Summary of the invention:
The problem to be solved in the present invention provides a kind of just energy de-oiling simultaneously, debitterize at normal temperatures exactly for above deficiency, be applicable to the fermented orange wine of producing after mechanize squeezing orange blossom, and its production method.
Its technical scheme is as follows:
A kind of machine-processed fermented orange wine, its production technique comprises the following steps:
1) anti-oxidant brown stain: the clear juice of the oranges and tangerines that juice extractor is squeezed out, pulp add the saccharosonic acid of juice, pulp weight 0.1 ‰-0.2 ‰ clearly immediately, and pulp is delivered to the squeezing of stoning juice extractor and gets the clear juice of two road oranges and tangerines, and the clear juice of twice is merged to obtain to orange juice.
2) acid adjustment: in orange juice, add food grade CaCO
3acid adjustment to 0.6-0.7g/100ml(by Citric acid monohydrate Food grade, in former orange juice containing citric acid 0.9-1.3g/100ml), stir that within 20-25 minute, to reach neutralization reaction complete.
3) de-oiling, debitterize: in the orange juice after acid adjustment, add the cyclodextrin of orange juice weight 0.2%-1.5% fully to stir 20-30 minute, make cyclodextrin to the tangerine oil in orange juice and bitter principle material inclusion complexation sufficient reacting.
4) adjust sugar: the sucrose of take allotment orange juice total reducing sugar as 20-22g/100ml(be that the 100ml orange juice is containing sucrose 20-22g, the sucrose add-on equals total reducing sugar and subtracts the fruit juice sugar degree, after calculating the sucrose add-on, take sucrose: water is brewed into the syrup with fructose fragrance as 2:1 is watered, pump in orange juice and stir evenly while hot, product temperature 18-22 ℃ now), obtain allotment fruit juice.
5) yeast preparation:
The one-level preparation:
Get triangular flask, the sterilizing syrup (being to contain 5-8g sucrose in 100ml water) of dress 5-8g/100ml, to the active fruit wine dried yeast powder that adds 10g/100ml in the sterilizing syrup (being to contain the active fruit wine dried yeast powder of 10g in 100ml sterilizing syrup), in 33-37 ℃ of activation 15-25 minute, obtain the activation yeast slurry;
Two-stage system is standby:
The allotment fruit juice of packing in the Ka Shi tank, the activation yeast slurry to adding allotment fruit juice weight 10% in allotment fruit juice, shake up temperature control 25-33 ℃ and cultivate 2-4 hour, obtains the yeast kind, and observing the moving animated period of yeast tide, to enter three tier structure standby;
Three tier structure is standby:
The allotment fruit juice of packing in the distiller's yeast tank, to the yeast kind that moves into allotment fruit juice weight 5%-10% in allotment fruit juice, cultivate 7-9 hour for temperature control 20-25 ℃, obtains distiller's yeast liquid, and the moving animated period of yeast tide pumps into ferment tank.
From activated yeast, to the yeast segmentation of allotment fruit juice fermentation, cultivate, every grade of temperature difference is no more than 10 ℃, with this, reduces the infringement to yeast, improves the yeast growth rate.
Ripe distiller's yeast is containing reach more than 60,000/ml of yeast number, bud ratio 25% left and right, and the yeast conidial cell wall is thin, and Dissolve things inside is sparkling and crystal-clear bright, and vitality is vigorous, and dead yeast is lower than 2/ml, cleaning-less bacteria infection.
Above-mentioned nutrient solution is 70% of vessel volume, and container is the ventilation closing device, and incubation period vibration or stirring frequently, pass into sterile air (oxygen).
6) fermentation: will allocate fruit juice and pump into the sterilization fermentor tank, the distiller's yeast liquid of 18-22 ℃ of access allotment fruit juice weight 8%-12% of product temperature, charging successively, every tank feed time is no more than 24 hours.Per hour with sterile air, stir fermentation juice minimum 3 minutes, temperature control 18-22 ℃ fermentation.
7) mend sugared supervention ferment: when the sugary 6-8g/100ml of dropping to of fermented liquid, add Fructus Hordei Germinatus maltose and honeybee sugar, Fructus Hordei Germinatus maltose 5-7g/100ml(is containing Fructus Hordei Germinatus maltose 5-7g in the 100ml fermented liquid), honeybee sugar 2-4g/100ml, the about 5.5g/100ml of sugar amount is mended in conversion altogether; The SO that adds again 25-35mg/L
2(be containing SO in the 1L fermented liquid
225-35mg) temperature control 18-22 ℃ is continued fermentation.Within 3-5 days, is approximately the yeast growth phase, the animated period mistake, should stop passing into sterile air, and temperature control 15-20 ℃ allows its static fermentation.Through left and right Primary Fermentation in 10 days, finish, more than wine degree 12 degree, below sugared 2g/100ml, extraction middle level pure mellow wine enters another tank and enters rear ferment again.Face slag and end slag concentrate on a tank secondary fermentation.Cyclic dextrin clathrate complex thing and pomace are separated from pure mellow wine with end slag, face slag.
