CN103726308A - Oil-repellent finishing liquid for woolen sweater and preparation method for oil-repellent finishing liquid - Google Patents
Oil-repellent finishing liquid for woolen sweater and preparation method for oil-repellent finishing liquid Download PDFInfo
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- CN103726308A CN103726308A CN201310688859.1A CN201310688859A CN103726308A CN 103726308 A CN103726308 A CN 103726308A CN 201310688859 A CN201310688859 A CN 201310688859A CN 103726308 A CN103726308 A CN 103726308A
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Abstract
The invention discloses oil-repellent finishing liquid for a woolen sweater and a preparation method for the oil-repellent finishing liquid. The oil-repellent finishing liquid for the woolen sweater consists of the following components in parts by weight: 6 to 8 parts of polyethylene glycol monomethyl ether, 3 to 5 parts of an emulsifier OP-13, 2 to 5 parts of polypropylene glycol, 6 to 10 parts of sodium polyacrylate, 14 to 17 parts of ethanol and 185 to 200 parts of water. The finishing liquid is prepared by the steps of heating, stirring, sealed storage and the like. The prepared finishing liquid has a good oil-repellent effect.
Description
Technical field
The present invention relates to a kind of dressing liquid and preparation method thereof, particularly relate to a kind of woollen sweater oil-repellent finiss liquid and preparation method thereof.
Background technology
Woollen sweater is than common cotton clothing, and it is high a lot of that price is wanted.In dress, after people uncloak, if oil droplet has been spread across on woollen sweater in the process of having dinner, can affect people's normal dress.Conventional woollen sweater does not have the good oily effect of refusing, and needs us by after using dressing liquid to arrange woollen sweater, improves the oily effect of refusing of woollen sweater.After conventional dressing liquid arranges woollen sweater, its refuse oily effect improve not obvious, woollen sweater to refuse wet goods level still lower, so we need to develop and can significantly improve the dressing liquid that woollen sweater is refused wet goods level.
Summary of the invention
The technical problem solving: conventional woollen sweater arranges the problem of refusing oily weak effect later through dressing liquid.
Technical scheme: the invention discloses a kind of woollen sweater oil-repellent finiss liquid, woollen sweater oil-repellent finiss liquid is comprised of according to weight ratio following composition: macrogol monomethyl ether is that 6～8 parts, polyoxyethylene nonylphenol ether-13 are that 3～5 parts, polypropylene glycol are that 2～5 parts, Sodium Polyacrylate are that 6～10 parts, ethanol are that 14～17 parts, water are 185～200 parts.
A kind of preparation method of woollen sweater oil-repellent finiss liquid, preparation method comprises the following steps: (1) blending tank temperature is adjusted to 80 ℃～90 ℃, to adding macrogol monomethyl ether in blending tank, be that 6～8 parts, polyoxyethylene nonylphenol ether-13 are 3～5 parts, stir, speed of agitator is set as 130rpm, till stirring; (2) to adding polypropylene glycol in blending tank, be that 2～5 parts, Sodium Polyacrylate are 6～10 parts again, again stir, speed of agitator is set as 130rpm, till stirring; (3) finally adding ethanol is that 14～17 parts, water are 185～200 parts again, finally stirs, and speed of agitator is set as 130rpm, till stirring, naturally cooling after evenly, seals up for safekeeping after being cooled to room temperature.
Wherein, blending tank temperature is preferably adjusted to 80 ℃.To adding macrogol monomethyl ether in blending tank, be preferably 8 parts.To adding ethanol in blending tank, be preferably 17 parts.
Beneficial effect: after common woollen sweater carries out dressing liquid arrangement of the present invention, the wet goods level of refusing of common woollen sweater is 4 to 5 grades, has the good oily effect of refusing.
The specific embodiment
Embodiment 1
(1) blending tank temperature is adjusted to 90 ℃, to adding macrogol monomethyl ether in blending tank, is that 6kg, polyoxyethylene nonylphenol ether-13 are 5kg, stirs, and speed of agitator is set as 130rpm, till stirring; (2) to adding polypropylene glycol in blending tank, be that 2kg, Sodium Polyacrylate are 6kg again, again stir, speed of agitator is set as 130rpm, till stirring; (3) finally adding ethanol is that 14kg, water are 200kg again, finally stirs, and speed of agitator is set as 130rpm, till stirring, naturally cooling after evenly, seals up for safekeeping after being cooled to room temperature.
Embodiment 2
(1) blending tank temperature is adjusted to 80 ℃, to adding macrogol monomethyl ether in blending tank, is that 7kg, polyoxyethylene nonylphenol ether-13 are 3kg, stirs, and speed of agitator is set as 130rpm, till stirring; (2) to adding polypropylene glycol in blending tank, be that 4kg, Sodium Polyacrylate are 8kg again, again stir, speed of agitator is set as 130rpm, till stirring; (3) finally adding ethanol is that 17kg, water are 190kg again, finally stirs, and speed of agitator is set as 130rpm, till stirring, naturally cooling after evenly, seals up for safekeeping after being cooled to room temperature.
