CN106614616A - Microemulsion containing trinexapac-ethyl and paclobutrazol - Google Patents

Microemulsion containing trinexapac-ethyl and paclobutrazol Download PDF

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Publication number
CN106614616A
CN106614616A CN201610881302.3A CN201610881302A CN106614616A CN 106614616 A CN106614616 A CN 106614616A CN 201610881302 A CN201610881302 A CN 201610881302A CN 106614616 A CN106614616 A CN 106614616A
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Prior art keywords
paclobutrazol
snacethyl
trinexan
microemulsion
cosolvent
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CN201610881302.3A
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Chinese (zh)
Inventor
黄禹
曾显斌
赵国正
侯勇
夏中梅
王云海
刘祥宇
张超
曾芸
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Sichuan Lanyue Science & Technology Co Ltd
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Sichuan Lanyue Science & Technology Co Ltd
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Priority to CN201610881302.3A priority Critical patent/CN106614616A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647Triazoles; Hydrogenated triazoles
    • A01N43/6531,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/42Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing within the same carbon skeleton a carboxylic group or a thio analogue, or a derivative thereof, and a carbon atom having only two bonds to hetero atoms with at the most one bond to halogen, e.g. keto-carboxylic acids

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention provides microemulsion containing trinexapac-ethyl and paclobutrazol. The microemulsion is prepared from components in percentage by weight as follows: 1%-40% of trinexapac-ethyl, 1%-10% of paclobutrazol, 1%-20% of a solvent, 1%-15% of a cosolvent, 10%-50% of an emulsifier, 1%-10% of an antifreezing agent and the balance of water. The microemulsion containing trinexapac-ethyl and paclobutrazol has excellent lodging-resistant and lawn-dwarfing effects as well as low use cost, little environmental pollution and good environmental protection effect.