8) ferment after: extract Primary Fermentation pure mellow wine tank out and become canful (liquid level is from tank actinal surface 10cm left and right), add the SO of 30mg/L
2, temperature control 15-20 ℃, through 14-16 days (containing 6 days clarification phases), rear ferment finished; Allow pure mellow wine naturally clarify, the wine degree reaches 12 degree or, more than 14 degree, below residual sugar 0.4g/100ml, acidity 0.6-0.8g/100ml, finish rear ferment.After taking out limpid wine liquid and becoming canful, more than supplying pure mellow wine wine degree 14 degree with white orchid ground wine, add the SO of 100mg/L
2, enter the ageing phase, at this moment be called former wine; The distillation of wine pin is white orchid ground wine.Face slag and end slag are through fermentation ends, and after extracting its pure mellow wine out, the recrement distillation is white orchid ground wine.
9) ageing: after 2-3 month ageing, carry out tank switching one time, former wine also becomes canful, and the wine pin is concentrated and clarified, last wine pin distillation white orchid ground wine.After former wine ageing half a year (through aestivate) again tank switching once, surpass every 1 year, 2 years tank switchings of former wine of 1 year ageing phase once later, operation is the same.
10) lower glue, allotment, sterilizing, filtration obtain finished product: lower glue after former 8 months phases of wine ageing, and under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 0.6-2.5g/100ml, glue is clarified former wine, and time 8-15 days, after blending allotment, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
The oranges and tangerines that use in the present invention comprise red tangerine, Pon mandarin orange, granulated sugar tangerine, sweet orange, orange, navel orange, blood orange, Xia Cheng, white shaddock, sweet shaddock etc.
Cyclodextrin can be selected alpha-cylodextrin, γ-cyclodextrin, beta-cyclodextrin, δ-cyclodextrin, preferably beta-cyclodextrin (β-CD).
The production technique of orange wine of the present invention comprises the following steps:
1) anti-oxidant brown stain: the clear juice of the oranges and tangerines that juice extractor is squeezed out, pulp add the saccharosonic acid of juice, pulp weight 0.1 ‰-0.2 ‰ clearly immediately, and pulp is delivered to the squeezing of stoning juice extractor and gets the clear juice of two road oranges and tangerines, and the clear juice of twice is merged to obtain to orange juice.
2) acid adjustment: in orange juice, add food grade CaCO
3acid adjustment to 0.6-0.7g/100ml(by Citric acid monohydrate Food grade, in former orange juice containing citric acid 0.9-1.3g/100ml), stir that within 20-25 minute, to reach neutralization reaction complete.
3) de-oiling, debitterize: in the orange juice after acid adjustment, add the cyclodextrin of orange juice weight 0.2%-1.5% fully to stir 20-30 minute, make cyclodextrin to the tangerine oil in orange juice and bitter principle material inclusion complexation sufficient reacting.
4) adjust sugar: the sucrose of take allotment orange juice total reducing sugar as 20-22g/100ml(be that the 100ml orange juice is containing sucrose 20-22g, the sucrose add-on equals total reducing sugar and subtracts the fruit juice sugar degree, after calculating the sucrose add-on, take sucrose: water is brewed into the syrup with fructose fragrance as 2:1 is watered, pump in orange juice and stir evenly while hot, product temperature 18-22 ℃ now), obtain allotment fruit juice.
5) yeast preparation:
The one-level preparation:
Get triangular flask, the sterilizing syrup (being to contain 5-8g sucrose in 100ml water) of dress 5-8g/100ml, to the active fruit wine dried yeast powder that adds 10g/100ml in the sterilizing syrup (being to contain the active fruit wine dried yeast powder of 10g in 100ml sterilizing syrup), in 33-37 ℃ of activation 15-25 minute, obtain the activation yeast slurry;
Two-stage system is standby:
The allotment fruit juice of packing in the Ka Shi tank, the activation yeast slurry to adding allotment fruit juice weight 10% in allotment fruit juice, shake up temperature control 25-33 ℃ and cultivate 2-4 hour, obtains the yeast kind, and observing the moving animated period of yeast tide, to enter three tier structure standby;
Three tier structure is standby:
The allotment fruit juice of packing in the distiller's yeast tank, to the yeast kind that moves into allotment fruit juice weight 5%-10% in allotment fruit juice, cultivate 7-9 hour for temperature control 20-25 ℃, obtains distiller's yeast liquid, and the moving animated period of yeast tide pumps into ferment tank.
From activated yeast, to the yeast segmentation of allotment fruit juice fermentation, cultivate, every grade of temperature difference is no more than 10 ℃, with this, reduces the infringement to yeast, improves the yeast growth rate.
Ripe distiller's yeast is containing reach more than 60,000/ml of yeast number, bud ratio 25% left and right, and the yeast conidial cell wall is thin, and Dissolve things inside is sparkling and crystal-clear bright, and vitality is vigorous, and dead yeast is lower than 2/ml, cleaning-less bacteria infection.
Above-mentioned nutrient solution is 70% of vessel volume, and container is the ventilation closing device, and incubation period vibration or stirring frequently, pass into sterile air (oxygen).
6) fermentation: will allocate fruit juice and pump into the sterilization fermentor tank, the distiller's yeast liquid of 18-22 ℃ of access allotment fruit juice weight 8%-12% of product temperature, charging successively, every tank feed time is no more than 24 hours.Per hour with sterile air, stir fermentation juice minimum 3 minutes, temperature control 18-22 ℃ fermentation.
