CN106538594A - A kind of agricultural gyphosate solution with thickening builder and preparation method thereof - Google Patents
A kind of agricultural gyphosate solution with thickening builder and preparation method thereof Download PDFInfo
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- CN106538594A CN106538594A CN201610933584.7A CN201610933584A CN106538594A CN 106538594 A CN106538594 A CN 106538594A CN 201610933584 A CN201610933584 A CN 201610933584A CN 106538594 A CN106538594 A CN 106538594A
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- parts
- gyphosate solution
- container
- agricultural
- dichloro
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
- A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/24—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients to enhance the sticking of the active ingredients
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
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- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of agricultural gyphosate solution with thickening builder, including the mass fraction of following components and each component is：30 50 parts of the gyphosate solution of 30% purity, 8 12 parts of amidogen ether APG, 58 parts of empgen BB, 35 parts of cetyl trimethylammonium bromide, 47 parts of sodium N-lauroyl sarcosinate, 10 14 parts of polyethylene glycol, 25 parts of N methyl pyrrolidones, 13 parts of penta chrysanthemum fat of dichloro alkynes, the gyphosate solution that the present invention is provided is after spraying, the penta chrysanthemum fat of dichloro alkynes contained in gyphosate solution has potent absorption affinity with amidogen ether APG, glyphosate stoste is made to adsorb in plant surface, improve weeding ability, containing sodium N-lauroyl sarcosinate, cetyl trimethylammonium bromide and N methyl pyrrolidones make glyphosate have extremely strong affinity, glyphosate stoste is made to be more easy to the inside into plant, instant effect, weeding ability is strong.
Description
Technical field
The present invention relates to gyphosate solution technical field, specially a kind of agricultural glyphosate water with thickening builder
Agent and preparation method thereof.
Background technology
The herbicidal properties of glyphosate be 1971 by discoveries such as U.S.'s D.D. Bairds, by Monsanto Company's Development and Production
, the important kind of World Herbicide is had become to the eighties in last century.Glyphosate goes out life for the chronic wide spectrum of inner sucting conduction type
Property herbicide, enolpyruvyl shikimene phosphate synthase in major inhibitor body, so as to suppress shikimene to phenylalanine, cruel
The conversion of propylhomoserin and tryptophan, making the synthesis of protein be interfered causes Plant death.Glyphosate is after cauline leaf absorbs
Plant parts are transmitted to, the plant of the section more than 40 such as unifacial leaf and dicotyledonous, annual and perennial, draft and shrub can be prevented and kill off
Thing.Glyphosate is combined with the metal ion such as iron, aluminium quickly and is lost activity after burying, and the seed and soil to hiding in soil is micro-
Biology has no adverse effects.And the adhesive force and affinity using increase glyphosate stoste of glyphosate surface modifier, make glyphosate
Stoste is more easy to be absorbed by plants, and reaches more preferable herbicidal effect, and the gyphosate solution of market sale, take effect relatively slow, weeding effect
It is really undesirable, for this purpose, we provide a kind of agricultural gyphosate solution with thickening builder.
The content of the invention
It is an object of the invention to provide a kind of agricultural gyphosate solution with thickening builder and preparation method thereof,
To solve the problems, such as to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme：It is a kind of agricultural with the careless sweet of thickening builder
Phosphine aqua, including the mass fraction of following components and each component is：Gyphosate solution 30-50 parts of 30% purity, amidogen ether alkyl
Many glucosides 8-12 parts, empgen BB 5-8 parts, cetyl trimethylammonium bromide 3-5 parts, sodium N-lauroyl sarcosinate 4-
7 parts, polyethylene glycol 10-14 parts, 1-METHYLPYRROLIDONE 2-5 parts, penta chrysanthemum fat 1-3 parts of dichloro alkynes.
Preferably, including following components and the mass fraction of each component is：Gyphosate solution 35-45 parts of 30% purity,
Amidogen ether APG 9-11 parts, empgen BB 6-7.5 parts, cetyl trimethylammonium bromide 3.5-4.5 parts, bay
Sarcosinate 4.5-6.5 parts, polyethylene glycol 11-13 parts, 1-METHYLPYRROLIDONE 3-4 parts, penta chrysanthemum fat 1.5-2.5 of dichloro alkynes
Part.
