CN105230634A - Isolane missible oil and preparation method thereof - Google Patents
Isolane missible oil and preparation method thereof Download PDFInfo
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- CN105230634A CN105230634A CN201510766621.5A CN201510766621A CN105230634A CN 105230634 A CN105230634 A CN 105230634A CN 201510766621 A CN201510766621 A CN 201510766621A CN 105230634 A CN105230634 A CN 105230634A
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Abstract
The invention relates to isolane missible oil and a preparation method thereof and belongs to the technical field of agricultural plant fungicide and growth regulating agents. The isolane missible oil is characterized by being prepared from hymexazol, isoprothiolane, 150# solvent oil, emulsifying agents and ethyl alcohol which are of certain quality percentage concentration through the preparation method. Alcohol cosolvent is matched with the 150# solvent oil, the solubility of the hymexazol in the 150# solvent oil is effectively improved, and adverse influences of dimethylbenzene xylene which is volatilized easily on the environment and harm of plant residues to bodies of consumers are effectively reduced. The isolane missible oil is high in drug property and growth regulation performance, low in toxicity, free of residue, stable in application effect, good in plant absorption, convenient to prepare and low in cost, and resistance and adaptability to the adverse environment of plants are improved. The problems that in the prior art, dimethylbenzene xylene is low in boiling point and easy to volatilize and has high toxicity and much residues, so that environmental pollution and plant residues are caused, and the body health of farm operators and consumers is threatened are solved.
Description
Technical field
The present invention relates to a kind of transplanting missible oil and preparation method thereof, belong to agricultural plant bactericide and growth regulator technical field.
Background technology
Transplanting spirit is a kind of multifunctional plant bactericide and growth regulator.It is except having bactericidal effect, can also produce resistance and adaptive capacity, liking thus deeply by friend peasant by inducing plant after entering plant corpus to germ, low temperature, the poor environment such as saline and alkaline.Missible oil is transplanted in preparation must use solvent.Dimethylbenzene is that the missible oil of preparation transplanting at present uses maximum solvents, although xylene solvent has good missible oil stability, plant absorption is also better, but xylene solvent boiling point is low, volatile, there is larger toxicity and remain, both can injure operator in sprinkling process, and the healthy of consumer can be endangered again.In view of above reason, within 2014, rise, for reducing the harmful effect that organic solvent volatilizees to environment and consumer's health, country makes clear stipulaties to emulsifiable concentrates for agricultural chemicals solvent: the organic solvents such as benzene,toluene,xylene, methyl alcohol, DMF must not exceed limit value in missible oil.But in actual production process, for maturation process smoothly with the ordering about of economic interests, preparation is transplanted missible oil and is adopted xylene organic solvent still very general.
Summary of the invention
The object of the invention is to, there is provided a kind of property of medicine and growth regulating strong, improve plant to adverse circumstances resistance and adaptability, boiling point is high, effective minimizing organic matter volatilization causes harmful effect to environment, easy to make, with low cost, effect is stablized, transplanting missible oil of good absorbing and preparation method thereof; Solve prior art low, volatile because of xylene solvent boiling point, there is larger toxicity and residual, cause environmental pollution and plant residue, jeopardize agriculture operator and the healthy problem of consumer.
The present invention realizes above-mentioned purpose by the following technical solutions
A kind of transplanting missible oil and preparation method thereof, is characterized in that: transplant missible oil and be made up of the raw material of following mass percent concentration:
Dislike mould clever 10% Isoprothiolane 10% emulsifier 10%
Alcohols 10%150# solvent naphtha supplies surplus
150# solvent naphtha is solvent;
Alcohols refers to all alcohol comprising ethanol; Alcohols is cosolvent;
Emulsifier is formed by 45:55 mixture by peaceful newborn 34# and agriculture breast 500#.