Description

Microemulsion containing TrinexAN_SNacethyl and paclobutrazol
Technical field:
The invention belongs to plant growth regulator field, more particularly to be one kind be mainly used in wheat, lodging resistance in rice and The microemulsion containing TrinexAN_SNacethyl and paclobutrazol that lawn is downgraded.
Background technology:
TrinexAN_SNacethyl belongs to cyclohexane-carboxylic acid plant growth regulator, by suppressing the biosynthesis of gibberellin prosperous to adjust plant It is long.For cereal crop and winter rape, can prevent from lodging and improving efficiency of crop;Moving frequency can be reduced for lawn;With Can promote maturation in sugarcane.Because TrinexAN_SNacethyl active compound fusing point is relatively low, at present main formulation is the breast for only containing single TrinexAN_SNacethyl composition Oil and microemulsion, there are no the combination dosage form containing TrinexAN_SNacethyl.Half-life of the TrinexAN_SNacethyl in soil is less than 7 days, main metabolic Thing is carbon dioxide, safe, but haves the shortcomings that efficiency time is short.
Paclobutrazol is category triazole type plant growth regulator, is the inhibitor of endogenous gibberellins synthesis.Apply on paddy rice Then substantially weaken rice seedling apical growth advantage, promote lateral bud (tiller) to grow.Rice shoot appearance is short strengthen many tillers, leaf color it is dark green, Well developed root system.Paclobutrazol low concentration promotes the photosynthetic efficiency of rice seedling blade;High concentration suppresses photosynthetic efficiency, improves root system respiration strong Degree, reduces aerial part respiratory intensity, improves Stoma of Leaves resistance, reduces leaf transpiration effect.The agricultural application valency of paclobutrazol Value is its control effect to plant growth.With plant growth is delayed, suppress cane elongation, shorten internode, promote plant Tiller, promotion bud differentiation, increase plant stress-resistance performance, improve yield and other effects.Long half time of the paclobutrazol in soil reaches 0.5-1, is not easily decomposed, and the growth for accumulating and affecting succeeding crop is easily caused in soil.
The existing commercially available plant growth regulator containing paclobutrazol composition mostly is wettable powder or suspending agent, there is suspensibility not Height, the more complicated problem of technological process in preparation processing production process.
The content of the invention:
The shortcoming existed for prior art and deficiency, the invention aims to provide a kind of resistant to lodging, effect is downgraded on lawn Really good, use cost is low, low in the pollution of the environment, the good microemulsion containing TrinexAN_SNacethyl and paclobutrazol of environment protecting.
The object of the present invention is achieved like this:
Microemulsion containing TrinexAN_SNacethyl and paclobutrazol in the present invention, by weight percentage including following components:
TrinexAN_SNacethyl 1~40%,
Paclobutrazol 1~10%,
Solvent 1~20%,
Cosolvent 1~15%,
Emulsifying agent 10~50%,
Antifreezing agent 1~10%,
Water surplus.
After the present invention is by TrinexAN_SNacethyl and paclobutrazol compounding, microemulsion is processed into.Microemulsion by active compound, surfactant, water, Cosolvent, defoamer etc. are constituted, and belong to dispersion stable during thermodynamics Jing.Be characterized in water as medium, without or it is few Containing organic solvent, thus do not fire not quick-fried, production operation, store and transport safe, low in the pollution of the environment, a large amount of organic solvents of saving;Agricultural chemicals point Divergence is high, and up to miniaturization degree, agricultural chemicals particle is generally 0.1~0.01 micron, and outward appearance is similar to transparent or sub-translucent liquid; Good dispersion in water, adhesive force strong to target body permeability is good.The present invention compounds TrinexAN_SNacethyl and paclobutrazol, is contained using TrinexAN_SNacethyl Ratio collocation based on amount, supplemented by paclobutrazol content, both ensure that the due effect of both plant growth regulator, also overcome The shortcoming that the TrinexAN_SNacethyl half-life is too short and paclobutrazol half-life is long.
The above-mentioned microemulsion containing TrinexAN_SNacethyl and paclobutrazol, by weight percentage including following components:
TrinexAN_SNacethyl 10~30%,
Paclobutrazol 3~8%,
Solvent 6~18%,
Cosolvent 5~10%,
Emulsifying agent 20~40%,
Antifreezing agent 3~6%,
Water surplus.
Above-mentioned solvent is at least one in toluene, dimethylbenzene, ethanol, methyl alcohol, acetone, cyclohexanone, dimethyl sulfoxide.
Above-mentioned cosolvent is at least one in normal propyl alcohol, isopropanol, n-butanol, isobutanol, n-octyl alcohol.
Above-mentioned emulsifying agent is APES, AEO, alkylbenzenesulfonate, alkylsurfuric acid Salt, styrylphenol polyoxyethylene ether, alkyl phenol formaldehyde resin polyoxyethylene ether, polyoxyethylene sorbitan list bay Acid esters, polyoxyethylene sorbitan monooleate, disecoctylmaleate sodium sulfonate, AEO sulfuric acid At least one in ester.
Above-mentioned antifreezing agent is at least one in ethylene glycol, propane diols, glycerine, urea.
Preparation process of the present invention containing TrinexAN_SNacethyl and paclobutrazol microemulsion comprises the following steps:
(1)Dispensing in proportion:
(2)TrinexAN_SNacethyl and paclobutrazol original medicinal solvent and cosolvent are fully dissolved;
(3)Emulsifying agent, antifreeze are added in above-mentioned a bulk solution, is well mixed;