Preferably, including following components and the mass fraction of each component is：40 parts of the gyphosate solution of 30% purity, amidogen ether
10 parts of APG, 6.5 parts of empgen BB, 4 parts of cetyl trimethylammonium bromide, sodium N-lauroyl sarcosinate 5
Part, 12 parts of polyethylene glycol, 3.5 parts of 1-METHYLPYRROLIDONE, 2 parts of penta chrysanthemum fat of dichloro alkynes.
A kind of preparation method of the agricultural gyphosate solution with thickening builder, comprises the following steps：
S1：Amidogen ether APG and penta chrysanthemum fat raw material of dichloro alkynes are added in container, and container is heated, in container
Temperature be 50-55 DEG C, be stirred, mixing time be 10-15 minutes；
S2：Temperature in container is reduced to into 30-35 DEG C, is then added successively empgen BB, the moon into container
Osmanthus sarcosinate and 1-METHYLPYRROLIDONE, stir, and mixing time is 10-15 minutes；
S3：Temperature in container is reduced to into 10-15 DEG C, then adds the glyphosate water of 30% purity into container successively
Agent, cetyl trimethylammonium bromide and polyethylene glycol, stir, and mixing time is 5-10 minutes；
S4：Liquid in container is filtered, impurity therein is removed, is carried out packing and storing.
Compared with prior art, the invention has the beneficial effects as follows：After spraying, grass is sweet for the gyphosate solution that the present invention is provided
The penta chrysanthemum fat of dichloro alkynes contained in phosphine aqua has potent absorption affinity with amidogen ether APG, is planting the absorption of glyphosate stoste
Thing surface, improves weeding ability, containing sodium N-lauroyl sarcosinate, cetyl trimethylammonium bromide and 1-METHYLPYRROLIDONE
Make glyphosate that there is extremely strong affinity, make glyphosate stoste be more easy to the inside into plant, instant effect, weeding ability are strong.
Specific embodiment
Below in conjunction with embodiments of the invention, the technical scheme in the embodiment of the present invention is clearly and completely retouched
State, it is clear that described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based on the present invention
In embodiment, the every other enforcement obtained under the premise of creative work is not made by those of ordinary skill in the art
Example, belongs to the scope of protection of the invention.
Embodiment one
A kind of agricultural gyphosate solution with thickening builder, including the mass fraction of following components and each component
For：40 parts of the gyphosate solution of 30% purity, 10 parts of amidogen ether APG, 6.5 parts of empgen BB, cetyl three
4 parts of methyl bromide ammonium, 5 parts of sodium N-lauroyl sarcosinate, 12 parts of polyethylene glycol, 3.5 parts of 1-METHYLPYRROLIDONE, penta chrysanthemum of dichloro alkynes
2 parts of fat.
A kind of preparation method of the agricultural gyphosate solution with thickening builder, comprises the following steps：
S1：Amidogen ether APG and penta chrysanthemum fat raw material of dichloro alkynes are added in container, and container is heated, in container
Temperature be 50 DEG C, be stirred, mixing time be 14 minutes；
S2：Temperature in container is reduced to into 32 DEG C, then adds empgen BB, lauroyl into container successively
Base sodium sarcosinate and 1-METHYLPYRROLIDONE, stir, and mixing time is 12 minutes；
S3：Temperature in container is reduced to into 15 DEG C, then add into container successively 30% purity gyphosate solution,
Cetyl trimethylammonium bromide and polyethylene glycol, stir, and mixing time is 8 minutes；
S4：Liquid in container is filtered, impurity therein is removed, is carried out packing and storing.
Embodiment two
A kind of agricultural gyphosate solution with thickening builder, including the mass fraction of following components and each component
For：45 parts of the gyphosate solution of 30% purity, 11 parts of amidogen ether APG, 6 parts of empgen BB, cetyl front three
3 parts of base ammonium bromide, 5 parts of sodium N-lauroyl sarcosinate, 13 parts of polyethylene glycol, 4 parts of 1-METHYLPYRROLIDONE, penta chrysanthemum fat 3 of dichloro alkynes
Part.