7) mend sugared supervention ferment: when the sugary 6-8g/100ml of dropping to of fermented liquid, add Fructus Hordei Germinatus maltose and honeybee sugar, Fructus Hordei Germinatus maltose 5-7g/100ml(is containing Fructus Hordei Germinatus maltose 5-7g in the 100ml fermented liquid), honeybee sugar 2-4g/100ml, the about 5.5g/100ml of sugar amount is mended in conversion altogether; The SO that adds again 25-35mg/L
2(be containing SO in the 1L fermented liquid
225-35mg) temperature control 18-22 ℃ is continued fermentation.Within 3-5 days, is approximately the yeast growth phase, the animated period mistake, should stop passing into sterile air, and temperature control 15-20 ℃ allows its static fermentation.Through left and right Primary Fermentation in 10 days, finish, more than wine degree 12 degree, below sugared 2g/100ml, extraction middle level pure mellow wine enters another tank and enters rear ferment again.Face slag and end slag concentrate on a tank secondary fermentation.Cyclic dextrin clathrate complex thing and pomace are separated from pure mellow wine with end slag, face slag.
8) ferment after: extract Primary Fermentation pure mellow wine tank out and become canful (liquid level is from tank actinal surface 10cm left and right), add the SO of 30mg/L
2, temperature control 15-20 ℃, through 14-16 days (containing 6 days clarification phases), rear ferment finished; Allow pure mellow wine naturally clarify, the wine degree reaches 12 degree or, more than 14 degree, below residual sugar 0.4g/100ml, acidity 0.6-0.8g/100ml, finish rear ferment.After taking out limpid wine liquid and becoming canful, more than supplying pure mellow wine wine degree 14 degree with white orchid ground wine, add the SO of 100mg/L
2, enter the ageing phase, at this moment be called former wine; The distillation of wine pin is white orchid ground wine.Face slag and end slag are through fermentation ends, and after extracting its pure mellow wine out, the recrement distillation is white orchid ground wine.
9) ageing: after 2-3 month ageing, carry out tank switching one time, former wine also becomes canful, and the wine pin is concentrated and clarified, last wine pin distillation white orchid ground wine.After former wine ageing half a year (through aestivate) again tank switching once, surpass every 1 year, 2 years tank switchings of former wine of 1 year ageing phase once later, operation is the same.
10) lower glue, allotment, sterilizing, filtration obtain finished product: lower glue after former 8 months phases of wine ageing, and under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 0.6-2.5g/100ml, glue is clarified former wine, and time 8-15 days, after blending allotment, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
The inventor completes the present invention program's design and lab scale from first arrival in 2010 in March, 2012, and in company's pilot scale successes such as Sichuan China orange wine industry companies, obtain promising result in December, 2012, proves that the inventive method is practical.
Compared with prior art, the beneficial effect that the present invention has is:
1, before fermentation, adopt cyclodextrin to carry out the inclusion complexation reaction to tangerine oil and bitter principle material simultaneously, can be fermented after reaction, after fermentation, the inclusion complexation reactant is separated from wine.Do not need de-oiling, debitterize are taked to independent operation, simplify like this production process, save human and material resources, reduce production costs.Be applicable to produce fermented orange wine after mechanize squeezing orange blossom, filled up the blank that machine-processed fermented orange wine is produced.
2, preferred beta-cyclodextrin in cyclodextrin, beta-cyclodextrin has hydrophilic surface relative to, a relatively hydrophobic center, so it can react with generation inclusion complexations such as tangerine oil, naringins in orange blossom, thereby the materials such as tangerine oil, naringin " are inlayed " in the middle of ring, be that the matter interactions such as beta-cyclodextrin and tangerine oil, naringin have formed new mixture, make tangerine oil lose bacteriostatic action, de-oiling, debitterize are totally thorough, are the assurances that wine fermentation is obtained better quality.
3, the present invention, at normal temperatures with regard to energy de-oiling, debitterize, makes oranges and tangerines can keep well the fine local flavor of its intrinsic gracefulness, exquisiteness.By test, during fermentation, not only ferment all right, and vinosity is graceful, fine and smooth, without bitter taste, the assorted flavor of naivete, there is the distinctive fragrance flavor of oranges and tangerines.
4, due to the sugary only 8%-11% of orange blossom, sugary more than 22% lower than Wine grape, the present invention, except adding sucrose in fermentation, allotment, has also added part Fructus Hordei Germinatus maltose, honey and soybean oligopeptide powder, maize oligopeptide powder, to improve nutrition and the local flavor of oranges and tangerines fermented wine.
5, the present invention activates yeast and adopts sucrose water, can fully improve the breeding potential of yeast.
Embodiment:
Embodiment mono-:
The present embodiment orange wine makes by following steps:
1) anti-oxidant brown stain: the clear juice of the oranges and tangerines that juice extractor is squeezed out, pulp add the saccharosonic acid of juice, pulp weight 0.1 ‰ clearly immediately, and pulp is delivered to the squeezing of stoning juice extractor and gets the clear juice of two road oranges and tangerines, and the clear juice of twice is merged to obtain to orange juice.
2) acid adjustment: in orange juice, add food grade CaCO
3acid adjustment is to 0.7g/100ml, stirs that within 20 minutes, to reach neutralization reaction complete.
