CN102978961A - Preparation method of long-acting slow-release fragrance silk quilt - Google Patents
Preparation method of long-acting slow-release fragrance silk quilt Download PDFInfo
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- CN102978961A CN102978961A CN2012104925888A CN201210492588A CN102978961A CN 102978961 A CN102978961 A CN 102978961A CN 2012104925888 A CN2012104925888 A CN 2012104925888A CN 201210492588 A CN201210492588 A CN 201210492588A CN 102978961 A CN102978961 A CN 102978961A
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Abstract
The invention relates to a preparation method of a long-acting slow-release fragrance silk quilt. The preparation method comprises the following steps of: (1) refining, bleaching, rinsing and dewatering cocoon strippings to obtain silks with the cleanliness of 99 percent; (2) putting the silks treated in the step (1) into a reaction tank, injecting a fragrance mixed solution of which the temperature is 50 to 60 DEG C into the reaction tank, keeping the temperature for 30 to 40 minutes, and performing pliancy and fragrance treatment on the silks; (3) taking out the silks subjected to the pliancy and fragrance treatment, dewatering the silks until the water content is less than 25 percent, and taking out and drying the silks; (4) carding the dried silks into a silk quilt batt, attaching a gauze fabric to the silk quilt batt, and performing fixed-point fixation to ensure that the gauze fabric is fully attached to the silks; and (5) covering the silk quilt batt by using a fabric, and quilting. By the preparation method, the original taste of the conventional silks is changed, the prepared silk quilt has a lasting fresh fragrance and better hand feeling, the silks cannot cause silk loss and make people feel fresh, and during preparation, an adhesive is not added, so that the silk quilt is soft in hand feeling in use and cannot generate yellowing.
Description
Technical field
The present invention relates to a kind of preparation method of cocoon silk quilt, particularly a kind of preparation method of long-acting slow-release fragrance cocoon silk quilt.
Background technology
Cocoon silk quilt has lightweight, and fiber is long, and is warming good, breathes freely, and is called as the elaboration in the cotton-padded mattress, the superfine product on the bed, and people also constantly increase the research of cocoon silk quilt in recent years, enter one after another people's life such as products such as negative ion silk quilts.And silk in use has the natural taste of silk, and a lot of consumers can not adapt to it, has greatly affected the applicable crowd of cocoon silk quilt.
Therefore, need especially a kind of preparation method of long-acting slow-release fragrance cocoon silk quilt, solved the problem of above-mentioned existing existence.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of long-acting slow-release fragrance cocoon silk quilt, for the deficiencies in the prior art, make product have the function of lasting release fragrance, fragrance silk fragrance is effectively discharged, do not affect the serviceability of cocoon silk quilt simultaneously.
Technical problem solved by the invention can realize by the following technical solutions:
A kind of preparation method of long-acting slow-release fragrance cocoon silk quilt is characterized in that it comprises the steps:
(1) the cocoon skin by refining, bleaching, flushing and dehydration, obtain cleanliness factor and reach 99% silk;
(2) silk of processing in (1) is put into retort, inject 50-60 ℃ fragrance mixed solution, kept temperature 30-40 minute, carry out submissive and the fragrance processing to silk;
(3) silk after submissive and fragrance is processed takes out, dewater to moisture less than 25%, take out oven dry;
(4) will dry after silk be carded to the silk comforter batt, enclose the gauze fabric and fix a point to fix, gauze fabric and silk are fully fitted;
(5) the silk comforter batt is coated with fabric, and quilting.
In one embodiment of the invention, described fragrance mixed solution comprises the component of following percentage by weight: hydrophilic amino silicone oil 8-12%, and bleeding agent 3-5%, glacial acetic acid 5-10%, fragrance microcapsules 10-20%, deionized water 20-40%, surplus is water.
Further, described fragrance microcapsules comprise rose fragrance microcapsules, lavender fragrance microcapsules, jasmine fragrance microcapsules or all sorts of flowers fragrance microcapsules.
Further, described bleeding agent be He Te 5788JFC-1, in spin a kind of among the OEP-70 of the JFC-C of chemical industry or Xing state chemical industry.
In one embodiment of the invention, the pH value of described fragrance mixed solution is 5-7.
In one embodiment of the invention, the temperature of described retort is 50-60 ℃.
In one embodiment of the invention, the weight ratio of described silk and fragrance mixed solution is 1:15-20.
In one embodiment of the invention, the temperature of described oven dry is 60-90 ℃.