A kind of transplanting missible oil and preparation method thereof, is characterized in that: described transplanting missible oil is prepared from by the following method: in the flask being provided with thermometer and agitator,
Add the mould spirit of evil that mass percent concentration is 10%
Add the Isoprothiolane that mass percent concentration is 10%
Add the alcohols that mass percent concentration is 10%
Add the 150# solvent naphtha that mass percent concentration is 50%;
Heating-up temperature 50 ~ 60 DEG C, adds the emulsifier that mass percent concentration is 10% until completely dissolved again, keeps temperature 50 ~ 60 DEG C, stirs 30 minutes, surplus 150# solvent naphtha is supplied, and stirs 10 minutes, is cooled to 25 DEG C, leaves standstill 20 minutes, weigh, bottling, i.e. obtained transplanting missible oil product.
The present invention's beneficial effect is compared with prior art:
This transplanting missible oil and preparation method thereof adopts 150# solvent naphtha as solvent, and it is higher than the boiling point of xylene solvent, effectively reduces harmful effect and plant residue that organic solvent volatilization causes environment to the infringement of consumer's health.Co-solvent coordinates with 150# solvent naphtha, the dissolubility of mould spirit in 150# solvent naphtha is disliked in effective raising, give full play to and dislike mould spirit and Isoprothiolane active ingredient, the characteristic of absorption sterilization in strengthening, soil disinfection and plant growth regulating, raising plant is to the resistance of adverse circumstances and adaptability.Effect is stablized, and plant absorption is good, easy to make, with low cost.Improve that to solve prior art low, volatile because of xylene solvent boiling point, there is larger toxicity and residual, cause environmental pollution and plant residue, jeopardize agriculture operator and the healthy problem of consumer.
Embodiment
Below the present invention is described in further detail:
A kind of transplanting missible oil and preparation method thereof, is characterized in that: transplant missible oil and be made up of the raw material of following mass percent concentration:
Dislike mould clever 10%, Isoprothiolane 10%, emulsifier 10%,
Alcohols 10%, 150# solvent naphtha supplies surplus;
150# solvent naphtha is solvent;
Alcohols refers to all alcohol comprising ethanol; Alcohols is cosolvent;
Emulsifier is formed by 45:55 mixture by peaceful newborn 34# and agriculture breast 500#.
A kind of transplanting missible oil and preparation method thereof, is characterized in that: described transplanting missible oil is prepared from by the following method: in the flask being provided with thermometer and agitator,
Add the mould spirit of evil that mass percent concentration is 10%
Add the Isoprothiolane that mass percent concentration is 10%
Add the alcohols that mass percent concentration is 10%
Add the 150# solvent naphtha that mass percent concentration is 50%;
Heating-up temperature 50 ~ 60 DEG C, adds the emulsifier that mass percent concentration is 10% until completely dissolved again, keeps temperature 50 ~ 60 DEG C, stirs 30 minutes, surplus 150# solvent naphtha is supplied, and stirs 10 minutes, is cooled to 25 DEG C, leaves standstill 20 minutes, weigh, bottling, i.e. obtained transplanting missible oil product.
Missible oil is transplanted below to produce 1000g:
embodiment:
Form according to the raw material of above-mentioned mass percent concentration, prepare by the following method:
In the 1000ml there-necked flask that thermometer and agitator are housed,
Add mould clever 103.1 grams of the evil that purity is 97%,
Add the Isoprothiolane 103.1 grams that purity is 97%,
Add ethanol 100 grams,
Add 150# solvent naphtha 500 grams,
Heating-up temperature is 50 ~ 60 DEG C, until completely dissolved, then adds 100 grams of emulsifier, keeps temperature 50 ~ 60 DEG C, stir 30 minutes, surplus 150# solvent naphtha is supplied, and stirs 10 minutes, is cooled to 25 DEG C, leave standstill 20 minutes, weigh, bottling, be i.e. obtained transplanting missible oil product.
Carry out the test of stability, heat storage stability and low-temperature stability to transplanting missible oil prepared by embodiment, result of the test is all up to standard.
