CN102772456A - Manufacturing method of sarcandra glabra extraction extractum - Google Patents
Manufacturing method of sarcandra glabra extraction extractum Download PDFInfo
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- CN102772456A CN102772456A CN2012102870306A CN201210287030A CN102772456A CN 102772456 A CN102772456 A CN 102772456A CN 2012102870306 A CN2012102870306 A CN 2012102870306A CN 201210287030 A CN201210287030 A CN 201210287030A CN 102772456 A CN102772456 A CN 102772456A
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- pileae scriptae
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 27
- 238000000605 extraction Methods 0.000 title abstract description 8
- 240000004274 Sarcandra glabra Species 0.000 title abstract 6
- 235000010842 Sarcandra glabra Nutrition 0.000 title abstract 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 41
- 238000010992 reflux Methods 0.000 claims abstract description 38
- 238000009835 boiling Methods 0.000 claims abstract description 33
- 239000006228 supernatant Substances 0.000 claims abstract description 32
- 239000000843 powder Substances 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 230000015556 catabolic process Effects 0.000 claims abstract description 13
- 238000006731 degradation reaction Methods 0.000 claims abstract description 13
- 238000003809 water extraction Methods 0.000 claims abstract description 13
- 238000010790 dilution Methods 0.000 claims abstract description 9
- 239000012895 dilution Substances 0.000 claims abstract description 9
- 239000000243 solution Substances 0.000 claims abstract description 9
- 230000008021 deposition Effects 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 238000005520 cutting process Methods 0.000 claims abstract description 5
- 239000007788 liquid Substances 0.000 claims description 28
- 239000012141 concentrate Substances 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 7
- 230000004087 circulation Effects 0.000 claims description 6
- 230000001476 alcoholic effect Effects 0.000 claims description 2
- 239000000047 product Substances 0.000 abstract description 9
- 239000000470 constituent Substances 0.000 abstract description 2
- 239000003814 drug Substances 0.000 abstract description 2
- 235000013402 health food Nutrition 0.000 abstract description 2
- 239000012530 fluid Substances 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 238000007865 diluting Methods 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 description 5
- 239000006072 paste Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 206010061218 Inflammation Diseases 0.000 description 2
- -1 cyanogen glycoside Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 206010003011 Appendicitis Diseases 0.000 description 1
- 208000008035 Back Pain Diseases 0.000 description 1
- 208000010392 Bone Fractures Diseases 0.000 description 1
- 208000017897 Carcinoma of esophagus Diseases 0.000 description 1
- 206010007882 Cellulitis Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010017076 Fracture Diseases 0.000 description 1
- 208000008930 Low Back Pain Diseases 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 206010030155 Oesophageal carcinoma Diseases 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 206010061902 Pancreatic neoplasm Diseases 0.000 description 1
- 206010035664 Pneumonia Diseases 0.000 description 1
- 241001302750 Psychotria rubra Species 0.000 description 1
- 208000015634 Rectal Neoplasms Diseases 0.000 description 1
- 208000005718 Stomach Neoplasms Diseases 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 229940046011 buccal tablet Drugs 0.000 description 1
- 239000006189 buccal tablet Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 201000005619 esophageal carcinoma Diseases 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 206010017758 gastric cancer Diseases 0.000 description 1
- JMANVNJQNLATNU-UHFFFAOYSA-N glycolonitrile Natural products N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 208000015486 malignant pancreatic neoplasm Diseases 0.000 description 1
- 230000002175 menstrual effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 206010038038 rectal cancer Diseases 0.000 description 1
- 201000001275 rectum cancer Diseases 0.000 description 1
- 201000003068 rheumatic fever Diseases 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 201000011549 stomach cancer Diseases 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 230000008736 traumatic injury Effects 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
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Abstract
The invention discloses a manufacturing method of a sarcandra glabra extraction extractum. The manufacturing method comprises the following steps of: (1) size degradation: cutting off raw material sarcandra glabra, smashing and grinding into coarse powder for standby; (2) water extraction: adding corresponding times volume of water in the ground coarse powder according to the ratio of material to water which is 1:20, and carrying out boiling water reflux extraction; (3) deposition: enabling a boiling water reflux extracting solution to deposit for two hours under the temperature which does not exceed the room temperature by 30 DEG C so as to obtain white paste sticky matter; (4) concentration: carrying out common concentration on the white paste sticky matter and then carrying out vacuum concentration; (5) alcohol dilution: adding ethanol in an object obtained through concentration under a stirring condition according to the ratio of material to water which is 1:4 so as to dilute, and taking a supernatant fluid; and (6) hot reflux: carrying out boiling water reflux treatment on the supernatant fluid obtained through diluting under a room temperature condition. The manufacturing method disclosed by the invention is simple, the product extraction efficiency is high, and the production cost is greatly reduced; and the active constituent of the generated sarcandra glabra extraction extractum is high, the sarcandra glabra extraction extractum can be used for medicine and health food industries, and the sarcandra glabra extraction extractum has an extensive development prospect.