A kind of preparation method of the agricultural gyphosate solution with thickening builder, comprises the following steps：
S1：Amidogen ether APG and penta chrysanthemum fat raw material of dichloro alkynes are added in container, and container is heated, in container
Temperature be 53 DEG C, be stirred, mixing time be 12 minutes；
S2：Temperature in container is reduced to into 35 DEG C, then adds empgen BB, lauroyl into container successively
Base sodium sarcosinate and 1-METHYLPYRROLIDONE, stir, and mixing time is 10 minutes；
S3：Temperature in container is reduced to into 12 DEG C, then add into container successively 30% purity gyphosate solution,
Cetyl trimethylammonium bromide and polyethylene glycol, stir, and mixing time is 6 minutes；
S4：Liquid in container is filtered, impurity therein is removed, is carried out packing and storing.
For gyphosate solution proposed by the present invention is for the weeding experiment of weeds in farmland：
Experiment purpose：
The test adsorptivity of gyphosate solution with thickening builder proposed by the present invention and building performance.
Test method：
4 pieces of the clover seedling field (being respectively labeled as A, B, C, D) of one mu of size is taken, wherein two pieces of clover fields of A, B adopt cauline leaf
The gyphosate solution of the spray-on process sprinkling present invention, in addition agriculture of the two pieces of clover fields of C, D using cauline leaf spray-on process sprinkling market sale
Up to herbicide, then respectively B clovers field and D clovers field is uniformly sprayed using sprayer using clear water, then for 4 pieces
Observed after three days and after seven days after the spray of clover field.
Experimental result：
After three days：The universal yellowing of clover seedling in A clovers field, and it is withered part occur；Clover seedling in C clovers field occurs
, there is not withered situation in local yellowing；The universal yellowing of clover seedling in B clovers field；The clover seedling in D clovers field occurs fragmentary general
It is yellow.
After seven days：It is withered that large area occurs in clover seedling in A clovers field；The universal yellowing of clover seedling in C clovers field, and go out
Now part is withered；The universal yellowing of clover seedling in B clovers field, and it is withered part occur；It is general that part occurs in the clover seedling in D clovers field
It is yellow.
From above-mentioned experiment, the gyphosate solution with thickening builder proposed by the present invention has potent absorption
Ability and affinity, using effect are good, instant effect.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding can carry out various changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention
And modification, the scope of the present invention be defined by the appended.
Claims (4)
1. a kind of agricultural with the gyphosate solution for viscosifying builder, it is characterised in that：Including following components and each component
Mass fraction is：Gyphosate solution 30-50 parts of 30% purity, amidogen ether APG 8-12 parts, empgen BB 5-8
Part, cetyl trimethylammonium bromide 3-5 parts, sodium N-lauroyl sarcosinate 4-7 parts, polyethylene glycol 10-14 parts, N- methylpyrroles
Alkanone 2-5 part, penta chrysanthemum fat 1-3 parts of dichloro alkynes.
2. according to claim 1 a kind of agricultural with the gyphosate solution for viscosifying builder, it is characterised in that：Including
The mass fraction of following components and each component is：Gyphosate solution 35-45 parts of 30% purity, amidogen ether APG 9-11
Part, empgen BB 6-7.5 parts, cetyl trimethylammonium bromide 3.5-4.5 parts, sodium N-lauroyl sarcosinate 4.5-
6.5 parts, polyethylene glycol 11-13 parts, 1-METHYLPYRROLIDONE 3-4 parts, penta chrysanthemum fat 1.5-2.5 parts of dichloro alkynes.
3. according to claim 1 a kind of agricultural with the gyphosate solution for viscosifying builder, it is characterised in that：Including
The mass fraction of following components and each component is：40 parts of the gyphosate solution of 30% purity, 10 parts of amidogen ether APG, 12
6.5 parts of alkyl betaine, 4 parts of cetyl trimethylammonium bromide, 5 parts of sodium N-lauroyl sarcosinate, 12 parts of polyethylene glycol, N- first
3.5 parts of base pyrrolidones, 2 parts of penta chrysanthemum fat of dichloro alkynes.