(4)Water is slowly added in above-mentioned system, is stirred into freely scattered, homogeneous, transparent, stable faint yellow Liquid.
The present invention containing TrinexAN_SNacethyl and paclobutrazol microemulsion with advantages below:
1st, microemulsion of the present invention, with water as main matrix, has saved a large amount of organic solvents, and environmental pollution is little, without residual after administration Stay;
2nd, it is nonflammable, storage, transportation safety;
3rd, simple production process, it is easy to prepare, low cost;
4th, lodging-prevention, lawn Dwarf Effect on Dwarf are good.
Specific embodiment
Embodiment 1:
Microemulsion of the present embodiment 1 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 25%, paclobutrazol 2%, second Alcohol 5%, toluene 5%, cyclohexanone 5%, normal propyl alcohol 3%, ethylene glycol 1%, APES 15%, lauryl sodium sulfate 0.5%, water surplus.
The present embodiment 1 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with ethanol, toluene and cyclohexanone mixed solution, add cosolvent normal propyl alcohol, antifreeze ethylene glycol and emulsifying agent alkyl phenol APEO and lauryl sodium sulfate, after being sufficiently mixed uniformly, water are slowly added in above-mentioned system, and stirring mixing is equal It is even, become homogeneous, transparent, stable microemulsion.
Embodiment 2:
Microemulsion of the present embodiment 2 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 25%, paclobutrazol 5%, first Alcohol 5%, dimethylbenzene 7%, dimethyl sulfoxide 3%, normal propyl alcohol 2%, n-butanol 2%, ethylene glycol 1%, propane diols 1%, AEO 15%, polyoxyethylene 20 sorbitan monolaurate 10%, polyoxyethylene alkyl ether sulfate 3%, water surplus.
The present embodiment 2 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with methyl alcohol, dimethylbenzene and dimethyl sulfoxide mixed solution, add cosolvent normal propyl alcohol and n-butanol, antifreeze ethylene glycol, Propane diols and emulsifying agent AEO, polyoxyethylene 20 sorbitan monolaurate and AEO After sulfuric ester is sufficiently mixed uniformly, water is slowly added in above-mentioned system, is uniformly mixed, become homogeneous, transparent, stable Microemulsion.
Embodiment 3:
Microemulsion of the present embodiment 3 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 20%, paclobutrazol 8%, first Alcohol 5%, dimethylbenzene 5%, cyclohexanone 7%, isopropanol 2%, n-butanol 1%, ethylene glycol 1%, glycerine 0.5%, urea 1%, alkyl phenol gathers Oxygen vinethene 17%, styrylphenol polyoxyethylene ether 8%, disecoctylmaleate sodium sulfonate 2%, water surplus.
The present embodiment 3 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with methyl alcohol, dimethylbenzene and cyclohexanone mixed solution, add cosolvent isopropanol, n-butanol, antifreeze ethylene glycol, the third three Alcohol, urea and emulsifying agent APES, styrylphenol polyoxyethylene ether and maleic acid di-sec-octyl sulphur After sour sodium is sufficiently mixed uniformly, water is slowly added in above-mentioned system, is uniformly mixed, become homogeneous, transparent, stable Microemulsion.
Embodiment 4:
Microemulsion of the present embodiment 4 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 10%, paclobutrazol 8%, two First sulfoxide 2%, dimethylbenzene 8%, isopropanol 3%, n-butanol 1%, ethylene glycol 2%, glycerine 1%, alkylphenol-formaldehyde resin polyoxyethylene Ether 22%, styrylphenol polyoxyethylene ether 5%, calcium dodecyl benzene sulfonate 1.5%, water surplus.
The present embodiment 4 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with dimethyl sulfoxide and dimethylbenzene mixed solution, add cosolvent isopropanol and n-butanol, antifreeze ethylene glycol, glycerine It is abundant with emulsifying agent alkyl phenol formaldehyde resin polyoxyethylene ether, styrylphenol polyoxyethylene ether and calcium dodecyl benzene sulfonate After being well mixed, water is slowly added in above-mentioned system, is uniformly mixed, become homogeneous, transparent, stable microemulsion.
Embodiment 5:
Microemulsion of the present embodiment 5 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 15%, paclobutrazol 5%, first Alcohol 5%, dimethylbenzene 8%, isopropanol 3%, n-butanol 1%, glycerine 2%, urea 0.5%, OPEO 25%, styrene Base phenol APEO 6%, lauryl sodium sulfate 0.5%, water surplus.
The present embodiment 5 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with methyl alcohol, dimethylbenzene mixed solution, add cosolvent isopropanol and n-butanol, antifreeze glycerine, urea and emulsification After agent APES, styrylphenol polyoxyethylene ether and lauryl sodium sulfate are sufficiently mixed uniformly, by water In being slowly added to above-mentioned system, it is uniformly mixed, becomes homogeneous, transparent, stable microemulsion.
Embodiment 6:
Microemulsion of the present embodiment 6 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 30%, paclobutrazol 3%, first Alcohol 5%, dimethylbenzene 10%, dimethyl sulfoxide 5%, isopropanol 5%, n-octyl alcohol 2%, ethylene glycol 2%, propane diols 1%, octyl phenol polyoxyethylene Ether 20%, styrylphenol polyoxyethylene ether 8%, disecoctylmaleate sodium sulfonate 1%, water surplus.
The present embodiment 6 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with methyl alcohol, dimethylbenzene and dimethyl sulfoxide mixed solution, add cosolvent isopropanol and n-octyl alcohol, antifreeze ethylene glycol and Propane diols, emulsifying agent APES, styrylphenol polyoxyethylene ether and maleic acid di-sec-octyl sulfonic acid Sodium be sufficiently mixed it is uniform after, water is slowly added in above-mentioned system, be uniformly mixed, become homogeneous, transparent, stable micro- Emulsion.
