CN104186549A - Compound composition preparation of fungicide - Google Patents
Compound composition preparation of fungicide Download PDFInfo
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- CN104186549A CN104186549A CN201410413090.7A CN201410413090A CN104186549A CN 104186549 A CN104186549 A CN 104186549A CN 201410413090 A CN201410413090 A CN 201410413090A CN 104186549 A CN104186549 A CN 104186549A
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Abstract
The invention discloses a compound composition preparation of a fungicide. The compound composition preparation is prepared from the following effective ingredients in percentage by weight: 0.1%-2% of natural antibacterial compounds, 1%-30% of antibiotic fungicides and a proper amount of a microbial fungicide, wherein 1g of the microbial fungicide includes 10-1000 hundred million of living spores. The compound composition preparation can be prepared into dosage forms of oil suspending agents, wettable powder, water suspending agents and water dispersible granules and can be used for controlling plant diseases caused by a plurality of pathogenic microorganisms. The compound composition preparation can effectively control resistant germs, is wide in sterilization range and long in pesticide effect and has the advantages of high efficiency, and labor-saving, time-saving and effort-saving properties. According to the compound composition preparation of the fungicide, the selected fungicides are biological-source pesticides, and the preparation is efficient, is low in toxicity, is safe to human, livestock and crops, can protect the crops without damaging natural enemies and has good environmental compatibility; the compound composition preparation is simple in production process and low in use cost and is suitable for market promotion and application.
Description
Technical field
The present invention relates to a kind of agriculture chemicals fungicide field, for preventing and treating the bactericide compounded composite preparation of the plant disease being caused by multiple pathogenic microorganisms.
Background technology
In recent years, the rules of agricultural chemicals aspect are pointed out in world wide, and many synthetic pesticides are even forbidden in restriction, and this measure is for being very necessary to the consideration of human health and environmental protection aspect.The research emphasis of academia has been placed on to remove to find active substance in natural resources (comprising from microorganism to animals and plants with biosphere) and has substituted synthetic pesticide.Many vegetable source natural bacteriostatic compounds have been applied to disinfectant use in agriculture field, comprise many Coumarinses, Polyphenols and flavonoid class compound etc., and have developed a series of botanical fungicides with independent intellectual property right.
Antibiotics bactericide is that a class utilizes the metabolite of microorganisms to carry out the agricultural chemicals of Suppressing phytopathogens growth and breeding.Effective working concentration of most antibiotics is lower, have systemic action and in ooze effect, be easily absorbed by plants, there is therapeutic action.And easily decomposed by organism, therefore lower to people, animal toxicity, residual hazard problem is little, does not destroy the ecological balance, suitable being applied in the nuisanceless production of vegetables.
Microbial bactericide refer to microorganism and metabolite thereof and by them, processed there is the bioactivator that suppresses plant disease.Microbial bactericide is mainly secreted antibacterial material and is suppressed pathogen growth, and inducing plant system of defense is resisted pathogen invasion simultaneously, disturbs biosynthesis and destroys cell structure, thereby reaching biological and ecological methods to prevent plant disease, pests, and erosion object.Microbial bactericide is a kind of microbial source fungicide, and interior absorption is strong, nontoxic to people and animals, and the various crop diseases such as rice blast and banded sclerotial blight, wheat powdery mildew, graw mold of tomato are had to good preventive effect.
The defect of the bactericide kind that contains single-activity component common various degrees in disinfectant use in agriculture control, as narrow in bactericidal range, control efficiency is poor, and dispenser dosage great Yi causes pesticide resistance, and application times adds to have weighed environmental pollution etc.There are some methods of using as crop allocation adjustment, different agricultural chemicals rotations etc. in actual mechanical process, are difficult to really play obvious effect.
Different cultivars being carried out composite, is to prevent and treat the modal method of resistance germ.Heterogeneity carries out compositely can improving control efficiency, expands bactericidal range, reduces the consumption of active ingredient, reduces environmental pollution, is the important means of integrated control field disease.
Through retrieval, at present do not find natural bacteriostatic compound, antibiotics bactericide and microbial bactericide is composite and the patent documentation of application.
