CN107177901A - A kind of antibiotic aging-resistant textile material and preparation method thereof - Google Patents
A kind of antibiotic aging-resistant textile material and preparation method thereof Download PDFInfo
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- CN107177901A CN107177901A CN201710531338.3A CN201710531338A CN107177901A CN 107177901 A CN107177901 A CN 107177901A CN 201710531338 A CN201710531338 A CN 201710531338A CN 107177901 A CN107177901 A CN 107177901A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/06—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyolefin as constituent
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of antibiotic aging-resistant textile material and preparation method thereof, it is made from the following raw materials in parts by weight：25 35 parts of doughnut, 25 40 parts of polyester fiber, 5 20 parts of polypropylene fibre, 14 parts of nano ceramics, 15 25 parts of soybean fiber, 5 10 parts of cocoanut fiber, 10 15 parts of epoxy propane butyl ether, 28 parts of poly beta-hydroxybutyrate, 25 parts of double methyl methacrylate triethylene glycol ester, 58 parts of hyaluronic acid, 23 parts of yellow phosphorus lipid, 13 parts of Firebrake ZB, 69 parts of ethyl-para-hydroxybenzoate, 36 parts of Cyhalothrin, 25 parts of tetrachloro dihydroxy triphenylmenthane sodium sulfonate, 25 parts of adhesive, 25 parts of dispersant, 14 parts of heat stabilizer.The antibiotic aging-resistant textile material being prepared from, its ageing-resistant performance is excellent while having antibiotic effect concurrently.Meanwhile, also disclose the preparation method of this antibiotic aging-resistant textile material.
Description
Technical field
The present invention relates to textile material field, a kind of antibiotic aging-resistant textile material and preparation method thereof is related specifically to.
Background technology
With the continuous improvement of people's living standards, the requirement for weaving face fabric is also more and more, functional textile
In addition to basic fabric property, also need possess the effect such as antiultraviolet, antibacterial, aspect, health care.Antibacterial fibre weaving material
Material refers to the fiber or fabric that there are killing or inhibiting effect to microorganisms such as bacterium, fungi and viruses, its purpose not only for
Prevent textile from being stain and damaged by microorganism, it is often more important that in order to prevent infecting disease, it is ensured that the health of human body and dress
Comfortably, the cross-infection rate of PE is reduced, textile is obtained the New function of health care.Antibiotic fabric is to obtain fabric
The functions such as antibacterial, mould proof, deodorization that must well, can effectively suppress the microbial growth in fibre, prevent from infecting disease, with
Ensure healthiness.The textile of functionalization of the present invention assigns that its wearability is ageing-resistant, while there is certain antibacterial effect, can
To better meet popular and society demand.
The content of the invention
In order to solve the above technical problems, the present invention provides a kind of antibiotic aging-resistant textile material and preparation method thereof, pass through
It is combined using specified raw material, coordinates corresponding production technology, obtained antibiotic aging-resistant textile material, its ageing-resistant performance
It is excellent while have antibiotic effect concurrently, the requirement of industry is disclosure satisfy that, with preferable application prospect.
The purpose of the present invention can be achieved through the following technical solutions：
A kind of antibiotic aging-resistant textile material, is made from the following raw materials in parts by weight：：25-35 parts of doughnut, polyester fiber
25-40 parts, 5-20 parts of polypropylene fibre, 1-4 parts of nano ceramics, 15-25 parts of soybean fiber, 5-10 parts of cocoanut fiber, expoxy propane butyl
10-15 parts of ether, 2-8 parts of poly-beta-hydroxy-butyrate, 2-5 parts of double methyl methacrylate triethylene glycol ester, hyaluronic acid 5-8
Part, 2-3 parts of yellow phosphorus lipid, 1-3 parts of Firebrake ZB, 6-9 parts of ethyl-para-hydroxybenzoate, 3-6 parts of Cyhalothrin, tetrachloro dihydroxy
2-5 parts of base triphenylmenthane sodium sulfonate, 2-5 parts of adhesive, 2-5 parts of dispersant, 1-4 parts of heat stabilizer.
Preferably, adhesive is selected from triphenyl phosphite, 5-sulphosalicylic acid dihydrate, trisodium citrate monocalcium salt and closed
One or more in thing and dibutyl phthalate.
