CN105742145B - A kind of integral structure of integrated TEM fluorescent screens and STEM detectors - Google Patents

A kind of integral structure of integrated TEM fluorescent screens and STEM detectors Download PDF

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Publication number
CN105742145B
CN105742145B CN201610187670.8A CN201610187670A CN105742145B CN 105742145 B CN105742145 B CN 105742145B CN 201610187670 A CN201610187670 A CN 201610187670A CN 105742145 B CN105742145 B CN 105742145B
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China
Prior art keywords
lens barrel
fluorescent screens
stem
detectors
tem
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CN201610187670.8A
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CN105742145A (en
Inventor
王义林
张大梁
周向志
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Zhenjiang Lehua Technology Co Ltd
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Zhenjiang Lehua Technology Co Ltd
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Priority to CN201610187670.8A priority Critical patent/CN105742145B/en
Priority claimed from CN201410345490.9A external-priority patent/CN104091745B/en
Publication of CN105742145A publication Critical patent/CN105742145A/en
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/26Electron or ion microscopes; Electron or ion diffraction tubes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/02Details
    • H01J37/22Optical, image processing or photographic arrangements associated with the tube
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/02Details
    • H01J37/244Detectors; Associated components or circuits therefor
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/26Electron or ion microscopes; Electron or ion diffraction tubes
    • H01J37/28Electron or ion microscopes; Electron or ion diffraction tubes with scanning beams

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Electron Sources, Ion Sources (AREA)
  • Microscoopes, Condenser (AREA)

Abstract

The invention discloses a kind of integral structure of integrated TEM fluorescent screens and STEM detectors, belong to the accessory structure design field of transmission electron microscope, the integral structure of integrated the TEM fluorescent screens and STEM detectors passes through the mounting and adjusting part on the sidepiece interface of lens barrel, and on the adjustment part inside lens barrel integrated installation TEM fluorescent screens and STEM detectors, so that only needing to change position of the adjustment part in transmission electron microscope lens barrel, just TEM fluorescent screens or STEM detectors can be realized to receive electron beam, so as to meet a sidepiece interface of lens barrel while installing the purpose of CCD camera fluorescent screen (TEM fluorescent screens) and STEM detectors, and then meet function maximized demand of the user for transmission electron microscope, realize the cost performance overflowed.