Summary of the invention
The invention provides a kind of bactericide compounded composite preparation, its active ingredient raw materials by following percentage by weight is made: natural bacteriostatic compound 0.1-2%, antibiotics bactericide 1-30%, microbial bactericide 10-1000 hundred million living spores/g.The present invention utilizes the characteristic of biopesticide, is the plant disease that caused by multiple pathogenic microorganisms of control, and natural bacteriostatic thing and antibiotics bactericide and microbial bactericide are carried out composite, make disinfecting composite biological agent, realize a dispenser, sick worm is double to be controlled, good drug efficacy, and the lasting period is long.
The technical solution used in the present invention is as follows:
A bactericide compounded composite preparation, is made by the active ingredient raw materials of following percentage by weight: natural bacteriostatic compound 0.1-2%, antibiotics bactericide 1-30%, microbial bactericide 10-1000 hundred million living spores/g.
Described natural bacteriostatic compound is selected from least one in Quercetin, Nobiletin, resveratrol, Pidolidone, Osthole, aesculetin, ovobiocin, eugenol, cinnamic acid, S-Ethyl ethylthio sulfonate.
Described antibiotics bactericide is selected from least one in many antibiotic, Shen piperazine mycin, antimycoin 120, Zhongshengmycin, geliomycin, Ningnanmycin, Wuyiencin, kasugarnycin, jinggangmeisu, Gongzhuling mycin, streptomycin sulphate.
Described microbial bactericide is selected from least one in Trichoderma, waxy Bacillus, bacillus licheniformis, bacillus subtilis, Pseudomonas fluorescence, gliocladium germ, agrobacterium radiobacter, onion bulb sick leave monad, bacillus amyloliquefaciens, carrot soft rot Erwinia.
Described preparation formulation is a kind of in oil-suspending agent, wetting powder, aqueous suspension agent, water dispersible granules.
Advantage of the present invention:
(1) the present invention is the complex preparation of natural bacteriostatic compound and antibiotics bactericide and microbial bactericide, can effectively prevent and treat resistance germ, bactericidal range is wide, and lasting medicine, can realize a dispenser integrated control, plurality of advantages such as having efficient, saving of labor, save time, be laborsaving, the effect of increasing production of keeping a full stand of seedings is obvious.Production technology of the present invention is simple, and use cost is cheap, is easy to marketing and application.
(2) bactericide that the present invention selects is biogenic pesticide; efficiently, preparation low toxicity; to people and animals and crop safety; both can cover crop; do not injure again natural enemy; very little on ecosystem environment impact, meet the developing direction of current agricultural chemicals, so this complex preparation is a kind of extremely potential environment friendly agricultural preparation.
Embodiment
By example, embodiments of the present invention are further described below, these examples should not be construed as by any way and limit the scope of the invention.
Embodiment 1
The preparation of 10.2% oil-suspending agent: Osthole 0.1%, kasugarnycin 10%, waxy Bacillus 0.1%, emulsifier 15%, histosol 1.5%, white carbon 1.5%, vegetable oil complements to 100%.After stirring, sand milling to particle diameter is less than 5um, filters, and is 10.2% oil-suspending agent.
Embodiment 2
The preparation of 20.5% oil-suspending agent: Pidolidone 0.2%, Astromicin 20%, bacillus subtilis 0.3%, emulsifier 20%, histosol 1.5%, white carbon 1.5%, vegetable oil complements to 100%.After stirring, sand milling to particle diameter is less than 5um, filters, and is 20.5% oil-suspending agent.
Embodiment 3
The preparation of 15% aqueous suspension agent: cinnamic acid 0.4%, Shen piperazine mycin 14.5%, bacillus licheniformis 0.1%, emulsifier 5%, ethylene glycol 2%, xanthans 0.2%, Sodium Benzoate 0.2%, water complements to 100%, stir, sand milling to particle diameter is less than 5um, is 15% aqueous suspension agent.