Embodiment 7:
Microemulsion of the present embodiment 7 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 30%, paclobutrazol 5%, second Alcohol 5%, dimethylbenzene 8%, cyclohexanone 8%, isopropanol 4%, n-butanol 1%, isobutanol 1%, ethylene glycol 2%, propane diols 2%, poly alkyl alcohol Oxygen vinethene 15%, styrylphenol polyoxyethylene ether 10%, polyoxyethylene alkyl ether sulfate 2%, water surplus.
The present embodiment 7 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with ethanol, dimethylbenzene and cyclohexanone mixed solution, add cosolvent isopropanol, n-butanol and isobutanol, antifreeze second Glycol and propane diols, emulsifying agent AEO, styrylphenol polyoxyethylene ether and AEO After sulfuric ester is sufficiently mixed uniformly, water is slowly added in above-mentioned system, is uniformly mixed, become homogeneous, transparent, stable Microemulsion.
Embodiment 8:
Microemulsion of the present embodiment 8 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 15%, paclobutrazol 8%, first Alcohol 3%, dimethylbenzene 10%, cyclohexanone 2%, isopropanol 4%, n-butanol 1%, n-octyl alcohol 2%, ethylene glycol 1%, glycerine 4%, alkyl phenol APEO 25%, alkyl phenol formaldehyde resin polyoxyethylene ether 6%, polyoxyethylene alkyl ether sulfate 2%, water surplus.
The present embodiment 8 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with methyl alcohol, dimethylbenzene and cyclohexanone mixed solution, add cosolvent isopropanol, n-butanol and n-octyl alcohol, antifreeze second Glycol and glycerine, emulsifying agent APES, alkyl phenol formaldehyde resin polyoxyethylene ether and aliphatic alcohol polyethenoxy After ether sulfuric ester is sufficiently mixed uniformly, water is slowly added in above-mentioned system, is uniformly mixed, become homogeneous, transparent, steady Fixed microemulsion.
Embodiment 9:
Microemulsion of the present embodiment 9 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 20%, paclobutrazol 3%, second Alcohol 3%, toluene 6%, cyclohexanone 1%, normal propyl alcohol 2%, n-butanol 2%, glycerine 2%, urea 1%, polyoxyethylene sorbitan list Laurate 25%, styrylphenol polyoxyethylene ether 12%, calcium dodecyl benzene sulfonate 2%, water surplus.
The present embodiment 9 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with ethanol, toluene and cyclohexanone mixed solution, add cosolvent normal propyl alcohol and n-butanol, antifreeze glycerine and urine Element, emulsifier polyoxyethylene sorbitan mono-laurate, styrylphenol polyoxyethylene ether and DBSA Calcium be sufficiently mixed it is uniform after, water is slowly added in above-mentioned system, be uniformly mixed, become homogeneous, transparent, stable micro- Emulsion.
Embodiment 10:
Microemulsion of the present embodiment 10 containing TrinexAN_SNacethyl and paclobutrazol, includes by weight percentage:TrinexAN_SNacethyl 20%, paclobutrazol 5%, second Alcohol 3%, dimethylbenzene 6%, acetone 3%, isopropanol 5%, n-octyl alcohol 2%, ethylene glycol 2%, glycerine 2%, APES 20%, Styrylphenol polyoxyethylene ether 10%, disecoctylmaleate sodium sulfonate 1%, excess water.
The present embodiment 10 contains the preparation method of the microemulsion of TrinexAN_SNacethyl and paclobutrazol:First by TrinexAN_SNacethyl and paclobutrazol active compound Dissolved with ethanol, dimethylbenzene and acetone mixed solution, add cosolvent isopropanol and n-octyl alcohol, antifreeze ethylene glycol and the third three Alcohol, emulsifying agent APES, styrylphenol polyoxyethylene ether and disecoctylmaleate sodium sulfonate fill Divide after being well mixed, water is slowly added in above-mentioned system, be uniformly mixed, become homogeneous, transparent, stable micro emulsion Agent.
Application example:
By the microemulsion containing TrinexAN_SNacethyl and paclobutrazol obtained by above-described embodiment 1, with 15% commercially available paclobutrazol wettable powder Agent, 25% anti-fall emulsifiable concentrate carry out contrast test on wheat, and test site is Chengdu Qionglai City wheat planting base and Guangyuan City Qingchuan County wheat planting base, experimental cultivar is river agriculture 11, and test period was carried out for continuous 2 years 2014 and 2015.Place Reason arranges as follows(It is shown in Table 1):
Table 1:
Process by more than is carried out being watered spraying by respective concentration in the wheat later stage, and result is shown in Table 2, table 3:
Table 2:The impact of different disposal and application concentration to wheat lodging resistance(Chengdu Qionglai)
The impact of table 3, different disposal and application concentration to wheat lodging resistance(Guangyuan Qing Chuan)
From table 2 and table 3 as can be seen that the wheat for having sprayed plant growth regulator is compared with clear water control group, there is significantly anti- Lodging is acted on;The paclobutrazol microemulsion of 25% TrinexAN_SNacethyl provided by the present invention+2% is anti-fall with 15% paclobutrazol wettable powder and 25% The plant growth regulator of emulsifiable concentrate both one-components is compared, and has notable difference, Jing continuous two on wheat lodging resistance Year two places verification experimental verification, otherness substantially, effect stability.
Above-described embodiment is that the above to the present invention is further described, but this should not be interpreted as in the present invention The scope for stating theme is only limitted to above-described embodiment.All technologies realized based on the above belong to the scope of the present invention.

