be reduced, the sweet feeling is added, the aftertaste is improved, the offensive odor is covered, the improvement effect on the smoke is remarkable, and the ice-feeling matcha flavor gel has a better practical value.
In addition, the essence formula of the comparative examples 1 to 3 is beyond the scope of the invention, the aroma gel is used for cigarettes, the smoking aroma of the cigarettes is not compatible, the irritation of smoke is increased, the aftertaste comfort is reduced, the offensive odor is increased, the improvement effect on the smoke is poor, and the sensory score value is obviously lower than that of a blank control.
In addition, the gel matrix of comparative examples 4-6 is beyond the scope of the present invention, and it cannot effectively reduce the smell of oil in the gel, which brings adverse effects to the sensory quality of the cigarette.
Finally, it should be noted that: the above examples are only intended to illustrate the technical solution of the present invention and not to limit it; although the present invention has been described in detail with reference to preferred embodiments, those skilled in the art will understand that: modifications to the specific embodiments of the invention or equivalent substitutions for parts of the technical features may be made; without departing from the spirit of the present invention, it is intended to cover all aspects of the invention as defined by the appended claims.
Claims (13)
1. A gel composition for cigarettes comprises 50-97 wt% of gel matrix and 3-50 wt% of essence solution;
the gel matrix comprises the following components:
2. the gel composition for cigarette according to claim 1, wherein the gel matrix comprises the following components:
3. the gel composition for cigarette as claimed in claim 1, wherein the polyethylene glycol material is polyethylene glycol having an average molecular weight in the range of 750-12000.
4. The gel composition for cigarette as claimed in claim 1, wherein the polyethylene glycol material is selected from one or more of polyethylene glycol 1000, polyethylene glycol 1500, polyethylene glycol 4000, and polyethylene glycol 10000.
5. The gel composition for cigarettes as claimed in claim 1, wherein the polyethylene glycol material comprises polyethylene glycol 1000, polyethylene glycol 1500, polyethylene glycol 4000 and polyethylene glycol 10000 in a weight ratio of 8-12: 8-12: 8-12: 8 to 12.
6. The cigarette gel composition of claim 1, the flavor solution being an ice-feel matcha flavor solution.
7. The gel composition for cigarette as claimed in claim 1, wherein the ice-feeling matcha flavor essence solution contains ice-feeling matcha flavor essence and a solvent;
the ice taste matcha flavor essence contains the following aroma components:
4.59 to 5.61 parts of ice-feeling essence;
1.75-2.15 parts of jasmine essence;
0.49-0.61 part of flower fragrance essence;
0.32 to 0.40 portion of tea essence; and
0.08 to 0.11 portion of auxiliary essence;
wherein,
the ice essence is selected from one or more of peppermint oil, menthol, menthone and menthyl acetate;
the jasmine essence is selected from one or more of jasmine essential oil, methyl dihydrojasmonate, cis-jasmone and phenethyl alcohol;
the floral essence is selected from one or more of geranium oil, bergamot oil, hexanoic acid leaf alcohol ester, α -ionone, α -damascenone;
the tea essence is selected from one or more of linalool, tea scented ketone, indole, benzyl alcohol, tea scented spirane, and Tieguanyin tea leaf essential oil;
the auxiliary essence is one or more selected from dihydroactinidiolide, gamma-caprolactone and peru extract.
8. The gel composition for cigarettes as claimed in claim 7, wherein the ice matcha flavor essence contains the following aroma components in parts by weight:
0.675-0.825 parts of peppermint oil;
2.7-3.3 parts of menthol;
0.54-0.66 parts of menthone;
0.675 to 0.825 parts of menthyl acetate;
0.27-0.33 parts of jasmine essential oil;
0.54-0.66 parts of methyl dihydrojasmonate;
0.405-0.495 parts of cis-jasmone;
0.54-0.66 parts of phenethyl alcohol;
0.135-0.165 parts of geranium oil;
0.27-0.33 parts of bergamot oil;
0.0675-0.0825 parts of hexanoic acid leaf alcohol ester;
0.0135-0.0165 part of α -ionone;
0.00675-0.00825 parts of α -damascenone;
0.135-0.165 parts of linalool;
0.0675-0.0825 parts of tea scented ketone;
0.027-0.033 parts of indole;
0.0675-0.0825 parts of benzyl alcohol;
0.0135-0.0165 parts of tea-scented spirane;
0.0135-0.0165 parts of Tieguanyin essential oil;
0.054-0.066 parts of dihydroactinidiolide;
0.027-0.033 parts of gamma-caprolactone; and
0.00675-0.00825 parts of Peru extract.
9. The gel composition for cigarette as claimed in claim 7, wherein the concentration of the ice-taste green tea essence in the ice-taste green tea essence solution is 8-12 wt%.
10. A process for preparing a gel composition for tobacco as claimed in any one of claims 1 to 9, comprising the steps of:
the method comprises the following steps:
(1) heating and melting a polyethylene glycol material and stearic acid according to the formula of the gel composition for the cigarettes, and mixing to obtain a mixture;
optionally, propylene glycol is also added;
(2) citric acid, malic acid, tea polysaccharide and a perfume solution were added to the mixture.
11. A filter stick for tobacco products, wherein the gel composition for cigarettes as claimed in any one of claims 1 to 9 is provided in the filter stick.
12. The filter rod of claim 11, wherein the gel composition for cigarettes is in the form of a strip, the gel composition of the strip is positioned in the filter rod, and the length direction of the gel composition of the strip is parallel to the length direction of the filter rod.
13. A tobacco product comprising the tobacco product filter rod according to any one of claims 11 to 12.
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Cited By (1)
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