Embodiment 4
The preparation of 25% wetting powder: S-Ethyl ethylthio sulfonate 0.5%, jinggangmeisu 24%, bacillus subtilis 0.5%, sodium lignin sulfonate 5%, K-121%, white carbon 2%, kaolin complements to 100%, after stirring, sand milling to particle diameter is less than 5um, is 25% wetting powder.
Embodiment 5
The preparation of 20% water dispersible granules: eugenol 0.3%, many antibiotic 19.5%, Pseudomonas fluorescence 0.2%, dispersant 5%, K-121.5%, kaolin complements to 100%, after stirring, air-flow crushing, granulation, is 20% water dispersible granules.
Finally in conjunction with following five examples, the control efficiency of bactericide compounded composite preparation to several corps diseases is described.Concrete outcome respectively in Table 1, table 2, table 3, table 4, table 5.
The control of table 1 pair rice green smut, banded sclerotial blight and rice blast is tested to fruit
As shown in Table 1, Osthole-kasugarnycin-waxy Bacillus oil suspended emulsion has good control efficiency to the false smut of paddy rice, banded sclerotial blight and rice blast.
Table 2 pair grape powdery mildew and gray mold prevent and treat result of the test
As shown in Table 2, Pidolidone-Astromicin-bacillus subtilis oil suspended emulsion has good control efficiency to grape powdery mildew and gray mold.
Table 3 pair cucumber downy mildew and fusarium wilt prevent and treat result of the test
As shown in Table 3, cinnamic acid-Shen piperazine mycin-bacillus licheniformis aqueous suspension emulsion has good control efficiency to cucumber downy mildew and fusarium wilt.
Table 4 pair wheat sharp eyespot and powdery mildew prevent and treat result of the test
As shown in Table 4, S-Ethyl ethylthio sulfonate-jinggangmeisu-bacillus subtilis wetting powder has good control efficiency to wheat sharp eyespot and powdery mildew.
Table 5 pair green mold of apple, spot defoliation and ring spot prevent and treat result of the test
As shown in Table 5, eugenol-many antibiotic-Pseudomonas fluorescence water dispersible granules have good control efficiency to green mold of apple, spot defoliation and ring spot.
Claims (5)
1. a bactericide compounded composite preparation, is characterized in that, its active ingredient raw materials by following percentage by weight is made: natural bacteriostatic compound 0.1-2%, antibiotics bactericide 1-30%, microbial bactericide 10-1000 hundred million living spores/g.
2. a kind of bactericide compounded composite preparation according to claim 1, it is characterized in that, described natural bacteriostatic compound is selected from least one in Quercetin, Nobiletin, resveratrol, Pidolidone, Osthole, aesculetin, ovobiocin, eugenol, cinnamic acid, S-Ethyl ethylthio sulfonate.
3. a kind of bactericide compounded composite preparation according to claim 1, it is characterized in that, described antibiotics bactericide is selected from least one in many antibiotic, Shen piperazine mycin, antimycoin 120, Zhongshengmycin, geliomycin, Ningnanmycin, Wuyiencin, kasugarnycin, jinggangmeisu, Gongzhuling mycin, streptomycin sulphate.
4. a kind of bactericide compounded composite preparation according to claim 1, it is characterized in that, described microbial bactericide is selected from least one in Trichoderma, waxy Bacillus, bacillus licheniformis, bacillus subtilis, Pseudomonas fluorescence, gliocladium germ, agrobacterium radiobacter, onion bulb sick leave monad, bacillus amyloliquefaciens, carrot soft rot Erwinia.
5. a kind of bactericide compounded composite preparation according to claim 1, described preparation formulation is a kind of in oil-suspending agent, wetting powder, aqueous suspension agent, water dispersible granules.