3) de-oiling, debitterize: in the orange juice after acid adjustment, add the cyclodextrin (selecting β-CD here) of orange juice weight 1.5% fully to stir 20 minutes, make cyclodextrin to the tangerine oil in orange juice and bitter principle material inclusion complexation sufficient reacting.
4) adjust sugar: the sucrose of take allotment orange juice total reducing sugar is 22g/100ml, obtains allotment fruit juice.
5) yeast preparation:
The one-level preparation:
Get triangular flask, the sterilizing syrup of dress 5g/100ml, to the active fruit wine dried yeast powder (select Angel Yeast BV818 here, also can select other fruit wine dried yeast powder) that adds 10g/100ml in the sterilizing syrup, in 37 ℃ of activation 15 minutes, obtain the activation yeast slurry;
Two-stage system is standby:
The allotment fruit juice of packing in the Ka Shi tank, the activation yeast slurry to adding allotment fruit juice weight 10% in allotment fruit juice, shake up 33 ℃ of temperature controls and cultivate 2 hours, obtains the yeast kind;
Three tier structure is standby:
The allotment fruit juice of packing in the distiller's yeast tank, to the yeast kind that moves into allotment fruit juice weight 10% in allotment fruit juice, 25 ℃ of temperature controls are cultivated 7 hours, obtain distiller's yeast liquid.
6) fermentation: will allocate fruit juice and pump into the sterilization fermentor tank, the distiller's yeast liquid fermentation of 18 ℃ of access allotment fruit juice weight 12% of product temperature.
7) mend sugared supervention ferment: when the sugary 6g/100ml of dropping to of fermented liquid, add Fructus Hordei Germinatus maltose and honeybee sugar, Fructus Hordei Germinatus maltose 7g/100ml, honeybee sugar 2g/100ml; The SO that adds again 35mg/L
218 ℃ of continuation fermentations of temperature control.The yeast growth animated period is 20 ℃ of temperature controls later, allow its static fermentation.Through left and right Primary Fermentation in 10 days, finish again.More than wine degree 12 degree, below sugared 2g/100ml, extraction middle level pure mellow wine enters another tank and enters rear ferment.Face slag and end slag concentrate on a tank secondary fermentation.β-CD Inclusion Complexes and pomace are separated from pure mellow wine with end slag, face slag.
8) ferment after: extract Primary Fermentation pure mellow wine tank out and become canful (liquid level is from tank actinal surface 10cm left and right), add the SO of 30mg/L
2, 15 ℃ of temperature controls, through 16 days (containing 6 days clarification phases), rear ferment finished; Allow pure mellow wine naturally clarify, more than the wine degree reaches 12 degree, below residual sugar 0.4g/100ml, acidity 0.8g/100ml, ferment after finishing.After taking out limpid wine liquid and becoming canful, more than supplying pure mellow wine wine degree 14 degree with white orchid ground wine, add the SO of 100mg/L
2, enter the ageing phase.
9) ageing: after 2-3 month ageing, carry out tank switching one time, former wine also becomes canful, and the wine pin is concentrated and clarified, last wine pin distillation white orchid ground wine.After former wine ageing half a year (through aestivate) again tank switching once, surpass every 1 year, 2 years tank switchings of former wine of 1 year ageing phase once later, operation is the same.
10) lower glue, allotment, sterilizing, filtration obtain finished product: lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 0.6g/100ml, glue is clarified former wine, 15 days time, after blending allotment, adds the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
The production technique of the present embodiment orange wine comprises the following steps:
1) anti-oxidant brown stain: the clear juice of the oranges and tangerines that juice extractor is squeezed out, pulp add the saccharosonic acid of juice, pulp weight 0.1 ‰ clearly immediately, and pulp is delivered to the squeezing of stoning juice extractor and gets the clear juice of two road oranges and tangerines, and the clear juice of twice is merged to obtain to orange juice.
2) acid adjustment: in orange juice, add food grade CaCO
3acid adjustment is to 0.7g/100ml, stirs that within 20 minutes, to reach neutralization reaction complete.
3) de-oiling, debitterize: in the orange juice after acid adjustment, add the cyclodextrin (selecting β-CD here) of orange juice weight 1.5% fully to stir 20 minutes, make cyclodextrin to the tangerine oil in orange juice and bitter principle material inclusion complexation sufficient reacting.
4) adjust sugar: the sucrose of take allotment orange juice total reducing sugar is 22g/100ml, obtains allotment fruit juice.
5) yeast preparation:
The one-level preparation:
Get triangular flask, the sterilizing syrup of dress 5g/100ml, to the active fruit wine dried yeast powder (select Angel Yeast BV818 here, also can select other fruit wine dried yeast powder) that adds 10g/100ml in the sterilizing syrup, in 37 ℃ of activation 15 minutes, obtain the activation yeast slurry;
Two-stage system is standby:
The allotment fruit juice of packing in the Ka Shi tank, the activation yeast slurry to adding allotment fruit juice weight 10% in allotment fruit juice, shake up 33 ℃ of temperature controls and cultivate 2 hours, obtains the yeast kind;
Three tier structure is standby:
The allotment fruit juice of packing in the distiller's yeast tank, to the yeast kind that moves into allotment fruit juice weight 10% in allotment fruit juice, 25 ℃ of temperature controls are cultivated 7 hours, obtain distiller's yeast liquid.