The preparation method of long-acting slow-release fragrance cocoon silk quilt of the present invention, compared with prior art, it is former flavoursome to have changed traditional silk, and the cocoon silk quilt of preparation has lasting pure and fresh fragrance, better feel and silk can output not run the hair phenomenon, improve the taste of natural silk, give pure and fresh sensation, continuing to use after 1 year still has light fragrance, in preparation process, do not add adhesive, cocoon silk quilt is in use soft, can not produce yellowing phenomenon, realizes purpose of the present invention.
Characteristics of the present invention can be consulted the detailed description of the following better embodiment of this case and be obtained to be well understood to.
The specific embodiment
For technological means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, below in conjunction with specifically, further set forth the present invention.
The preparation method of long-acting slow-release fragrance cocoon silk quilt of the present invention, it comprises the steps:
(1) the cocoon skin by refining, bleaching, flushing and dehydration, obtain cleanliness factor and reach 99% silk;
(2) silk of processing in (1) is put into retort, inject 50-60 ℃ fragrance mixed solution, kept temperature 30-40 minute, carry out submissive and the fragrance processing to silk;
(3) silk after submissive and fragrance is processed takes out, dewater to moisture less than 25%, take out oven dry;
(4) will dry after silk be carded to the silk comforter batt, enclose the gauze fabric and fix a point to fix, gauze fabric and silk are fully fitted;
(5) the silk comforter batt is coated with fabric, and quilting.
In the present invention, described fragrance mixed solution comprises the component of following percentage by weight: hydrophilic amino silicone oil 8-12%, and bleeding agent 3-5%, glacial acetic acid 5-10%, fragrance microcapsules 10-20%, deionized water 20-40%, surplus is water.
Described fragrance microcapsules comprise rose fragrance microcapsules, lavender fragrance microcapsules, jasmine fragrance microcapsules or all sorts of flowers fragrance microcapsules.
Described bleeding agent be He Te 5788JFC-1, in spin a kind of among the OEP-70 of the JFC-C of chemical industry or Xing state chemical industry.
In the present invention, the pH value of described fragrance mixed solution is 5-7.
In the present invention, the temperature of described retort is 50-60 ℃.
In the present invention, the weight ratio of described silk and fragrance mixed solution is 1:15-20.
In the present invention, the temperature of described oven dry is 60-90 ℃.
Coat quilting with light and thin fabric again after long-acting slow-release fragrance cocoon silk quilt of the present invention has adopted the gauze fabric to coat, silk and gauze are fully fitted, greatly improve the feel of cocoon silk quilt, do not run the hair phenomenon but can not produce.
Embodiment 1
(1) the cocoon skin by refining, bleaching, flushing and dehydration, obtain cleanliness factor and reach 99% silk;
(2) silk of processing in (1) is put into retort, inject 50 ℃ fragrance mixed solution, kept temperature 30 minutes, carry out submissive and the fragrance processing to silk;
(3) silk after submissive and fragrance is processed takes out, dewater to moisture less than 25%, take out oven dry;
(4) will dry after silk be carded to the silk comforter batt, enclose the gauze fabric and fix a point to fix, gauze fabric and silk are fully fitted;
(5) the silk comforter batt is coated with fabric, and quilting.
Wherein, described fragrance mixed solution comprises the component of following percentage by weight: hydrophilic amino silicone oil 8%, and bleeding agent 3%, glacial acetic acid 5%, fragrance microcapsules 10%, deionized water 20%, surplus is water.
Described fragrance microcapsules comprise rose fragrance microcapsules, lavender fragrance microcapsules, jasmine fragrance microcapsules or all sorts of flowers fragrance microcapsules.Described bleeding agent is the 5788JFC-1 of He Te.The pH value of described fragrance mixed solution is 5.The temperature of described retort is 50 ℃.The weight ratio of described silk and fragrance mixed solution is 1:15.The temperature of described oven dry is 60 ℃.
Embodiment 2
(1) the cocoon skin by refining, bleaching, flushing and dehydration, obtain cleanliness factor and reach 99% silk;
(2) silk of processing in (1) is put into retort, inject 60 ℃ fragrance mixed solution, kept temperature 40 minutes, carry out submissive and the fragrance processing to silk;
(3) silk after submissive and fragrance is processed takes out, dewater to moisture less than 25%, take out oven dry;
(4) will dry after silk be carded to the silk comforter batt, enclose the gauze fabric and fix a point to fix, gauze fabric and silk are fully fitted;
(5) the silk comforter batt is coated with fabric, and quilting.
Wherein, described fragrance mixed solution comprises the component of following percentage by weight: hydrophilic amino silicone oil 10%, and bleeding agent 4%, glacial acetic acid 8%, fragrance microcapsules 15%, deionized water 30%, surplus is water.