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| CN201410413090.7A CN104186549A (en) | 2014-08-20 | 2014-08-20 | Compound composition preparation of fungicide |
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|---|---|---|---|---|
| CN104663731A (en) * | 2015-02-09 | 2015-06-03 | 河北农业大学 | Bactericidal composition and application thereof |
| CN104886070A (en) * | 2015-01-12 | 2015-09-09 | 四川利尔作物科学有限公司 | Bactericidal composition and application thereof |
| CN105410063A (en) * | 2015-11-18 | 2016-03-23 | 无锡市稼宝药业有限公司 | Farm chemical for rice bacterial leaf blight |
| CN105707126A (en) * | 2016-03-29 | 2016-06-29 | 陕西先农生物科技有限公司 | Bactericidal composition, preparation and application of bactericidal composition |
| CN105941484A (en) * | 2016-05-11 | 2016-09-21 | 江西正邦生物化工有限责任公司 | Trichoderma asperellum spore and phenazino-1-carboxylic acid compound sterilization composition |
| CN106172719A (en) * | 2016-07-06 | 2016-12-07 | 东北农业大学 | A kind of snap bean antistaling agent |
| CN106386869A (en) * | 2016-08-31 | 2017-02-15 | 上海交通大学 | Trichoderma seed coating as well as preparation method and application thereof |
| CN107094797A (en) * | 2017-03-17 | 2017-08-29 | 南京工业大学 | Process for preparing biological pesticide by compounding bacillus cereus and antibiotics |
| CN107216185A (en) * | 2016-03-22 | 2017-09-29 | 上海农乐生物制品股份有限公司 | It is a kind of to prevent and treat bioorganic pesticide fertilizer of soil-borne disease and preparation method thereof |
| CN107306999A (en) * | 2016-04-26 | 2017-11-03 | 上海农乐生物制品股份有限公司 | A kind of bactericidal composition based on shenqinmycin and the bactericide containing said composition |
| CN107593771A (en) * | 2017-09-08 | 2018-01-19 | 信阳农林学院 | One kind preventing and treating tea tree tea moire blight microorganism and plant source compound agricultural chemicals |
| CN107897198A (en) * | 2017-12-20 | 2018-04-13 | 山东省烟台市农业科学研究院 | The complex composition and its application of Zhongshengmycin and eugenol |
| CN108077313A (en) * | 2016-11-22 | 2018-05-29 | 上海农乐生物制品股份有限公司 | A kind of shenqinmycin waxy Bacillus compounding suspending agent and its preparation and application |
| CN108077314A (en) * | 2016-11-22 | 2018-05-29 | 上海农乐生物制品股份有限公司 | A kind of shenqinmycin waxy Bacillus compound water dispersible granule and its preparation and application |
| CN108101630A (en) * | 2017-12-20 | 2018-06-01 | 上海农乐生物制品股份有限公司 | A kind of functional biological medicine fertilizer and its preparation and application |
| CN108522511A (en) * | 2018-07-16 | 2018-09-14 | 江门市植保有限公司 | A kind of bactericidal composition containing eugenol and kasugarnycin |
| CN108656283A (en) * | 2018-05-23 | 2018-10-16 | 安徽省高雅家居有限公司 | A kind of timber preservative |
| CN108739809A (en) * | 2018-06-13 | 2018-11-06 | 北京清源保生物科技有限公司 | It is a kind of prevention fungal disease bactericidal composition and its application |
| CN108818828A (en) * | 2018-05-23 | 2018-11-16 | 安徽省高雅家居有限公司 | A kind of environment-friendly type anticorrosion composition for wood |
| CN109221296A (en) * | 2018-10-25 | 2019-01-18 | 黑龙江惊哲森林农业科技开发有限责任公司 | A kind of plant degerming bio-fermented liquid and preparation method thereof |
| CN109258692A (en) * | 2017-07-18 | 2019-01-25 | 郭少波 | A kind of compounded combination pharmacy agent containing kasugarnycin and Pseudomonas fluorescence |
| CN109805032A (en) * | 2019-02-28 | 2019-05-28 | 广西地源之本肥业有限公司 | A kind of microorganism biological and ecological methods to prevent plant disease, pests, and erosion agent and preparation method thereof inhibiting bacterial disease |