6) fermentation: will allocate fruit juice and pump into the sterilization fermentor tank, the distiller's yeast liquid fermentation of 18 ℃ of access allotment fruit juice weight 12% of product temperature.
7) mend sugared supervention ferment: when the sugary 6g/100ml of dropping to of fermented liquid, add Fructus Hordei Germinatus maltose and honeybee sugar, Fructus Hordei Germinatus maltose 7g/100ml, honeybee sugar 2g/100ml; The SO that adds again 35mg/L
218 ℃ of continuation fermentations of temperature control.The yeast growth animated period is 20 ℃ of temperature controls later, allow its static fermentation.Through left and right Primary Fermentation in 10 days, finish again.More than wine degree 12 degree, below sugared 2g/100ml, extraction middle level pure mellow wine enters another tank and enters rear ferment.Face slag and end slag concentrate on a tank secondary fermentation.β-CD Inclusion Complexes and pomace are separated from pure mellow wine with end slag, face slag.
8) ferment after: extract Primary Fermentation pure mellow wine tank out and become canful (liquid level is from tank actinal surface 10cm left and right), add the SO of 30mg/L
2, 15 ℃ of temperature controls, through 16 days (containing 6 days clarification phases), rear ferment finished; Allow pure mellow wine naturally clarify, more than the wine degree reaches 12 degree, below residual sugar 0.4g/100ml, acidity 0.8g/100ml, ferment after finishing.After taking out limpid wine liquid and becoming canful, more than supplying pure mellow wine wine degree 14 degree with white orchid ground wine, add the SO of 100mg/L
2, enter the ageing phase.
9) ageing: after 2-3 month ageing, carry out tank switching one time, former wine also becomes canful, and the wine pin is concentrated and clarified, last wine pin distillation white orchid ground wine.After former wine ageing half a year (through aestivate) again tank switching once, surpass every 1 year, 2 years tank switchings of former wine of 1 year ageing phase once later, operation is the same.
10) lower glue, allotment, sterilizing, filtration obtain finished product: lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 0.6g/100ml, glue is clarified former wine, 15 days time, after blending allotment, adds the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment bis-:
The present embodiment orange wine makes by following steps:
1) anti-oxidant brown stain: the clear juice of the oranges and tangerines that juice extractor is squeezed out, pulp add the saccharosonic acid of juice, pulp weight 0.2 ‰ clearly immediately, and pulp is delivered to the squeezing of stoning juice extractor and gets the clear juice of two road oranges and tangerines, and the clear juice of twice is merged to obtain to orange juice.
2) acid adjustment: in orange juice, add food grade CaCO
3acid adjustment is to 0.6g/100ml, stirs that within 25 minutes, to reach neutralization reaction complete.
3) de-oiling, debitterize: in the orange juice after acid adjustment, add the cyclodextrin (selecting alpha-cylodextrin here) of orange juice weight 0.2% fully to stir 30 minutes, make cyclodextrin to the tangerine oil in orange juice and bitter principle material inclusion complexation sufficient reacting.
4) adjust sugar: the sucrose of take allotment orange juice total reducing sugar is 20g/100ml, obtains allotment fruit juice.
5) yeast preparation:
The one-level preparation:
Get triangular flask, the sterilizing syrup of dress 8g/100ml, to the active fruit wine dried yeast powder (select Angel Yeast BV818 here, also can select other fruit wine dried yeast powder) that adds 10g/100ml in the sterilizing syrup, in 33 ℃ of activation 25 minutes, obtain the activation yeast slurry;
Two-stage system is standby:
The allotment fruit juice of packing in the Ka Shi tank, the activation yeast slurry to adding allotment fruit juice weight 10% in allotment fruit juice, shake up 25 ℃ of temperature controls and cultivate 4 hours, obtains the yeast kind;
Three tier structure is standby:
The allotment fruit juice of packing in the distiller's yeast tank, to the yeast kind that moves into allotment fruit juice weight 5% in allotment fruit juice, 20 ℃ of temperature controls are cultivated 9 hours, obtain distiller's yeast liquid.
6) fermentation: will allocate fruit juice and pump into the sterilization fermentor tank, the distiller's yeast liquid fermentation of 22 ℃ of access allotment fruit juice weight 8% of product temperature.
7) mend sugared supervention ferment: when the sugary 8g/100ml of dropping to of fermented liquid, add Fructus Hordei Germinatus maltose and honeybee sugar, Fructus Hordei Germinatus maltose 5g/100ml, honeybee sugar 4g/100ml; The SO that adds again 25mg/L
222 ℃ of continuation fermentations of temperature control.The yeast growth animated period is 15 ℃ of temperature controls later, allow its static fermentation.Through left and right Primary Fermentation in 10 days, finish again.More than wine degree 12 degree, below sugared 2g/100ml, extraction middle level pure mellow wine enters another tank and enters rear ferment.Face slag and end slag concentrate on a tank secondary fermentation.Alpha-cylodextrin Inclusion Complexes and pomace are separated from pure mellow wine with end slag, face slag.
8) ferment after: extract Primary Fermentation pure mellow wine tank out and become canful (liquid level is from tank actinal surface 10cm left and right), add the SO of 30mg/L
2, 20 ℃ of temperature controls, through 14 days (containing 6 days clarification phases), rear ferment finished; Allow pure mellow wine naturally clarify, more than the wine degree reaches 14 degree, below residual sugar 0.4g/100ml, acidity 0.6g/100ml, ferment after finishing.After taking out limpid wine liquid and becoming canful, more than supplying pure mellow wine wine degree 14 degree with white orchid ground wine, add the SO of 100mg/L
2, enter the ageing phase.