The mould spirit of evil in the present invention has efficiently, low toxicity, nuisanceless, environmental protection advantage, effectively can suppress the mycelial normal growth of disease fungus in plant soil or directly kill germ, again can Promoting plant growth, have simultaneously and promote that crop root growth is grown, strong plantlets and rootage, improve the characteristic of crops survival rate.The permeability of disliking mould spirit is high, within two hours, just can move to plant stem, within 20 hours, is namely movable to plant complete stool.The present invention will dislike mould spirit and Isoprothiolane compatibility, 150# solvent naphtha is adopted to make solvent, alcohols such as ethanol, methyl alcohol is adopted to make cosolvent, be aided with emulsifier, not only reach the property of medicine and growth regulating strong, improve plant to resistance, the adaptability of adverse circumstances, effective minimizing organic matter volatilization causes dysgenic object to environment, and easy to make, with low cost, greatly alleviate the burden of peasant.Effect is stablized, and good absorbing, to become generic renewal product, market prospects are good.
The above is preferred embodiment of the present invention, above-mentioned illustrating does not do any pro forma restriction to flesh and blood of the present invention, any simple modification that person of an ordinary skill in the technical field has done above embodiment according to technical spirit of the present invention after having read this specification or distortion, and the technology contents of above-mentioned announcement may be utilized to be changed or be modified to the Equivalent embodiments of equivalent variations, all still belong in the scope of technical solution of the present invention, and do not deviate from the spirit and scope of the invention.
Claims (2)
1. transplant missible oil and preparation method thereof for one kind, it is characterized in that: transplant missible oil and be made up of the raw material of following mass percent concentration:
Dislike mould clever 10%, Isoprothiolane 10%, emulsifier 10%,
Alcohols 10%, 150# solvent naphtha supplies surplus;
150# solvent naphtha is solvent;
Alcohols refers to all alcohol comprising ethanol; Alcohols is cosolvent;
Emulsifier is formed by 45:55 mixture by peaceful newborn 34# and agriculture breast 500#.
2. one according to claim 1 transplants missible oil and preparation method thereof, it is characterized in that: described transplanting missible oil is prepared from by the following method:
Add in the flask being provided with thermometer and agitator:
Mass percent concentration is the mould spirit of evil of 10%,
Mass percent concentration is the Isoprothiolane of 10%,
Mass percent concentration is 10% alcohols,
Mass percent concentration is the 150# solvent naphtha of 50%,
Heating-up temperature is 50 ~ 60 DEG C, until completely dissolved, then adds the emulsifier of 10%, keeps temperature 50 ~ 60 DEG C, stir 30 minutes, surplus 150# solvent naphtha is supplied, and stirs 10 minutes, is cooled to 25 DEG C, leave standstill 20 minutes, weigh, bottling, be i.e. obtained transplanting missible oil product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510766621.5A CN105230634A (en) | 2015-11-12 | 2015-11-12 | Isolane missible oil and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510766621.5A CN105230634A (en) | 2015-11-12 | 2015-11-12 | Isolane missible oil and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105230634A true CN105230634A (en) | 2016-01-13 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510766621.5A Pending CN105230634A (en) | 2015-11-12 | 2015-11-12 | Isolane missible oil and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1377579A (en) * | 2002-03-16 | 2002-11-06 | 湖北移栽灵农业科技股份有限公司 | Compound plant resistance revellent |
| CN102640747A (en) * | 2012-04-25 | 2012-08-22 | 南京太化化工有限公司 | Special emulsifier for cypermethrin and emulsifiable concentrate preparation of cypermethrin |
-
2015
- 2015-11-12 CN CN201510766621.5A patent/CN105230634A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1377579A (en) * | 2002-03-16 | 2002-11-06 | 湖北移栽灵农业科技股份有限公司 | Compound plant resistance revellent |
| CN102640747A (en) * | 2012-04-25 | 2012-08-22 | 南京太化化工有限公司 | Special emulsifier for cypermethrin and emulsifiable concentrate preparation of cypermethrin |
Non-Patent Citations (3)
| Title |
|---|
| 刘步林: "《农药剂型加工技术》", 31 October 1998 * |
| 周婉秋: "表面活性剂在农药中的应用", 《沈阳师范学院学报(自然科学版)》 * |
| 商胜华等: "20%移栽灵乳油对烟草抗病抗逆性的影响", 《贵州农业科学》 * |
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Application publication date: 20160113 |
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| RJ01 | Rejection of invention patent application after publication |