Description

A kind of integral structure of integrated TEM fluorescent screens and STEM detectors
The application is application number 201410345490.9,18 days July 2014 applying date, a kind of denomination of invention " integrated TEM The divisional application of the integral structure of fluorescent screen and STEM detectors ".
Technical field
The present invention relates to transmission electron microscope accessory structure design, more particularly to a kind of integrated TEM fluorescent screens and The integral structure of STEM detectors.
Background technology
Transmission electron microscope Transmission Electron Microscope, abbreviation TEM, transmission electron microscope It is a kind of high-resolution for being imaged with electromagnetism transmission focusing, high-amplification-factor using the extremely short electron beam of wavelength as light source Electronic optical instrument.
For shooting high-resolution electronic micro-image during transmission electron microscope use, electronic diffraction is shot and right Sample carries out the different application purposes such as in-situ study and make it that used CCD camera type is different, so, in a transmission electricity Single CCD camera configuration is equipped with sub- microscope to be difficult to meet needs.To solve the above problems, currently existing scheme is in transmission electricity Bottom is installed on sub- microscope and inserts formula CCD camera and side-plug-in CCD camera, formula CCD camera is inserted at bottom and side-plug-in CCD camera is pacified respectively Mounted in the egative film room bottom of transmission electron microscope and lens barrel sidepiece.
Scanning transmission electron microscope Scanning Transmission Electron Microscope, abbreviation STEM, It is quickly to be scanned Electron Beam Focusing to sample surfaces and in sample surfaces using magnetic lenses, by penetration of electrons sample into Picture.In scanning-mode it, electron source launches electronics, by before sample magnetic lenses by electron-beam convergence into small yardstick beam Spot, beam spot is focused on after specimen surface, and a region of point by point scanning sample is controlled by coil.A bit is scanned every Meanwhile, the STEM detectors below sample synchronously receive electronics.The signal received corresponding to the detector of each scan position Current strength is converted into be shown on fluorescent screen or computer display.Use STEM light fields detector or STEM dark field detectors STEM bright field images and STEM darkfield images can be then obtained respectively.STEM light fields detector and STEM dark field detectors need peace Mounted in transmission electron microscope lens barrel sidepiece interface.
The expense of one transmission electron microscope generally reaches millions of RMB, therefore, aobvious for a transmitted electron Micro mirror, people usually require to install various annexes additional, so that function is maximized, under prior art conditions, transmission electron microscope Sidepiece interface quantity is restricted in installation place, after STEM light fields detector and dark field detector is mounted with, it is impossible to pacify Fill side-plug-in CCD camera;It is mounted with after side-plug-in CCD camera, then the light/dark field detectors of STEM can only choose to install one, and then Transmission electron microscope is caused to reach the maximized demand of function.
The content of the invention
There is provided a kind of integrated TEM fluorescent screens and STEM detectors for above-mentioned problem for the purpose of the present invention Integral structure, to overcome transmission electron microscope sidepiece interface of the prior art to be restricted in installation place, causes not The problem of function maximized demand can be realized, so that side-plug-in CCD camera can either be installed, can install the spy of STEM light and shades again Device is surveyed, while CCD camera fluorescent screen also is installed in sidepiece, and then it is maximum for the function of transmission electron microscope to meet user The demand of change, realizes the cost performance overflowed.
To achieve these goals, the technical scheme taken of the present invention is:.
A kind of integral structure of integrated TEM fluorescent screens and STEM detectors, it is characterised in that including:Connect with sidepiece Mouthful lens barrel and by the sidepiece interface be arranged on the lens barrel on adjustment part, the adjustment part be sliding equipment or Switching mechanism, the face of facing of the adjustment part is shaped as right-angled trapezium, and a part for the adjustment part is located at the lens barrel It is internal;The upper bottom for facing face of the adjustment part and the waist for facing face of the adjustment part inside the lens barrel it Between angle be 135 °;TEM fluorescent screens and STEM detectors are integrated with the adjustment part inside the lens barrel;It is described TEM fluorescent screens are installed on the central plane for facing face of the adjustment part inside the lens barrel, the STEM detectors On the upper bottom surface up or down bottom surface for facing face for the adjustment part structure being installed on inside the lens barrel.
In one embodiment of the invention, the adjustment part is sliding equipment.
In one embodiment of the invention, one end that face is right angle of facing of the sliding equipment is located at the outer of the lens barrel Portion.
In one embodiment of the invention, the TEM fluorescent screens are installed on the sliding equipment inside the lens barrel The central plane for facing face on, the STEM detectors are installed on the face of facing of the sliding equipment inside the lens barrel On upper bottom surface.
In one embodiment of the invention, the adjustment part is switching mechanism.
In one embodiment of the invention, one end that face is right angle of facing of the switching mechanism is located at the outer of the lens barrel Portion.
In one embodiment of the invention, the TEM fluorescent screens are installed on the switching mechanism inside the lens barrel The central plane for facing face on, the STEM detectors are installed on the face of facing of the switching mechanism inside the lens barrel On bottom surface.
Compared with prior art, the beneficial effect of the technical program is:
The integral structure of a kind of integrated TEM fluorescent screens and STEM detectors that the present invention is provided, by the side of lens barrel Mounting and adjusting part on portion's interface, and integrated installation TEM fluorescent screens and STEM detections on the adjustment part inside lens barrel Device so that only need to change position of the adjustment part in transmission electron microscope lens barrel, just can realize TEM fluorescent screens or STEM detectors receive electron beam, so as to meet sidepiece interface of lens barrel while installing CCD camera fluorescent screen (TEM Fluorescent screen) and STEM detectors purpose, and then meet function maximized demand of the user for transmission electron microscope, it is real The cost performance now overflowed.
Brief description of the drawings
By reading the detailed description made with reference to the following drawings to non-limiting example, the present invention and its feature, outside Shape and advantage will become more apparent.Identical mark indicates identical part in whole accompanying drawings.Not deliberately according to than Example draws accompanying drawing, it is preferred that emphasis is show the purport of the present invention.
Fig. 1 be the embodiment of the present invention 1 provide integrated TEM fluorescent screens and STEM detectors integral structure it is standby when Structural representation.
Fig. 2 is that the integrated TEM fluorescent screens of the offer of the embodiment of the present invention 1 and the integral structure of STEM detectors are in position Structural representation during A.
Fig. 3 is that the integrated TEM fluorescent screens of the offer of the embodiment of the present invention 1 and the integral structure of STEM detectors are in position Structural representation during B.
Fig. 4 be the embodiment of the present invention 2 provide integrated TEM fluorescent screens and STEM detectors integral structure it is standby when Structural representation.
Fig. 5 is that the integrated TEM fluorescent screens of the offer of the embodiment of the present invention 2 and the integral structure of STEM detectors are in position Structural representation during A.
Fig. 6 is that the integrated TEM fluorescent screens of the offer of the embodiment of the present invention 2 and the integral structure of STEM detectors are in position Structural representation during B.
Embodiment
The present invention is further illustrated with specific embodiment below in conjunction with the accompanying drawings, but not as the limit of the present invention It is fixed.
Embodiment 1:
Fig. 1 be the embodiment of the present invention 1 provide integrated TEM fluorescent screens and STEM detectors integral structure it is standby when Structural representation;Fig. 2 is that the integrated TEM fluorescent screens of the offer of the embodiment of the present invention 1 and the integral structure of STEM detectors are in The structural representation during A of position;Fig. 3 is the integration of integrated TEM fluorescent screens and STEM detectors that the embodiment of the present invention 1 is provided Structure is in the structural representation during B of position;As illustrated, integrated TEM fluorescent screens and STEM that the embodiment of the present invention 1 is provided are visited Surveying the integral structure of device includes:Lens barrel 101 with sidepiece interface and the adjustment by sidepiece interface on lens barrel 101 Part, in the embodiment of the present invention 1, the adjustment part is sliding equipment 102, and the face of facing of sliding equipment 102 is shaped as always Angle is trapezoidal, and a part for sliding equipment 102 is located inside lens barrel 101, and another part of sliding equipment 102 is located at lens barrel 101 Outside, and sliding equipment 102 face face be right angle one end be located at lens barrel 101 outside, the other end of sliding equipment 102 Positioned at the inside of lens barrel 101, meanwhile, it is integrated with TEM fluorescent screens 104 and STEM on the sliding equipment 102 inside lens barrel 101 Detector 103, specifically, TEM fluorescent screens 104 are mounted on the central plane for facing face of the sliding equipment 102 inside lens barrel 101 On, STEM detectors 103 are mounted on the upper bottom surface for facing face of the sliding equipment 102 inside lens barrel 101.
In the integrated TEM fluorescent screens and the integral structure of STEM detectors that the embodiment of the present invention 1 is provided, sliding equipment Angle between the 102 upper bottom for facing face and the waist for facing face of the sliding equipment 102 inside lens barrel 101 is 135 °, Angle between the bottom for facing face of sliding equipment 102 and the waist for facing face of the sliding equipment 102 inside lens barrel 101 For 45 °, the sliding equipment 102 of the angle is set, ensure that the image of TEM fluorescent screens 104 is protected after being reflected by reflecting prism Hold original scale.
In the integrated TEM fluorescent screens and the integral structure of STEM detectors that the embodiment of the present invention 1 is provided, in addition to one CCD camera 105, CCD camera 105 is arranged on the other side interface of lens barrel 101, and position and the slip of CCD camera 105 The position of mechanism 102 is just corresponding.
It is standby in the integral structure of the integrated TEM fluorescent screens and STEM detectors that are provided using the embodiment of the present invention 1 In the case of, electron beam 11 reflects without any part, so that image will not be formed;When sliding equipment 102 is pushed into position A, Electron beam 11 is reflexed in CCD camera 105 by TEM fluorescent screens 104, so as to realize the function of transmission electron microscope; Further, when sliding equipment 102 being pushed into position B, electron beam 11 is irradiated on STEM detectors 103, so as to be converted into electricity Intensity of flow is shown on fluorescent screen or computer display, completes the function of scanning transmission electron microscope.
So, the embodiment of the present invention 1 provide integrated TEM fluorescent screens and STEM detectors integral structure, by Sliding equipment is installed on the sidepiece interface of lens barrel, and on the sliding equipment inside lens barrel integrated installation TEM fluorescent screens and STEM detectors so that only need to change position of the sliding equipment in transmission electron microscope lens barrel, just can realize that TEM is glimmering Optical screen or STEM detectors receive electron beam, so as to meet a sidepiece interface of lens barrel while installing CCD camera with glimmering The purpose of optical screen (TEM fluorescent screens) and STEM detectors, and then meet function maximization of the user for transmission electron microscope Demand, realize the cost performance that overflows.