Described fragrance microcapsules comprise rose fragrance microcapsules, lavender fragrance microcapsules, jasmine fragrance microcapsules or all sorts of flowers fragrance microcapsules.During being included as, described bleeding agent spins the JFC-C of chemical industry.The pH value of described fragrance mixed solution is 7.The temperature of described retort is 60 ℃.The weight ratio of described silk and fragrance mixed solution is 1:20.The temperature of described oven dry is 90 ℃.
Embodiment 3
(1) the cocoon skin by refining, bleaching, flushing and dehydration, obtain cleanliness factor and reach 99% silk;
(2) silk of processing in (1) is put into retort, inject 55 ℃ fragrance mixed solution, kept temperature 35 minutes, carry out submissive and the fragrance processing to silk;
(3) silk after submissive and fragrance is processed takes out, dewater to moisture less than 25%, take out oven dry;
(4) will dry after silk be carded to the silk comforter batt, enclose the gauze fabric and fix a point to fix, gauze fabric and silk are fully fitted;
(5) the silk comforter batt is coated with fabric, and quilting.
Wherein, described fragrance mixed solution comprises the component of following percentage by weight: hydrophilic amino silicone oil 12%, and bleeding agent 5%, glacial acetic acid 10%, fragrance microcapsules 20%, deionized water 40%, surplus is water.
Described fragrance microcapsules comprise rose fragrance microcapsules, lavender fragrance microcapsules, jasmine fragrance microcapsules or all sorts of flowers fragrance microcapsules.Described bleeding agent is included as the OEP-70 of Xing state chemical industry.The pH value of described fragrance mixed solution is 6.The temperature of described retort is 55 ℃.The weight ratio of described silk and fragrance mixed solution is 1:18.The temperature of described oven dry is 75 ℃.
More than show and described basic principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that describes in above-described embodiment and the specification just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications; these changes and improvements all fall in the claimed scope of the invention, and the claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (8)
1. the preparation method of a long-acting slow-release fragrance cocoon silk quilt is characterized in that it comprises the steps:
(1) the cocoon skin by refining, bleaching, flushing and dehydration, obtain cleanliness factor and reach 99% silk;
(2) silk of processing in (1) is put into retort, inject 50-60 ℃ fragrance mixed solution, kept temperature 30-40 minute, carry out submissive and the fragrance processing to silk;
(3) silk after submissive and fragrance is processed takes out, dewater to moisture less than 25%, take out oven dry;
(4) will dry after silk be carded to the silk comforter batt, enclose the gauze fabric and fix a point to fix, gauze fabric and silk are fully fitted;
(5) the silk comforter batt is coated with fabric, and quilting.
2. the preparation method of long-acting slow-release fragrance cocoon silk quilt as claimed in claim 1, it is characterized in that, described fragrance mixed solution comprises the component of following percentage by weight: hydrophilic amino silicone oil 8-12%, bleeding agent 3-5%, glacial acetic acid 5-10%, fragrance microcapsules 10-20%, deionized water 20-40%, surplus is water.
3. the preparation method of long-acting slow-release fragrance cocoon silk quilt as claimed in claim 2 is characterized in that, described fragrance microcapsules comprise rose fragrance microcapsules, lavender fragrance microcapsules, jasmine fragrance microcapsules or lily fragrance microcapsules.
4. the preparation method of long-acting slow-release fragrance cocoon silk quilt as claimed in claim 2 is characterized in that, described bleeding agent be He Te 5788JFC-1, in spin a kind of among the OEP-70 of the JFC-C of chemical industry or Xing state chemical industry.
5. the preparation method of long-acting slow-release fragrance cocoon silk quilt as claimed in claim 1 is characterized in that, the pH value of described fragrance mixed solution is 5-7.
6. the preparation method of long-acting slow-release fragrance cocoon silk quilt as claimed in claim 1 is characterized in that, the temperature of described retort is 50-60 ℃.
7. the preparation method of long-acting slow-release fragrance cocoon silk quilt as claimed in claim 1 is characterized in that, the weight ratio of described silk and fragrance mixed solution is 1:15-20.