4. a kind of preparation method of the agricultural gyphosate solution with thickening builder as claimed in claim 1, its feature
It is：Comprise the following steps：
S1：Amidogen ether APG and penta chrysanthemum fat raw material of dichloro alkynes are added in container, and container are heated, the temperature in container
Spend for 50-55 DEG C, be stirred, mixing time is 10-15 minutes；
S2：Temperature in container is reduced to into 30-35 DEG C, then adds empgen BB, lauroyl into container successively
Base sodium sarcosinate and 1-METHYLPYRROLIDONE, stir, and mixing time is 10-15 minutes；
S3：Temperature in container is reduced to into 10-15 DEG C, then add into container successively 30% purity gyphosate solution,
Cetyl trimethylammonium bromide and polyethylene glycol, stir, and mixing time is 5-10 minutes；
S4：Liquid in container is filtered, impurity therein is removed, is carried out packing and storing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610933584.7A CN106538594A (en) | 2016-11-01 | 2016-11-01 | A kind of agricultural gyphosate solution with thickening builder and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610933584.7A CN106538594A (en) | 2016-11-01 | 2016-11-01 | A kind of agricultural gyphosate solution with thickening builder and preparation method thereof |
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| CN106538594A true CN106538594A (en) | 2017-03-29 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610933584.7A Pending CN106538594A (en) | 2016-11-01 | 2016-11-01 | A kind of agricultural gyphosate solution with thickening builder and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108513980A (en) * | 2018-04-01 | 2018-09-11 | 南京拓际生物科技有限公司 | A kind of thickening type glyphosate, the compound aqueous auxiliary agent of glufosinate-ammonium and its preparation process |
| CN111328800A (en) * | 2020-04-13 | 2020-06-26 | 南京拓呗新材料科技有限公司 | Low-foam tackifying glyphosate aqueous agent assistant and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1306396A (en) * | 1998-06-04 | 2001-08-01 | 汉普郡化学公司 | N-acyl sarcosinates as glyphosate adjuvants |
| CN1545881A (en) * | 2003-12-04 | 2004-11-17 | 吴云清 | Synergy auxiliary agent of glyphosate isopropyl amine brine agent |
| CN1277473C (en) * | 1998-11-23 | 2006-10-04 | 孟山都公司 | Highly concentrated aqueous glyphosate compositions |
| WO2011008281A1 (en) * | 2009-07-14 | 2011-01-20 | Rhodia Operations | Agricultural adjuvant compositions, pesticide compositions, and methods for using such compositions |
| CN104068048A (en) * | 2014-05-27 | 2014-10-01 | 安徽省益农化工有限公司 | Glyphosate synergist |
-
2016
- 2016-11-01 CN CN201610933584.7A patent/CN106538594A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1306396A (en) * | 1998-06-04 | 2001-08-01 | 汉普郡化学公司 | N-acyl sarcosinates as glyphosate adjuvants |
| CN1277473C (en) * | 1998-11-23 | 2006-10-04 | 孟山都公司 | Highly concentrated aqueous glyphosate compositions |
| CN1545881A (en) * | 2003-12-04 | 2004-11-17 | 吴云清 | Synergy auxiliary agent of glyphosate isopropyl amine brine agent |
| WO2011008281A1 (en) * | 2009-07-14 | 2011-01-20 | Rhodia Operations | Agricultural adjuvant compositions, pesticide compositions, and methods for using such compositions |
| CN104068048A (en) * | 2014-05-27 | 2014-10-01 | 安徽省益农化工有限公司 | Glyphosate synergist |
Non-Patent Citations (1)
| Title |
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| 李达潮: "表面活性剂对草甘膦药效的影响", 《农药》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108513980A (en) * | 2018-04-01 | 2018-09-11 | 南京拓际生物科技有限公司 | A kind of thickening type glyphosate, the compound aqueous auxiliary agent of glufosinate-ammonium and its preparation process |
| CN111328800A (en) * | 2020-04-13 | 2020-06-26 | 南京拓呗新材料科技有限公司 | Low-foam tackifying glyphosate aqueous agent assistant and preparation method thereof |
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Application publication date: 20170329 |