Preferably, described dispersant is selected from taurate, aminoguanidine sulfonate, lignosulfonates and vinyl
One or more in sulfonate.
Preferably, described heat stabilizer be selected from certain herbaceous plants with big flowers acid glycerol three ester, iodine propilolic alcohol butyl mephenesin Carbamate, maleate and
One or more in orange osmanthus acid esters.
The preparation method of described antibiotic aging-resistant textile material, comprises the following steps：
（1）Each raw material is weighed according to parts by weight；
（2）By doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber, cocoanut fiber, epoxy propane butyl ether, poly-
Beta-hydroxy-butanoic acid ester, dispersant add reactor, stir and evenly mix, and are heated to 150-200 DEG C, stirring insulation 30-60 minutes, stirring
250-300 revs/min of speed；
（3）By step（2）In reactant be cooled to room temperature, add double methyl methacrylate triethylene glycol ester, hyaluronic acid,
Yellow phosphorus lipid, heat stabilizer, are again heated to 100-130 DEG C, stirring insulation 15 minutes, 250-300 revs/min of mixing speed；
（4）To step（3）Mixture injection high-temperature vapor, continue be incubated 30 minutes；
（5）By step（4）Mixture and Firebrake ZB, ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy triphen
Loprazolam sodium, adhesive injection reactor mesohigh homogenizer, are mixed, mixing speed is 250-300 revs/min, pressure
Strong to be adjusted to 15-20MPa, the reaction time is 25 minutes, and reaction temperature is 100 DEG C；
（6）By step（5）In reactant as spinning under inert gas environment, handled by drawing, deaerate drying, be cooled to
Room temperature is got product.
Preferably, the inert gas is argon gas.
Preferably, the spinning speed is 2000-2500m/min.
Preferably, the drying temperature is 60-75 DEG C, drying time 2-3 hours.
Compared with prior art, its advantage is the present invention：
（1）The present invention antibiotic aging-resistant textile material, with doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber,
Cocoanut fiber, epoxy propane butyl ether, poly-beta-hydroxy-butyrate are main component, by adding the contracting of methacrylate two three
Glycol ester, hyaluronic acid, yellow phosphorus lipid, Firebrake ZB, ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy three
Phenylmethane sodium sulfonate, adhesive, heat stabilizer, dispersant, be aided with heating response, uniform stirring, steam activation, pressurized dispersion,
Pull spinning, deaerate the technique such as dry so that the antibiotic aging-resistant textile material being prepared from, its ageing-resistant performance is excellent simultaneously
Have antibiotic effect concurrently, disclosure satisfy that the requirement of industry, with preferable application prospect.
（2）Antibiotic aging-resistant textile material raw material of the invention is cheap, technique is simple, is used suitable for heavy industrialization,
It is practical.
Embodiment
The technical scheme of invention is described in detail with reference to specific embodiment.
Embodiment 1
（1）25 parts of doughnut, 25 parts of polyester fiber, 5 parts of polypropylene fibre, 1 part of nano ceramics, soybean fiber 15 are weighed according to parts by weight
Part, 5 parts of cocoanut fiber, 10 parts of epoxy propane butyl ether, 2 parts of poly-beta-hydroxy-butyrate, methacrylate triethylene-glycol
2 parts of ester, 5 parts of hyaluronic acid, 2 parts of yellow phosphorus lipid, 1 part of Firebrake ZB, 6 parts of ethyl-para-hydroxybenzoate, 3 parts of Cyhalothrin,
2 parts of tetrachloro dihydroxy triphenylmenthane sodium sulfonate, 2 parts of triphenyl phosphite, 2 parts of taurate, 1 part of certain herbaceous plants with big flowers acid glycerol three ester；
（2）By doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber, cocoanut fiber, epoxy propane butyl ether, poly-
Beta-hydroxy-butanoic acid ester, taurate add reactor, stir and evenly mix, and are heated to 150 DEG C, stirring insulation 30 minutes, mixing speed
250 revs/min；
（3）By step（2）In reactant be cooled to room temperature, add double methyl methacrylate triethylene glycol ester, hyaluronic acid,
Yellow phosphorus lipid, certain herbaceous plants with big flowers acid glycerol three ester, are again heated to 100 DEG C, stirring insulation 15 minutes, 250 revs/min of mixing speed；
（4）To step（3）Mixture injection high-temperature vapor, continue be incubated 30 minutes；
（5）By step（4）Mixture and Firebrake ZB, ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy triphen
Loprazolam sodium, triphenyl phosphite injection reactor mesohigh homogenizer, are mixed, mixing speed is 250 revs/min,
Pressure is adjusted to 15MPa, and the reaction time is 25 minutes, and reaction temperature is 100 DEG C；
（6）By step（5）In reactant as spinning under ar gas environment, handled by drawing, deaerate drying, be cooled to room temperature
Get product, spinning speed is 2000m/min, drying temperature is 60 DEG C, drying time 2 hours.