Claims (6)

1. the microemulsion of TrinexAN_SNacethyl and paclobutrazol is contained, by weight percentage including following components:
TrinexAN_SNacethyl 1~40%,
Paclobutrazol 1~10%,
Solvent 1~20%,
Cosolvent 1~15%,
Emulsifying agent 10~50%,
Antifreezing agent 1~10%,
Water surplus.
2. the microemulsion containing TrinexAN_SNacethyl and paclobutrazol as claimed in claim 1, it is characterised in that include by weight percentage with Lower component:
TrinexAN_SNacethyl 10~30%
Paclobutrazol 3~8%
Solvent 6~18%
Cosolvent 5~10%
Emulsifying agent 20~40%
Antifreezing agent 3~6%
Water surplus.
3. the microemulsion of TrinexAN_SNacethyl and paclobutrazol is contained as claimed in claim 1 or 2, it is characterised in that solvent is toluene, diformazan At least one in benzene, ethanol, methyl alcohol, acetone, cyclohexanone, dimethyl sulfoxide.
4. the microemulsion containing TrinexAN_SNacethyl and paclobutrazol as claimed in claim 1 or 2, it is characterised in that cosolvent be normal propyl alcohol, At least one in isopropanol, n-butanol, isobutanol, n-octyl alcohol.
5. the microemulsion of TrinexAN_SNacethyl and paclobutrazol is contained as claimed in claim 1 or 2, it is characterised in that emulsifying agent is poly- for alkyl phenol Oxygen vinethene, AEO, alkylbenzenesulfonate, alkyl sulfate, styrylphenol polyoxyethylene ether, alkane Base fluosite APEO, polyoxyethylene 20 sorbitan monolaurate, polyethenoxy sorbitan list oleic acid At least one in ester, disecoctylmaleate sodium sulfonate, polyoxyethylene alkyl ether sulfate.
6. the microemulsion containing TrinexAN_SNacethyl and paclobutrazol as claimed in claim 1 or 2, it is characterised in that antifreezing agent be ethylene glycol, At least one in propane diols, glycerine, urea.
CN201610881302.3A 2016-10-10 2016-10-10 Microemulsion containing trinexapac-ethyl and paclobutrazol Pending CN106614616A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107361059A (en) * 2017-08-14 2017-11-21 四川省兰月科技有限公司 Microemulsion containing amino-oligosaccharide and uniconazole P
WO2024036384A1 (en) * 2022-08-19 2024-02-22 Adama Australia Pty Limited Novel trinexapac-ethyl formulations