8. the preparation method of long-acting slow-release fragrance cocoon silk quilt as claimed in claim 1 is characterized in that, the temperature of described oven dry is 60-90 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN2012104925888A CN102978961A (en) | 2012-11-27 | 2012-11-27 | Preparation method of long-acting slow-release fragrance silk quilt |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012104925888A CN102978961A (en) | 2012-11-27 | 2012-11-27 | Preparation method of long-acting slow-release fragrance silk quilt |
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| CN102978961A true CN102978961A (en) | 2013-03-20 |
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| CN2012104925888A Pending CN102978961A (en) | 2012-11-27 | 2012-11-27 | Preparation method of long-acting slow-release fragrance silk quilt |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104687905A (en) * | 2015-03-25 | 2015-06-10 | 东华大学 | Production method of anti-aging silk quilt |
| CN104687904A (en) * | 2015-03-25 | 2015-06-10 | 东华大学 | Preparation method for sedative and dormitive silk quilt |
| CN105064046A (en) * | 2015-07-16 | 2015-11-18 | 华南师范大学 | Preparation method and application of fragrant microcapsule compounded organic silicone softener for cotton fabric |
| CN105361552A (en) * | 2015-11-13 | 2016-03-02 | 周克跃 | Silk-cotton composite quilt and production method thereof |
| CN105361553A (en) * | 2015-11-13 | 2016-03-02 | 周克跃 | Silk quilt and production method thereof |
| EP3064619A1 (en) * | 2015-02-27 | 2016-09-07 | COSETEX S.n.c. | Method of making a heat-insulating element, and heat-insulating element |
| CN106377122A (en) * | 2016-08-30 | 2017-02-08 | 江西金铭丝绸有限公司 | Preparation method of silk quilt |
| CN107419430A (en) * | 2015-09-01 | 2017-12-01 | 苏州先蚕丝绸生物科技有限公司 | A kind of feature silk non-woven fabric and its production method |
| CN107640071A (en) * | 2017-09-01 | 2018-01-30 | 广西桂华丝绸有限公司 | Jasmine tea perfume mulberry silk automobile seat back cushion |
| CN109137484A (en) * | 2018-09-18 | 2019-01-04 | 昆明滇艺非物质文化遗产研发有限公司 | A kind of production method of gambiered Guangdong gauze |
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| CN1177030A (en) * | 1997-09-30 | 1998-03-25 | 桐乡市群合气流纺织厂 | Method for functionally finishing fabric with steeping and rolling process |
| CN2504984Y (en) * | 2001-10-18 | 2002-08-14 | 蒋敏容 | Structure of silk quilt |
| CN101569479A (en) * | 2009-06-12 | 2009-11-04 | 西丰县易兴丝绵厂 | Method for producing negative ion silk quilt |
| CN102746450A (en) * | 2012-07-25 | 2012-10-24 | 浙江理工大学 | Self-adhesive long-acting slow-release essential oil microcapsule and preparation method and application thereof |
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- 2012-11-27 CN CN2012104925888A patent/CN102978961A/en active Pending
Patent Citations (4)
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| CN1177030A (en) * | 1997-09-30 | 1998-03-25 | 桐乡市群合气流纺织厂 | Method for functionally finishing fabric with steeping and rolling process |
| CN2504984Y (en) * | 2001-10-18 | 2002-08-14 | 蒋敏容 | Structure of silk quilt |
| CN101569479A (en) * | 2009-06-12 | 2009-11-04 | 西丰县易兴丝绵厂 | Method for producing negative ion silk quilt |
| CN102746450A (en) * | 2012-07-25 | 2012-10-24 | 浙江理工大学 | Self-adhesive long-acting slow-release essential oil microcapsule and preparation method and application thereof |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3064619A1 (en) * | 2015-02-27 | 2016-09-07 | COSETEX S.n.c. | Method of making a heat-insulating element, and heat-insulating element |
| CN104687905A (en) * | 2015-03-25 | 2015-06-10 | 东华大学 | Production method of anti-aging silk quilt |
| CN104687904A (en) * | 2015-03-25 | 2015-06-10 | 东华大学 | Preparation method for sedative and dormitive silk quilt |
| CN105064046A (en) * | 2015-07-16 | 2015-11-18 | 华南师范大学 | Preparation method and application of fragrant microcapsule compounded organic silicone softener for cotton fabric |
| CN107419430A (en) * | 2015-09-01 | 2017-12-01 | 苏州先蚕丝绸生物科技有限公司 | A kind of feature silk non-woven fabric and its production method |
| CN105361552A (en) * | 2015-11-13 | 2016-03-02 | 周克跃 | Silk-cotton composite quilt and production method thereof |
| CN105361553A (en) * | 2015-11-13 | 2016-03-02 | 周克跃 | Silk quilt and production method thereof |
| CN106377122A (en) * | 2016-08-30 | 2017-02-08 | 江西金铭丝绸有限公司 | Preparation method of silk quilt |
| CN106377122B (en) * | 2016-08-30 | 2018-09-14 | 江西金铭丝绸有限公司 | A kind of preparation method of silk quilt |
| CN107640071A (en) * | 2017-09-01 | 2018-01-30 | 广西桂华丝绸有限公司 | Jasmine tea perfume mulberry silk automobile seat back cushion |
| CN109137484A (en) * | 2018-09-18 | 2019-01-04 | 昆明滇艺非物质文化遗产研发有限公司 | A kind of production method of gambiered Guangdong gauze |
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Application publication date: 20130320 |