The performance test results of obtained antibiotic aging-resistant textile material are as shown in table 1.
Embodiment 2
（1）28 parts of doughnut, 30 parts of polyester fiber, 10 parts of polypropylene fibre, 2 parts of nano ceramics, soybean fiber are weighed according to parts by weight
18 parts, 7 parts of cocoanut fiber, 12 parts of epoxy propane butyl ether, 4 parts of poly-beta-hydroxy-butyrate, methacrylate two contract three second two
3 parts of alcohol ester, 6 parts of hyaluronic acid, 2 parts of yellow phosphorus lipid, 1 part of Firebrake ZB, 7 parts of ethyl-para-hydroxybenzoate, Cyhalothrin 4
Part, 3 parts of tetrachloro dihydroxy triphenylmenthane sodium sulfonate, 3 parts of 5-sulphosalicylic acid dihydrate, 3 parts of aminoguanidine sulfonate, iodine propine
2 parts of alcohol butyl mephenesin Carbamate；
（2）By doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber, cocoanut fiber, epoxy propane butyl ether, poly-
Beta-hydroxy-butanoic acid ester, aminoguanidine sulfonate add reactor, stir and evenly mix, and are heated to 170 DEG C, stirring insulation 40 minutes, stirring
270 revs/min of speed；
（3）By step（2）In reactant be cooled to room temperature, add double methyl methacrylate triethylene glycol ester, hyaluronic acid,
Yellow phosphorus lipid, iodine propilolic alcohol butyl mephenesin Carbamate, are again heated to 110 DEG C, stirring insulation 15 minutes, 270 revs/min of mixing speed
Clock；
（4）To step（3）Mixture injection high-temperature vapor, continue be incubated 30 minutes；
（5）By step（4）Mixture and Firebrake ZB, ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy triphen
Loprazolam sodium, 5-sulphosalicylic acid dihydrate injection reactor mesohigh homogenizer, are mixed, mixing speed is 270
Rev/min, pressure is adjusted to 17MPa, and the reaction time is 25 minutes, and reaction temperature is 100 DEG C；
（6）By step（5）In reactant as spinning under ar gas environment, handled by drawing, deaerate drying, be cooled to room temperature
Get product, spinning speed is 2200m/min, drying temperature is 65 DEG C, drying time 2.3 hours.
The performance test results of obtained antibiotic aging-resistant textile material are as shown in table 1.
Embodiment 3
（1）32 parts of doughnut, 35 parts of polyester fiber, 15 parts of polypropylene fibre, 3 parts of nano ceramics, soybean fiber are weighed according to parts by weight
23 parts, 9 parts of cocoanut fiber, 14 parts of epoxy propane butyl ether, 6 parts of poly-beta-hydroxy-butyrate, methacrylate two contract three second two
4 parts of alcohol ester, 7 parts of hyaluronic acid, 3 parts of yellow phosphorus lipid, 2 parts of Firebrake ZB, 8 parts of ethyl-para-hydroxybenzoate, Cyhalothrin 5
Part, 4 parts of tetrachloro dihydroxy triphenylmenthane sodium sulfonate, 4 parts of trisodium citrate monocalcium salt compound, 4 parts of lignosulfonates, maleic acid
3 parts of ester；
（2）By doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber, cocoanut fiber, epoxy propane butyl ether, poly-
Beta-hydroxy-butanoic acid ester, lignosulfonates add reactor, stir and evenly mix, and are heated to 190 DEG C, stirring insulation 50 minutes, stirring
290 revs/min of speed；
（3）By step（2）In reactant be cooled to room temperature, add double methyl methacrylate triethylene glycol ester, hyaluronic acid,
Yellow phosphorus lipid, maleate, are again heated to 120 DEG C, stirring insulation 15 minutes, 290 revs/min of mixing speed；
（4）To step（3）Mixture injection high-temperature vapor, continue be incubated 30 minutes；
（5）By step（4）Mixture and Firebrake ZB, ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy triphen
Loprazolam sodium, trisodium citrate monocalcium salt compound injection reactor mesohigh homogenizer, are mixed, mixing speed is 290
Rev/min, pressure is adjusted to 19MPa, and the reaction time is 25 minutes, and reaction temperature is 100 DEG C；
（6）By step（5）In reactant as spinning under ar gas environment, handled by drawing, deaerate drying, be cooled to room temperature
Get product, spinning speed is 2400m/min, drying temperature is 70 DEG C, drying time 2.7 hours.