| CN110800736A (en) * | 2019-11-27 | 2020-02-18 | 南京林业大学 | Oil suspending agent for preventing and treating termites and preparation method thereof |
| CN111345323A (en) * | 2020-04-17 | 2020-06-30 | 滨州学院 | Biological bactericide containing bacillus licheniformis |
| CN111587884A (en) * | 2020-06-28 | 2020-08-28 | 江苏省中国科学院植物研究所 | Application of aesculetin in preventing and treating plant oomycetes diseases |
| CN112075456A (en) * | 2020-09-16 | 2020-12-15 | 广西壮族自治区亚热带作物研究所（广西亚热带农产品加工研究所） | Biological pesticide for preventing and treating macadamia nut flower blight |
| WO2021109549A1 (en) * | 2019-12-06 | 2021-06-10 | 中国农业大学 | Joint application of quercetin and antibacterial medicament |
| CN113197224A (en) * | 2021-05-17 | 2021-08-03 | 淮阴工学院 | Synergistic compound for preventing and treating gray mold of strawberries and application thereof |
| CN114532344A (en) * | 2020-11-25 | 2022-05-27 | 陕西西大华特科技实业有限公司 | Bactericidal composition containing shenqinmycin and ethylicin and application thereof |
| CN115462380A (en) * | 2022-11-01 | 2022-12-13 | 中国农业科学院植物保护研究所 | Compound preparation containing wuyiencin and application thereof in preventing and treating grape gray mold |
| CN116250532A (en) * | 2023-02-16 | 2023-06-13 | 信阳农林学院 | Pesticide composition for preventing and treating banded sclerotial blight of wheat |
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| CN103636678A (en) * | 2013-11-29 | 2014-03-19 | 安徽省化工研究院 | Pesticide compound preparation of microbial fungicide and antibiotic insecticides |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104886070A (en) * | 2015-01-12 | 2015-09-09 | 四川利尔作物科学有限公司 | Bactericidal composition and application thereof |
| CN104663731A (en) * | 2015-02-09 | 2015-06-03 | 河北农业大学 | Bactericidal composition and application thereof |
| CN104663731B (en) * | 2015-02-09 | 2017-11-10 | 河北农业大学 | Bactericidal composition and application thereof |
| CN105410063A (en) * | 2015-11-18 | 2016-03-23 | 无锡市稼宝药业有限公司 | Farm chemical for rice bacterial leaf blight |
| CN107216185A (en) * | 2016-03-22 | 2017-09-29 | 上海农乐生物制品股份有限公司 | It is a kind of to prevent and treat bioorganic pesticide fertilizer of soil-borne disease and preparation method thereof |
| CN105707126A (en) * | 2016-03-29 | 2016-06-29 | 陕西先农生物科技有限公司 | Bactericidal composition, preparation and application of bactericidal composition |
| CN105707126B (en) * | 2016-03-29 | 2019-07-05 | 陕西先农生物科技有限公司 | A kind of bactericidal composition, preparation and its application |
| CN107306999A (en) * | 2016-04-26 | 2017-11-03 | 上海农乐生物制品股份有限公司 | A kind of bactericidal composition based on shenqinmycin and the bactericide containing said composition |
| CN105941484A (en) * | 2016-05-11 | 2016-09-21 | 江西正邦生物化工有限责任公司 | Trichoderma asperellum spore and phenazino-1-carboxylic acid compound sterilization composition |
| CN106172719A (en) * | 2016-07-06 | 2016-12-07 | 东北农业大学 | A kind of snap bean antistaling agent |
| CN106172719B (en) * | 2016-07-06 | 2019-04-16 | 东北农业大学 | A kind of snap bean antistaling agent |
| CN106386869A (en) * | 2016-08-31 | 2017-02-15 | 上海交通大学 | Trichoderma seed coating as well as preparation method and application thereof |
| CN108077313A (en) * | 2016-11-22 | 2018-05-29 | 上海农乐生物制品股份有限公司 | A kind of shenqinmycin waxy Bacillus compounding suspending agent and its preparation and application |
| CN108077314A (en) * | 2016-11-22 | 2018-05-29 | 上海农乐生物制品股份有限公司 | A kind of shenqinmycin waxy Bacillus compound water dispersible granule and its preparation and application |