Embodiment 2:
Fig. 4 be the embodiment of the present invention 2 provide integrated TEM fluorescent screens and STEM detectors integral structure it is standby when Structural representation;Fig. 5 is that the integrated TEM fluorescent screens of the offer of the embodiment of the present invention 2 and the integral structure of STEM detectors are in The structural representation during A of position;Fig. 6 is the integration of integrated TEM fluorescent screens and STEM detectors that the embodiment of the present invention 2 is provided Structure is in the structural representation during B of position;As illustrated, integrated TEM fluorescent screens and STEM that the embodiment of the present invention 2 is provided are visited Surveying the integral structure of device includes:Lens barrel 201 with sidepiece interface and the adjustment by sidepiece interface on lens barrel 201 Part, in the embodiment of the present invention 2, the adjustment part is switching mechanism 202, and the face of facing of switching mechanism 202 is shaped as always Angle is trapezoidal, and a part for switching mechanism 202 is located inside lens barrel 201, and another part of switching mechanism 202 is located at lens barrel 201 Outside, and switching mechanism 202 face face be right angle one end be located at lens barrel 201 outside, the other end of switching mechanism 202 Positioned at the inside of lens barrel 201, meanwhile, it is integrated with TEM fluorescent screens 204 and STEM on the switching mechanism 202 inside lens barrel 201 Detector 203, specifically, TEM fluorescent screens 204 are mounted on the central plane for facing face of the switching mechanism 202 inside lens barrel 201 On, STEM detectors 203 are mounted on the bottom surface for facing face of the switching mechanism 202 inside lens barrel 201.
In the integrated TEM fluorescent screens and the integral structure of STEM detectors that the embodiment of the present invention 2 is provided, switching mechanism Angle between the 202 upper bottom for facing face and the waist for facing face of the switching mechanism 202 inside lens barrel 201 is 135 °, Angle between the bottom for facing face of switching mechanism 202 and the waist for facing face of the switching mechanism 202 inside lens barrel 201 For 45 °, the switching mechanism 202 of the angle is set, ensure that the image of TEM fluorescent screens 204 is protected after being reflected by reflecting prism Hold original scale.
In the integrated TEM fluorescent screens and the integral structure of STEM detectors that the embodiment of the present invention 2 is provided, in addition to one CCD camera 205, CCD camera 205 is arranged on the other side interface of lens barrel 201, and position and the upset of CCD camera 205 The position of mechanism 202 is just corresponding.
It is standby in the integral structure of the integrated TEM fluorescent screens and STEM detectors that are provided using the embodiment of the present invention 2 In the case of, electron beam 22 reflects without any part, so that image will not be formed;When switching mechanism 202 is pushed into position A, Electron beam 22 is reflexed in CCD camera 205 by TEM fluorescent screens 204, so as to realize the function of transmission electron microscope; Further, when switching mechanism 202 is overturn to position B, electron beam 22 is irradiated on STEM detectors 203, so as to be converted into Current strength is shown on fluorescent screen or computer display, completes the function of scanning transmission electron microscope.
So, the embodiment of the present invention 2 provide integrated TEM fluorescent screens and STEM detectors integral structure, by Switching mechanism is installed on the sidepiece interface of lens barrel, and on the switching mechanism inside lens barrel integrated installation TEM fluorescent screens and STEM detectors so that only need to change position of the switching mechanism in transmission electron microscope lens barrel, just can realize that TEM is glimmering Optical screen or STEM detectors receive electron beam, so as to meet a sidepiece interface of lens barrel while installing CCD camera with glimmering The purpose of optical screen (TEM fluorescent screens) and STEM detectors, and then meet function maximization of the user for transmission electron microscope Demand, realize the cost performance that overflows.
In summary, the integral structure of integrated TEM fluorescent screens and STEM detectors provided in an embodiment of the present invention, passes through The mounting and adjusting part on the sidepiece interface of lens barrel, and the integrated installation TEM fluorescent screens on the adjustment part inside lens barrel With STEM detectors so that only need to change position of the adjustment part in transmission electron microscope lens barrel, just can realize TEM Fluorescent screen or STEM detectors receive electron beam, are used while installing CCD camera so as to meet a sidepiece interface of lens barrel The purpose of fluorescent screen (TEM fluorescent screens) and STEM detectors, and then it is maximum for the function of transmission electron microscope to meet user The demand of change, realizes the cost performance overflowed.
It should be appreciated by those skilled in the art that those skilled in the art combine prior art and above-described embodiment can be real The existing change case, will not be described here.Such change case has no effect on the substantive content of the present invention, will not be described here.
Presently preferred embodiments of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned Particular implementation, wherein the equipment and structure be not described in detail to the greatest extent are construed as giving reality with the common mode in this area Apply;Any those skilled in the art, many possible variations and modification are made not departing from technical solution of the present invention, or The equivalent embodiment of equivalent variations is revised as, this has no effect on the substantive content of the present invention.Therefore, it is every without departing from skill of the present invention The content of art scheme, according to the present invention technical spirit to it is made for any of the above embodiments it is any it is simple modification, equivalent variations and Modification, still fall within technical solution of the present invention protection in the range of.