The performance test results of obtained antibiotic aging-resistant textile material are as shown in table 1.
Embodiment 4
（1）35 parts of doughnut, 40 parts of polyester fiber, 20 parts of polypropylene fibre, 4 parts of nano ceramics, soybean fiber are weighed according to parts by weight
25 parts, 10 parts of cocoanut fiber, 15 parts of epoxy propane butyl ether, 8 parts of poly-beta-hydroxy-butyrate, methacrylate two contract three second
5 parts of diol ester, 8 parts of hyaluronic acid, 3 parts of yellow phosphorus lipid, 3 parts of Firebrake ZB, 9 parts of ethyl-para-hydroxybenzoate, Cyhalothrin
6 parts, 5 parts of tetrachloro dihydroxy triphenylmenthane sodium sulfonate, 5 parts of dibutyl phthalate, 5 parts of vinylsulfonate, orange osmanthus acid esters 4
Part；
（2）By doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber, cocoanut fiber, epoxy propane butyl ether, poly-
Beta-hydroxy-butanoic acid ester, vinylsulfonate add reactor, stir and evenly mix, and are heated to 200 DEG C, stirring insulation 60 minutes, stirring
300 revs/min of speed；
（3）By step（2）In reactant be cooled to room temperature, add double methyl methacrylate triethylene glycol ester, hyaluronic acid,
Yellow phosphorus lipid, orange osmanthus acid esters, are again heated to 130 DEG C, stirring insulation 15 minutes, 300 revs/min of mixing speed；
（4）To step（3）Mixture injection high-temperature vapor, continue be incubated 30 minutes；
（5）By step（4）Mixture and Firebrake ZB, ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy triphen
Loprazolam sodium, dibutyl phthalate injection reactor mesohigh homogenizer, are mixed, mixing speed is 300 revs/min
Clock, pressure is adjusted to 20MPa, and the reaction time is 25 minutes, and reaction temperature is 100 DEG C；
（6）By step（5）In reactant as spinning under ar gas environment, handled by drawing, deaerate drying, be cooled to room temperature
Get product, spinning speed is 2500m/min, drying temperature is 75 DEG C, drying time 3 hours.
The performance test results of obtained antibiotic aging-resistant textile material are as shown in table 1.
Comparative example 1
（1）25 parts of doughnut, 25 parts of polyester fiber, 5 parts of polypropylene fibre, 1 part of nano ceramics, soybean fiber 15 are weighed according to parts by weight
Part, 5 parts of cocoanut fiber, 2 parts of poly-beta-hydroxy-butyrate, 2 parts of double methyl methacrylate triethylene glycol ester, 5 parts of hyaluronic acid,
2 parts of yellow phosphorus lipid, 1 part of Firebrake ZB, 3 parts of Cyhalothrin, 2 parts of tetrachloro dihydroxy triphenylmenthane sodium sulfonate, phosphorous triphenyl phosphate
2 parts of ester, 2 parts of taurate, 1 part of certain herbaceous plants with big flowers acid glycerol three ester；
（2）By doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber, cocoanut fiber, poly-beta-hydroxy-butyrate, ox
Sulfonate adds reactor, stirs and evenly mixs, and is heated to 150 DEG C, stirring insulation 30 minutes, 250 revs/min of mixing speed；
（3）By step（2）In reactant be cooled to room temperature, add double methyl methacrylate triethylene glycol ester, hyaluronic acid,
Yellow phosphorus lipid, certain herbaceous plants with big flowers acid glycerol three ester, are again heated to 100 DEG C, stirring insulation 15 minutes, 250 revs/min of mixing speed；
（4）To step（3）Mixture injection high-temperature vapor, continue be incubated 30 minutes；
（5）By step（4）Mixture and Firebrake ZB, Cyhalothrin, tetrachloro dihydroxy triphenylmenthane sodium sulfonate, phosphorous acid
Triphenylmethyl methacrylate injects reactor mesohigh homogenizer, mixes, and mixing speed is 250 revs/min, and pressure is adjusted to 15MPa, instead
It is 25 minutes between seasonable, reaction temperature is 100 DEG C；
（6）By step（5）In reactant as spinning under ar gas environment, handled by drawing, deaerate drying, be cooled to room temperature
Get product, spinning speed is 2000m/min, drying temperature is 60 DEG C, drying time 2 hours.