Embodiment 3
(1) blending tank temperature is adjusted to 85 ℃, to adding macrogol monomethyl ether in blending tank, is that 8kg, polyoxyethylene nonylphenol ether-13 are 4kg, stirs, and speed of agitator is set as 130rpm, till stirring; (2) to adding polypropylene glycol in blending tank, be that 5kg, Sodium Polyacrylate are 10kg again, again stir, speed of agitator is set as 130rpm, till stirring; (3) finally adding ethanol is that 15kg, water are 185kg again, finally stirs, and speed of agitator is set as 130rpm, till stirring, naturally cooling after evenly, seals up for safekeeping after being cooled to room temperature.
To in the dressing liquid of commercially available common pure woollen sweater immersion embodiment 1, embodiment 2, embodiment 3, soak after 40min, one soaks one rolls, and pick-up is preliminary drying 24min at 66%, 82 ℃, then at 110 ℃, dries after washing.The testing standard of oil repellent energy is AATCC118.Test result sees the following form.
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Refuse wet goods level | 5 grades | 4 grades | 5 grades |
The wet goods level of refusing of the woollen sweater arranging through embodiment 1, embodiment 2, embodiment 3 dressing liquids is 4 to 5 grades, has the good oily effect of refusing.
Claims (5)
1. a woollen sweater oil-repellent finiss liquid, is characterized in that woollen sweater oil-repellent finiss liquid is comprised of according to weight ratio following composition: macrogol monomethyl ether is that 6～8 parts, polyoxyethylene nonylphenol ether-13 are that 3～5 parts, polypropylene glycol are that 2～5 parts, Sodium Polyacrylate are that 6～10 parts, ethanol are that 14～17 parts, water are 185～200 parts.
2. the preparation method of a kind of woollen sweater oil-repellent finiss liquid according to claim 1, it is characterized in that preparation method comprises the following steps: (1) blending tank temperature is adjusted to 80 ℃～90 ℃, to adding macrogol monomethyl ether in blending tank, be that 6～8 parts, polyoxyethylene nonylphenol ether-13 are 3～5 parts, stir, speed of agitator is set as 130rpm, till stirring; (2) to adding polypropylene glycol in blending tank, be that 2～5 parts, Sodium Polyacrylate are 6～10 parts again, again stir, speed of agitator is set as 130rpm, till stirring; (3) finally adding ethanol is that 14～17 parts, water are 185～200 parts again, finally stirs, and speed of agitator is set as 130rpm, till stirring, naturally cooling after evenly, seals up for safekeeping after being cooled to room temperature.
3. the preparation method of a kind of woollen sweater oil-repellent finiss liquid according to claim 2, is characterized in that blending tank temperature is adjusted to 80 ℃.
4. the preparation method of a kind of woollen sweater oil-repellent finiss liquid according to claim 2, it is characterized in that adding macrogol monomethyl ether in blending tank is 8 parts.
5. the preparation method of a kind of woollen sweater oil-repellent finiss liquid according to claim 2, it is characterized in that adding ethanol in blending tank is 17 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310688859.1A CN103726308A (en) | 2013-12-17 | 2013-12-17 | Oil-repellent finishing liquid for woolen sweater and preparation method for oil-repellent finishing liquid |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310688859.1A CN103726308A (en) | 2013-12-17 | 2013-12-17 | Oil-repellent finishing liquid for woolen sweater and preparation method for oil-repellent finishing liquid |
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| CN103726308A true CN103726308A (en) | 2014-04-16 |
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| CN201310688859.1A Pending CN103726308A (en) | 2013-12-17 | 2013-12-17 | Oil-repellent finishing liquid for woolen sweater and preparation method for oil-repellent finishing liquid |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104452302A (en) * | 2014-12-23 | 2015-03-25 | 常熟市中宏针织厂 | Arrangement process for knitted fabric |
| CN104499287A (en) * | 2014-12-23 | 2015-04-08 | 常熟市海虞富盛经纬编织造厂 | Wool fabric finishing liquid |
| CN107916570A (en) * | 2017-11-30 | 2018-04-17 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of wool fabric oil repellent finish |
Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61176560A (en) * | 1985-01-30 | 1986-08-08 | チバ‐ガイギー アーゲー | Acrylates and metacrylates having perfluoroalkylsulfone group, manufacture and use |