Claims (3)

1. the integral structure of a kind of integrated TEM fluorescent screens and STEM detectors, it is characterised in that including:Connect with sidepiece Mouthful lens barrel and by the sidepiece interface be arranged on the lens barrel on adjustment part, the adjustment part be sliding equipment or Switching mechanism, the face of facing of the adjustment part is shaped as right-angled trapezium, and a part for the adjustment part is located at the lens barrel It is internal;The upper bottom for facing face of the adjustment part and the waist for facing face of the adjustment part inside the lens barrel it Between angle be 135 °;
TEM fluorescent screens and STEM detectors are integrated with the adjustment part inside the lens barrel;The TEM fluorescent screens On the central plane for facing face for the adjustment part being installed on inside the lens barrel, the STEM detectors are installed on position On the upper bottom surface up or down bottom surface for facing face of the adjustment part inside the lens barrel.
2. the integral structure of the integrated TEM fluorescent screens and STEM detectors as described in claim 1, it is characterised in that institute The outside that one end that face is right angle is located at the lens barrel of facing of sliding equipment is stated, the TEM fluorescent screens are installed on positioned at described On the central plane for facing face of the sliding equipment inside lens barrel, the STEM detectors are installed on inside the lens barrel The sliding equipment the upper bottom surface for facing face on.
3. the integral structure of the integrated TEM fluorescent screens and STEM detectors as described in claim 1, it is characterised in that institute The outside that one end that face is right angle is located at the lens barrel of facing of switching mechanism is stated, the TEM fluorescent screens are installed on positioned at described On the central plane for facing face of the switching mechanism inside lens barrel, the STEM detectors are installed on inside the lens barrel The switching mechanism the bottom surface for facing face on.
CN201610187670.8A 2014-07-18 2014-07-18 A kind of integral structure of integrated TEM fluorescent screens and STEM detectors Active CN105742145B (en)

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CN201610187670.8A CN105742145B (en) 2014-07-18 2014-07-18 A kind of integral structure of integrated TEM fluorescent screens and STEM detectors

Applications Claiming Priority (2)

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CN201410345490.9A CN104091745B (en) 2014-07-18 2014-07-18 The integrated structure of a kind of integrated TEM window of tube and STEM detector
CN201610187670.8A CN105742145B (en) 2014-07-18 2014-07-18 A kind of integral structure of integrated TEM fluorescent screens and STEM detectors

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CN105742145B true CN105742145B (en) 2017-10-13

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4206349A (en) * 1977-12-01 1980-06-03 Hitachi, Ltd. Electron microscope
US5517033A (en) * 1994-07-25 1996-05-14 Gatan, Inc. Apparatus for improved image resolution in electron microscopy
CN1959416A (en) * 2005-11-01 2007-05-09 Fei公司 Stage assembly, particle-optical apparatus comprising such a stage assembly, and method of treating sample
CN202749334U (en) * 2012-04-10 2013-02-20 中国人民解放军南京军区福州总医院 Side-installed lens-coupling transmission electron microscope digital imaging apparatus
CN104091745B (en) * 2014-07-18 2016-06-01 镇江乐华电子科技有限公司 The integrated structure of a kind of integrated TEM window of tube and STEM detector

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4206349A (en) * 1977-12-01 1980-06-03 Hitachi, Ltd. Electron microscope
US5517033A (en) * 1994-07-25 1996-05-14 Gatan, Inc. Apparatus for improved image resolution in electron microscopy
CN1959416A (en) * 2005-11-01 2007-05-09 Fei公司 Stage assembly, particle-optical apparatus comprising such a stage assembly, and method of treating sample
CN202749334U (en) * 2012-04-10 2013-02-20 中国人民解放军南京军区福州总医院 Side-installed lens-coupling transmission electron microscope digital imaging apparatus
CN104091745B (en) * 2014-07-18 2016-06-01 镇江乐华电子科技有限公司 The integrated structure of a kind of integrated TEM window of tube and STEM detector

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