The performance test results of obtained antibiotic aging-resistant textile material are as shown in table 1.
Comparative example 2
（1）35 parts of doughnut, 40 parts of polyester fiber, 20 parts of polypropylene fibre, 25 parts of soybean fiber, cocoanut fiber are weighed according to parts by weight
10 parts, 15 parts of epoxy propane butyl ether, 8 parts of poly-beta-hydroxy-butyrate, 5 parts of double methyl methacrylate triethylene glycol ester, thoroughly
Bright 8 parts of matter acid, 3 parts of yellow phosphorus lipid, 9 parts of ethyl-para-hydroxybenzoate, 6 parts of Cyhalothrin, tetrachloro dihydroxy triphenylmenthane
5 parts of sodium sulfonate, 5 parts of dibutyl phthalate, 5 parts of vinylsulfonate, 4 parts of orange osmanthus acid esters；
（2）By doughnut, polyester fiber, polypropylene fibre, soybean fiber, cocoanut fiber, epoxy propane butyl ether, poly- beta-hydroxy fourth
Acid esters, vinylsulfonate add reactor, stir and evenly mix, and are heated to 200 DEG C, stirring insulation 60 minutes, mixing speed 300
Rev/min；
（3）By step（2）In reactant be cooled to room temperature, add double methyl methacrylate triethylene glycol ester, hyaluronic acid,
Yellow phosphorus lipid, orange osmanthus acid esters, are again heated to 130 DEG C, stirring insulation 15 minutes, 300 revs/min of mixing speed；
（4）To step（3）Mixture injection high-temperature vapor, continue be incubated 30 minutes；
（5）By step（4）Mixture and ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy triphenylmenthane sulphur
Sour sodium, dibutyl phthalate injection reactor mesohigh homogenizer, are mixed, mixing speed is 300 revs/min, pressure
Strong to be adjusted to 20MPa, the reaction time is 25 minutes, and reaction temperature is 100 DEG C；
（6）By step（5）In reactant as spinning under ar gas environment, handled by drawing, deaerate drying, be cooled to room temperature
Get product, spinning speed is 2500m/min, drying temperature is 75 DEG C, drying time 3 hours.
The performance test results of obtained antibiotic aging-resistant textile material are as shown in table 1.
Embodiment 1-4 and comparative example 1-2 obtained antibiotic aging-resistant textile material is subjected to char length, it is corrosion-resistant
Property, yellowing, Escherichia coli inhibiting rate, this several performance tests of dust mite recall rate.
Table 1
The antibiotic aging-resistant textile material of the present invention, with doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber, coconut palm
Subbundle, epoxy propane butyl ether, poly-beta-hydroxy-butyrate are main component, by adding three second of contracting of methacrylate two
Diol ester, hyaluronic acid, yellow phosphorus lipid, Firebrake ZB, ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy triphen
Loprazolam sodium, adhesive, heat stabilizer, dispersant, are aided with heating response, uniform stirring, steam activation, pressurized dispersion, lead
Draw spinning, deaerate the technique such as dry so that the antibiotic aging-resistant textile material being prepared from, its ageing-resistant performance is excellent while simultaneous
Have antibiotic effect, the requirement of industry is disclosure satisfy that, with preferable application prospect.The antibiotic aging-resistant textile material of the present invention is former
Material is cheap, technique is simple, is used suitable for heavy industrialization, practical.
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to utilize this hair
Equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks
Domain, is included within the scope of the present invention.