| CN107094797A (en) * | 2017-03-17 | 2017-08-29 | 南京工业大学 | Process for preparing biological pesticide by compounding bacillus cereus and antibiotics |
| CN109258692A (en) * | 2017-07-18 | 2019-01-25 | 郭少波 | A kind of compounded combination pharmacy agent containing kasugarnycin and Pseudomonas fluorescence |
| CN107593771A (en) * | 2017-09-08 | 2018-01-19 | 信阳农林学院 | One kind preventing and treating tea tree tea moire blight microorganism and plant source compound agricultural chemicals |
| CN107897198A (en) * | 2017-12-20 | 2018-04-13 | 山东省烟台市农业科学研究院 | The complex composition and its application of Zhongshengmycin and eugenol |
| CN108101630A (en) * | 2017-12-20 | 2018-06-01 | 上海农乐生物制品股份有限公司 | A kind of functional biological medicine fertilizer and its preparation and application |
| CN108656283A (en) * | 2018-05-23 | 2018-10-16 | 安徽省高雅家居有限公司 | A kind of timber preservative |
| CN108818828A (en) * | 2018-05-23 | 2018-11-16 | 安徽省高雅家居有限公司 | A kind of environment-friendly type anticorrosion composition for wood |
| CN108739809A (en) * | 2018-06-13 | 2018-11-06 | 北京清源保生物科技有限公司 | It is a kind of prevention fungal disease bactericidal composition and its application |
| CN108522511A (en) * | 2018-07-16 | 2018-09-14 | 江门市植保有限公司 | A kind of bactericidal composition containing eugenol and kasugarnycin |
| CN109221296A (en) * | 2018-10-25 | 2019-01-18 | 黑龙江惊哲森林农业科技开发有限责任公司 | A kind of plant degerming bio-fermented liquid and preparation method thereof |
| CN109805032A (en) * | 2019-02-28 | 2019-05-28 | 广西地源之本肥业有限公司 | A kind of microorganism biological and ecological methods to prevent plant disease, pests, and erosion agent and preparation method thereof inhibiting bacterial disease |
| CN110800736A (en) * | 2019-11-27 | 2020-02-18 | 南京林业大学 | Oil suspending agent for preventing and treating termites and preparation method thereof |
| WO2021109549A1 (en) * | 2019-12-06 | 2021-06-10 | 中国农业大学 | Joint application of quercetin and antibacterial medicament |
| CN111345323A (en) * | 2020-04-17 | 2020-06-30 | 滨州学院 | Biological bactericide containing bacillus licheniformis |
| CN111587884A (en) * | 2020-06-28 | 2020-08-28 | 江苏省中国科学院植物研究所 | Application of aesculetin in preventing and treating plant oomycetes diseases |
| CN112075456A (en) * | 2020-09-16 | 2020-12-15 | 广西壮族自治区亚热带作物研究所（广西亚热带农产品加工研究所） | Biological pesticide for preventing and treating macadamia nut flower blight |
| CN112075456B (en) * | 2020-09-16 | 2021-06-01 | 广西壮族自治区亚热带作物研究所（广西亚热带农产品加工研究所） | Biological pesticide for preventing and treating macadamia nut flower blight |
| CN114532344A (en) * | 2020-11-25 | 2022-05-27 | 陕西西大华特科技实业有限公司 | Bactericidal composition containing shenqinmycin and ethylicin and application thereof |
| CN113197224A (en) * | 2021-05-17 | 2021-08-03 | 淮阴工学院 | Synergistic compound for preventing and treating gray mold of strawberries and application thereof |
| CN115462380A (en) * | 2022-11-01 | 2022-12-13 | 中国农业科学院植物保护研究所 | Compound preparation containing wuyiencin and application thereof in preventing and treating grape gray mold |
| CN115462380B (en) * | 2022-11-01 | 2023-02-03 | 中国农业科学院植物保护研究所 | Compound preparation containing wuyiencin and application thereof in preventing and treating grape gray mold |
| CN116250532A (en) * | 2023-02-16 | 2023-06-13 | 信阳农林学院 | Pesticide composition for preventing and treating banded sclerotial blight of wheat |
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Application publication date: 20141210 |