| US4898981A (en) * | 1988-06-20 | 1990-02-06 | Ciba-Geigy Corporation | Heteroatom containing perfluoroalkyl terminated neopentyl glycols and compositions therefrom |
| US5019428A (en) * | 1988-01-29 | 1991-05-28 | Ciba-Geigy Corporation | Modified polyurethanes containing perfluoroaliphatic groups and use thereof |
| US5045624A (en) * | 1988-06-20 | 1991-09-03 | Ciba-Geigy Corporation | Heteroatom containing perfluoroalkyl terminated neopentyl glycols and compositions therefrom |
| EP0694532A1 (en) * | 1994-07-01 | 1996-01-31 | Ciba-Geigy Ag | Perfluoroalkyl sulfide, sulfone, polysulfone and polysulfide diols |
| CN1616754A (en) * | 1999-09-30 | 2005-05-18 | 西巴特殊化学品普法希股份有限公司 | Compositions for the oil and water repellent finishing of fiber materials |
| CN1687516A (en) * | 2005-04-14 | 2005-10-26 | 嘉兴市雀屏化工有限责任公司 | Post finishing method for moisture and oil repellant wool fabric |
| CN101177485A (en) * | 2007-10-31 | 2008-05-14 | 大连理工大学 | Low surface-energy fluorosiloxane containing double parallel main-chain structure and method for synthesizing the same |
| CN101349010A (en) * | 2008-08-28 | 2009-01-21 | 苏州大学 | Silk broadcloth anti-water anti-oil dressing agent, preparation method and uses thereof |
| CN101892589A (en) * | 2010-07-02 | 2010-11-24 | 山东新力过滤材料有限公司 | Water and oil repellent sizing agent |
| CN102002128A (en) * | 2010-10-22 | 2011-04-06 | 东华大学 | Organic-inorganic composite emulsion water-and-oil-repellent finishing agent and application thereof |
| CN102094329A (en) * | 2009-12-09 | 2011-06-15 | 北京服装学院 | Fluorine and silicon containing water and oil repellent finishing agent, preparation and application thereof |
| CN103194904A (en) * | 2013-04-27 | 2013-07-10 | 苏州大学 | Water-repellent and oil-repellent fabric finishing agent, as well as preparation method and applications thereof |
-
2013
- 2013-12-17 CN CN201310688859.1A patent/CN103726308A/en active Pending
Patent Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61176560A (en) * | 1985-01-30 | 1986-08-08 | チバ‐ガイギー アーゲー | Acrylates and metacrylates having perfluoroalkylsulfone group, manufacture and use |
| US5019428A (en) * | 1988-01-29 | 1991-05-28 | Ciba-Geigy Corporation | Modified polyurethanes containing perfluoroaliphatic groups and use thereof |
| US4898981A (en) * | 1988-06-20 | 1990-02-06 | Ciba-Geigy Corporation | Heteroatom containing perfluoroalkyl terminated neopentyl glycols and compositions therefrom |
| US5045624A (en) * | 1988-06-20 | 1991-09-03 | Ciba-Geigy Corporation | Heteroatom containing perfluoroalkyl terminated neopentyl glycols and compositions therefrom |
| EP0694532A1 (en) * | 1994-07-01 | 1996-01-31 | Ciba-Geigy Ag | Perfluoroalkyl sulfide, sulfone, polysulfone and polysulfide diols |
| CN1616754A (en) * | 1999-09-30 | 2005-05-18 | 西巴特殊化学品普法希股份有限公司 | Compositions for the oil and water repellent finishing of fiber materials |
| CN1687516A (en) * | 2005-04-14 | 2005-10-26 | 嘉兴市雀屏化工有限责任公司 | Post finishing method for moisture and oil repellant wool fabric |
| CN101177485A (en) * | 2007-10-31 | 2008-05-14 | 大连理工大学 | Low surface-energy fluorosiloxane containing double parallel main-chain structure and method for synthesizing the same |
| CN101349010A (en) * | 2008-08-28 | 2009-01-21 | 苏州大学 | Silk broadcloth anti-water anti-oil dressing agent, preparation method and uses thereof |
| CN102094329A (en) * | 2009-12-09 | 2011-06-15 | 北京服装学院 | Fluorine and silicon containing water and oil repellent finishing agent, preparation and application thereof |
| CN101892589A (en) * | 2010-07-02 | 2010-11-24 | 山东新力过滤材料有限公司 | Water and oil repellent sizing agent |
| CN102002128A (en) * | 2010-10-22 | 2011-04-06 | 东华大学 | Organic-inorganic composite emulsion water-and-oil-repellent finishing agent and application thereof |
| CN103194904A (en) * | 2013-04-27 | 2013-07-10 | 苏州大学 | Water-repellent and oil-repellent fabric finishing agent, as well as preparation method and applications thereof |
Non-Patent Citations (1)
| Title |
|---|
| 阎克路: "《染整工艺学教程第一分册》", 30 September 2005, article "特种功能整理", pages: 369-374 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104452302A (en) * | 2014-12-23 | 2015-03-25 | 常熟市中宏针织厂 | Arrangement process for knitted fabric |
| CN104499287A (en) * | 2014-12-23 | 2015-04-08 | 常熟市海虞富盛经纬编织造厂 | Wool fabric finishing liquid |
| CN107916570A (en) * | 2017-11-30 | 2018-04-17 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of wool fabric oil repellent finish |
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Application publication date: 20140416 |