Claims (8)
1. a kind of antibiotic aging-resistant textile material, it is characterised in that：It is made from the following raw materials in parts by weight：Doughnut 25-35
Part, 25-40 parts of polyester fiber, 5-20 parts of polypropylene fibre, 1-4 parts of nano ceramics, 15-25 parts of soybean fiber, 5-10 parts of cocoanut fiber, ring
10-15 parts of Ethylene Oxide butyl ether, 2-8 parts of poly-beta-hydroxy-butyrate, 2-5 parts of double methyl methacrylate triethylene glycol ester, thoroughly
Bright 5-8 parts of matter acid, 2-3 parts of yellow phosphorus lipid, 1-3 parts of Firebrake ZB, 6-9 parts of ethyl-para-hydroxybenzoate, Cyhalothrin 3-6
Part, 2-5 parts of tetrachloro dihydroxy triphenylmenthane sodium sulfonate, 2-5 parts of adhesive, 2-5 parts of dispersant, 1-4 parts of heat stabilizer.
2. antibiotic aging-resistant textile material according to claim 1, it is characterised in that：The adhesive is selected from phosphorous acid three
Phenyl ester, 5-sulphosalicylic acid dihydrate, trisodium citrate monocalcium salt compound and one kind or several in dibutyl phthalate
Kind.
3. antibiotic aging-resistant textile material according to claim 1, it is characterised in that：Described dispersant is selected from ox
One or more in sulfonate, aminoguanidine sulfonate, lignosulfonates and vinylsulfonate.
4. antibiotic aging-resistant textile material according to claim 1, it is characterised in that：Described heat stabilizer is selected from certain herbaceous plants with big flowers acid
One or more in triglycerides, iodine propilolic alcohol butyl mephenesin Carbamate, maleate and orange osmanthus acid esters.
5. according to the preparation method of any described antibiotic aging-resistant textile material of Claims 1 to 4, it is characterised in that including
Following steps：
（1）Each raw material is weighed according to parts by weight；
（2）By doughnut, polyester fiber, polypropylene fibre, nano ceramics, soybean fiber, cocoanut fiber, epoxy propane butyl ether, poly-
Beta-hydroxy-butanoic acid ester, dispersant add reactor, stir and evenly mix, and are heated to 150-200 DEG C, stirring insulation 30-60 minutes, stirring
250-300 revs/min of speed；
（3）By step（2）In reactant be cooled to room temperature, add double methyl methacrylate triethylene glycol ester, hyaluronic acid,
Yellow phosphorus lipid, heat stabilizer, are again heated to 100-130 DEG C, stirring insulation 15 minutes, 250-300 revs/min of mixing speed；
（4）To step（3）Mixture injection high-temperature vapor, continue be incubated 30 minutes；
（5）By step（4）Mixture and Firebrake ZB, ethyl-para-hydroxybenzoate, Cyhalothrin, tetrachloro dihydroxy triphen
Loprazolam sodium, adhesive injection reactor mesohigh homogenizer, are mixed, mixing speed is 250-300 revs/min, pressure
Strong to be adjusted to 15-20MPa, the reaction time is 25 minutes, and reaction temperature is 100 DEG C；
（6）By step（5）In reactant as spinning under inert gas environment, handled by drawing, deaerate drying, be cooled to
Room temperature is got product.
6. the preparation method of antibiotic aging-resistant textile material according to claim 5, it is characterised in that：Step（6）It is described
Inert gas is argon gas.
7. the preparation method of antibiotic aging-resistant textile material according to claim 5, it is characterised in that：Step（6）It is described
Spinning speed is 2000-2500m/min.
8. the preparation method of antibiotic aging-resistant textile material according to claim 5, it is characterised in that：Step（6）It is described
Drying temperature is 60-75 DEG C, drying time 2-3 hours.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108360116A (en) * | 2018-02-26 | 2018-08-03 | 合肥远科服装设计有限公司 | A kind of preparation method of textile material |
| CN108611699A (en) * | 2018-04-23 | 2018-10-02 | 合肥云都棉花有限公司 | A kind of antibacterial textile material and preparation method thereof |
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| CN108611699A (en) * | 2018-04-23 | 2018-10-02 | 合肥云都棉花有限公司 | A kind of antibacterial textile material and preparation method thereof |
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