9) ageing: after 2-3 month ageing, carry out tank switching one time, former wine also becomes canful, and the wine pin is concentrated and clarified, last wine pin distillation white orchid ground wine.After former wine ageing half a year (through aestivate) again tank switching once, surpass every 1 year, 2 years tank switchings of former wine of 1 year ageing phase once later, operation is the same.
10) lower glue, allotment, sterilizing, filtration obtain finished product: lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 2.5g/100ml, glue is clarified former wine, 8 days time, after blending allotment, adds the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
The production technique of the present embodiment orange wine comprises the following steps:
1) anti-oxidant brown stain: the clear juice of the oranges and tangerines that juice extractor is squeezed out, pulp add the saccharosonic acid of juice, pulp weight 0.2 ‰ clearly immediately, and pulp is delivered to the squeezing of stoning juice extractor and gets the clear juice of two road oranges and tangerines, and the clear juice of twice is merged to obtain to orange juice.
2) acid adjustment: in orange juice, add food grade CaCO
3acid adjustment is to 0.6g/100ml, stirs that within 25 minutes, to reach neutralization reaction complete.
3) de-oiling, debitterize: in the orange juice after acid adjustment, add the cyclodextrin (selecting alpha-cylodextrin here) of orange juice weight 0.2% fully to stir 30 minutes, make cyclodextrin to the tangerine oil in orange juice and bitter principle material inclusion complexation sufficient reacting.
4) adjust sugar: the sucrose of take allotment orange juice total reducing sugar is 20g/100ml, obtains allotment fruit juice.
5) yeast preparation:
The one-level preparation:
Get triangular flask, the sterilizing syrup of dress 8g/100ml, to the active fruit wine dried yeast powder (select Angel Yeast BV818 here, also can select other fruit wine dried yeast powder) that adds 10g/100ml in the sterilizing syrup, in 33 ℃ of activation 25 minutes, obtain the activation yeast slurry;
Two-stage system is standby:
The allotment fruit juice of packing in the Ka Shi tank, the activation yeast slurry to adding allotment fruit juice weight 10% in allotment fruit juice, shake up 25 ℃ of temperature controls and cultivate 4 hours, obtains the yeast kind;
Three tier structure is standby:
The allotment fruit juice of packing in the distiller's yeast tank, to the yeast kind that moves into allotment fruit juice weight 5% in allotment fruit juice, 20 ℃ of temperature controls are cultivated 9 hours, obtain distiller's yeast liquid.
6) fermentation: will allocate fruit juice and pump into the sterilization fermentor tank, the distiller's yeast liquid fermentation of 22 ℃ of access allotment fruit juice weight 8% of product temperature.
7) mend sugared supervention ferment: when the sugary 8g/100ml of dropping to of fermented liquid, add Fructus Hordei Germinatus maltose and honeybee sugar, Fructus Hordei Germinatus maltose 5g/100ml, honeybee sugar 4g/100ml; The SO that adds again 25mg/L
222 ℃ of continuation fermentations of temperature control.The yeast growth animated period is 15 ℃ of temperature controls later, allow its static fermentation.Through left and right Primary Fermentation in 10 days, finish again.More than wine degree 12 degree, below sugared 2g/100ml, extraction middle level pure mellow wine enters another tank and enters rear ferment.Face slag and end slag concentrate on a tank secondary fermentation.Alpha-cylodextrin Inclusion Complexes and pomace are separated from pure mellow wine with end slag, face slag.
8) ferment after: extract Primary Fermentation pure mellow wine tank out and become canful (liquid level is from tank actinal surface 10cm left and right), add the SO of 30mg/L
2, 20 ℃ of temperature controls, through 14 days (containing 6 days clarification phases), rear ferment finished; Allow pure mellow wine naturally clarify, more than the wine degree reaches 14 degree, below residual sugar 0.4g/100ml, acidity 0.6g/100ml, ferment after finishing.After taking out limpid wine liquid and becoming canful, more than supplying pure mellow wine wine degree 14 degree with white orchid ground wine, add the SO of 100mg/L
2, enter the ageing phase.
9) ageing: after 2-3 month ageing, carry out tank switching one time, former wine also becomes canful, and the wine pin is concentrated and clarified, last wine pin distillation white orchid ground wine.After former wine ageing half a year (through aestivate) again tank switching once, surpass every 1 year, 2 years tank switchings of former wine of 1 year ageing phase once later, operation is the same.
10) lower glue, allotment, sterilizing, filtration obtain finished product: lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 2.5g/100ml, glue is clarified former wine, 8 days time, after blending allotment, adds the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment tri-:
The present embodiment orange wine makes by following steps:
1) anti-oxidant brown stain: the clear juice of the oranges and tangerines that juice extractor is squeezed out, pulp add the saccharosonic acid of juice, pulp weight 0.15 ‰ clearly immediately, and pulp is delivered to the squeezing of stoning juice extractor and gets the clear juice of two road oranges and tangerines, and the clear juice of twice is merged to obtain to orange juice.