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Publication number Priority date Publication date Assignee Title
US20050032648A1 (en) * 2002-12-27 2005-02-10 Cooper Raymond B. Plant growth regulation compositions and methods using gibberellin biosynthesis inhibitor combinations
CN102238867A (en) * 2008-12-05 2011-11-09 先正达参股股份有限公司 Improved turfgrass quality
CN102826916A (en) * 2012-09-21 2012-12-19 黑龙江禾田丰泽兴农科技开发有限公司 Method for preparing microemulsion by mixing pesticide, liquid fertilizer and bioemulsifier
CN103141485A (en) * 2013-03-27 2013-06-12 四川国光农化股份有限公司 Plant growth regulator and preparation containing paclobutrazol and mepiquat chloride and preparation methods thereof
CN105981733A (en) * 2015-02-06 2016-10-05 陕西美邦农药有限公司 Pesticide composition containing antibacterial peptide

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050032648A1 (en) * 2002-12-27 2005-02-10 Cooper Raymond B. Plant growth regulation compositions and methods using gibberellin biosynthesis inhibitor combinations
CN102238867A (en) * 2008-12-05 2011-11-09 先正达参股股份有限公司 Improved turfgrass quality
CN102826916A (en) * 2012-09-21 2012-12-19 黑龙江禾田丰泽兴农科技开发有限公司 Method for preparing microemulsion by mixing pesticide, liquid fertilizer and bioemulsifier
CN103141485A (en) * 2013-03-27 2013-06-12 四川国光农化股份有限公司 Plant growth regulator and preparation containing paclobutrazol and mepiquat chloride and preparation methods thereof
CN105981733A (en) * 2015-02-06 2016-10-05 陕西美邦农药有限公司 Pesticide composition containing antibacterial peptide

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107361059A (en) * 2017-08-14 2017-11-21 四川省兰月科技有限公司 Microemulsion containing amino-oligosaccharide and uniconazole P
WO2024036384A1 (en) * 2022-08-19 2024-02-22 Adama Australia Pty Limited Novel trinexapac-ethyl formulations

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