2) acid adjustment: in orange juice, add food grade CaCO
3acid adjustment is to 0.65g/100ml, stirs that within 22 minutes, to reach neutralization reaction complete.
3) de-oiling, debitterize: in the orange juice after acid adjustment, add the cyclodextrin (selecting γ-cyclodextrin here) of orange juice weight 1% fully to stir 25 minutes, make cyclodextrin to the tangerine oil in orange juice and bitter principle material inclusion complexation sufficient reacting.
4) adjust sugar: the sucrose of take allotment orange juice total reducing sugar is 21g/100ml, obtains allotment fruit juice.
5) yeast preparation:
The one-level preparation:
Get triangular flask, the sterilizing syrup of dress 6g/100ml, to the active fruit wine dried yeast powder (select Angel Yeast BV818 here, also can select other fruit wine dried yeast powder) that adds 10g/100ml in the sterilizing syrup, in 35 ℃ of activation 20 minutes, obtain the activation yeast slurry;
Two-stage system is standby:
The allotment fruit juice of packing in the Ka Shi tank, the activation yeast slurry to adding allotment fruit juice weight 10% in allotment fruit juice, shake up 28 ℃ of temperature controls and cultivate 3 hours, obtains the yeast kind;
Three tier structure is standby:
The allotment fruit juice of packing in the distiller's yeast tank, to the yeast kind that moves into allotment fruit juice weight 7% in allotment fruit juice, 22 ℃ of temperature controls are cultivated 8 hours, obtain distiller's yeast liquid.
6) fermentation: will allocate fruit juice and pump into the sterilization fermentor tank, the distiller's yeast liquid fermentation of 20 ℃ of access allotment fruit juice weight 10% of product temperature.
7) mend sugared supervention ferment: when the sugary 7g/100ml of dropping to of fermented liquid, add Fructus Hordei Germinatus maltose and honeybee sugar, Fructus Hordei Germinatus maltose 6g/100ml, honeybee sugar 3g/100ml; The SO that adds again 30mg/L
220 ℃ of continuation fermentations of temperature control.The yeast growth animated period is 18 ℃ of temperature controls later, allow its static fermentation.Through left and right Primary Fermentation in 10 days, finish again.More than wine degree 12 degree, below sugared 2g/100ml, extraction middle level pure mellow wine enters another tank and enters rear ferment.Face slag and end slag concentrate on a tank secondary fermentation.γ-cyclodextrin Inclusion Complexes and pomace are separated from pure mellow wine with end slag, face slag.
8) ferment after: extract Primary Fermentation pure mellow wine tank out and become canful (liquid level is from tank actinal surface 10cm left and right), add the SO of 30mg/L
2, 18 ℃ of temperature controls, through 15 days (containing 6 days clarification phases), rear ferment finished; Allow pure mellow wine naturally clarify, more than the wine degree reaches 12 degree, below residual sugar 0.4g/100ml, acidity 0.7g/100ml, ferment after finishing.After taking out limpid wine liquid and becoming canful, more than supplying pure mellow wine wine degree 14 degree with white orchid ground wine, add the SO of 100mg/L
2, enter the ageing phase.
9) ageing: after 2-3 month ageing, carry out tank switching one time, former wine also becomes canful, and the wine pin is concentrated and clarified, last wine pin distillation white orchid ground wine.After former wine ageing half a year (through aestivate) again tank switching once, surpass every 1 year, 2 years tank switchings of former wine of 1 year ageing phase once later, operation is the same.
10) lower glue, allotment, sterilizing, filtration obtain finished product: lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 2g/100ml, glue is clarified former wine, 10 days time, after blending allotment, adds the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
The production technique of the present embodiment orange wine comprises the following steps:
1) anti-oxidant brown stain: the clear juice of the oranges and tangerines that juice extractor is squeezed out, pulp add the saccharosonic acid of juice, pulp weight 0.15 ‰ clearly immediately, and pulp is delivered to the squeezing of stoning juice extractor and gets the clear juice of two road oranges and tangerines, and the clear juice of twice is merged to obtain to orange juice.
2) acid adjustment: in orange juice, add food grade CaCO
3acid adjustment is to 0.65g/100ml, stirs that within 22 minutes, to reach neutralization reaction complete.
3) de-oiling, debitterize: in the orange juice after acid adjustment, add the cyclodextrin (selecting γ-cyclodextrin here) of orange juice weight 1% fully to stir 25 minutes, make cyclodextrin to the tangerine oil in orange juice and bitter principle material inclusion complexation sufficient reacting.
4) adjust sugar: the sucrose of take allotment orange juice total reducing sugar is 21g/100ml, obtains allotment fruit juice.
5) yeast preparation:
The one-level preparation:
Get triangular flask, the sterilizing syrup of dress 6g/100ml, to the active fruit wine dried yeast powder (select Angel Yeast BV818 here, also can select other fruit wine dried yeast powder) that adds 10g/100ml in the sterilizing syrup, in 35 ℃ of activation 20 minutes, obtain the activation yeast slurry;
Two-stage system is standby:
The allotment fruit juice of packing in the Ka Shi tank, the activation yeast slurry to adding allotment fruit juice weight 10% in allotment fruit juice, shake up 28 ℃ of temperature controls and cultivate 3 hours, obtains the yeast kind;
Three tier structure is standby:
The allotment fruit juice of packing in the distiller's yeast tank, to the yeast kind that moves into allotment fruit juice weight 7% in allotment fruit juice, 22 ℃ of temperature controls are cultivated 8 hours, obtain distiller's yeast liquid.
6) fermentation: will allocate fruit juice and pump into the sterilization fermentor tank, the distiller's yeast liquid fermentation of 20 ℃ of access allotment fruit juice weight 10% of product temperature.
7) mend sugared supervention ferment: when the sugary 7g/100ml of dropping to of fermented liquid, add Fructus Hordei Germinatus maltose and honeybee sugar, Fructus Hordei Germinatus maltose 6g/100ml, honeybee sugar 3g/100ml; The SO that adds again 30mg/L
220 ℃ of continuation fermentations of temperature control.The yeast growth animated period is 18 ℃ of temperature controls later, allow its static fermentation.Through left and right Primary Fermentation in 10 days, finish again.More than wine degree 12 degree, below sugared 2g/100ml, extraction middle level pure mellow wine enters another tank and enters rear ferment.Face slag and end slag concentrate on a tank secondary fermentation.γ-cyclodextrin Inclusion Complexes and pomace are separated from pure mellow wine with end slag, face slag.
8) ferment after: extract Primary Fermentation pure mellow wine tank out and become canful (liquid level is from tank actinal surface 10cm left and right), add the SO of 30mg/L
2, 18 ℃ of temperature controls, through 15 days (containing 6 days clarification phases), rear ferment finished; Allow pure mellow wine naturally clarify, more than the wine degree reaches 12 degree, below residual sugar 0.4g/100ml, acidity 0.7g/100ml, ferment after finishing.After taking out limpid wine liquid and becoming canful, more than supplying pure mellow wine wine degree 14 degree with white orchid ground wine, add the SO of 100mg/L
2, enter the ageing phase.
9) ageing: after 2-3 month ageing, carry out tank switching one time, former wine also becomes canful, and the wine pin is concentrated and clarified, last wine pin distillation white orchid ground wine.After former wine ageing half a year (through aestivate) again tank switching once, surpass every 1 year, 2 years tank switchings of former wine of 1 year ageing phase once later, operation is the same.
10) lower glue, allotment, sterilizing, filtration obtain finished product: lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 2g/100ml, glue is clarified former wine, 10 days time, after blending allotment, adds the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment tetra-:
Other technical scheme of the present embodiment is identical with the technical scheme of arbitrary embodiment in embodiment mono-to three, different is lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 0.6g/100ml, glue is clarified former wine, 15 days time, to the tangerine oil that adds former wine weight 0.01%-0.02% in former wine, the fragrant fruity of aquatic foods in order to modulate orange wine, after blending allotment, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment five:
Other technical scheme of the present embodiment is identical with the technical scheme of arbitrary embodiment in embodiment mono-to three, different is lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 2.5g/100ml, glue is clarified former wine, 8 days time, to the soybean oligopeptide powder that adds 0.1-0.2g/100ml in former wine, after blending allotment, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment six:
Other technical scheme of the present embodiment is identical with the technical scheme of arbitrary embodiment in embodiment mono-to three, different is lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 2g/100ml, glue is clarified former wine, 10 days time, to the maize oligopeptide powder that adds 0.2-0.5g/100ml in former wine, after blending allotment, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment seven:
Other technical scheme of the present embodiment is identical with the technical scheme of arbitrary embodiment in embodiment mono-to three, different is lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 0.6g/100ml, glue is clarified former wine, 15 days time, add the soybean oligopeptide powder of 0.1-0.2g/100ml and the maize oligopeptide powder of 0.2-0.5g/100ml in former wine, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment eight:
Other technical scheme of the present embodiment is identical with the technical scheme of arbitrary embodiment in embodiment mono-to three, different is lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 2g/100ml, glue is clarified former wine, 10 days time, add vitamins C 100mg in the former wine of every L, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment nine:
Other technical scheme of the present embodiment is identical with the technical scheme of arbitrary embodiment in embodiment mono-to three, different is lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 0.6g/100ml, glue is clarified former wine, 15 days time, add the soybean oligopeptide powder of 0.1-0.2g/100ml, the maize oligopeptide powder of 0.2-0.5g/100ml and the vitamins C of 100mg/L in former wine, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
Embodiment ten:
Other technical scheme of the present embodiment is identical with the technical scheme of arbitrary embodiment in embodiment mono-to three, different is lower glue after former 8 months phases of wine ageing, under the Ovum Gallus domesticus album of employing 0.5g/100ml or the bentonite of 0.6g/100ml, glue is clarified former wine, 15 days time, add the soybean oligopeptide powder of 0.1-0.2g/100ml, the maize oligopeptide powder of 0.2-0.5g/100ml, the tangerine oil of 0.01%-0.02% and the vitamins C of 100mg/L in former wine, add the SO of 80mg/L
2.Sweet wine is by pasteurize, then by diatomite filter coarse filtration and essence filter, then store one month; Dry wine adopts diatomite microporous membrane heat sterilization.Rear filling finished product up to standard.
In a word, soybean oligopeptide powder, maize oligopeptide powder, tangerine oil and vitamins C can be added in the backward former wine of lower glue after arbitrary combination, improve local flavor and the nutritive value of orange wine.