Description
Technical field
The present invention relates to a kind of production method of Herba Pileae Scriptae extract, relate in particular to a kind of production method of Herba Pileae Scriptae extract extractum.
Background technology
Herba Pileae Scriptae is golden Li Lanke perennial evergreen undershrub, is commonly called as MANSHANXIANG, kwan-yin tea, Psychotria rubra (Lour.) Poir. flower, Ramulus Sambuci Williamsii etc.Its form is beautiful, four seasons fragrance, has high medicinal, edible and ornamental value.Herba Pileae Scriptae grows in the dark and damp place of jungle, distributes extensively, and all there is distribution in East China, Central-South, southwest, aboundresources, and composition is various.
The contained chemical constituent of Herba Pileae Scriptae has volatile oil, esters, phenols, tannin, flavone, cyanogen glycoside, coumarin, lactone.The medicinal part herb, acrid in the mouth, hardship, property is flat.Effects such as anti-inflammation, heat-clearing and toxic substances removing, expelling wind and removing dampness, promoting blood circulation and stopping pain, the synthetism of stimulating the menstrual flow are arranged, be used to treat various diseases associated with inflammation, rheumatic arthritis, lumbago and skelalgia, sore swollen toxin pneumonia, appendicitis, acute cellulitis, tumor, traumatic injury, fracture etc.In recent years being used to treat cancer of pancreas, gastric cancer, rectal cancer, hepatocarcinoma, esophageal carcinoma etc. has than remarkable result.Usual amounts 9～30 grams; Suitable amount used externally, bright article are mashed or the dry product levigation, transfer with wine and apply the affected part.Because Herba Pileae Scriptae extract has safety preferably; The Herba Pileae Scriptae product of existing exploitation has dosage forms such as buccal tablet, pin, sheet at present; Herba Pileae Scriptae toothpaste is processed, FUFANG CAOSHANHU HANPIAN as raw material by Chemical Factory of Daily Use; Medicinal, daily or consumable products such as the healthy beverage of Herba Pileae Scriptae have produced good social and economic benefit.
Summary of the invention
One object of the present invention is to provide a kind of production method of Herba Pileae Scriptae extract, and another purpose is to provide a kind of production method of Herba Pileae Scriptae extract extractum.
For this reason, the invention provides a kind of production method of Herba Pileae Scriptae extract extractum, may further comprise the steps:
1) size degradation: the raw material Herba Pileae Scriptae is cut off with even velocity, smash that to wear into coarse powder subsequent use.
2) water extraction: will grind the water of good coarse powder, carry out the boiling water reflux, extract, with the corresponding times of amount of solid-liquid ratio adding of 1:20, boiling water reflux, extract, circulation 3 times, each return time is 2 hours.
3) deposition: with the boiling water reflux extracting liquid room temperature be not more than 30 the degree temperature under staticly settled 2 hours, obtain white paste dope.
4) concentrate: dialogue color shape dope carries out common concentrating earlier its concentration is concentrated into 14～15g/ml, under vacuum equipment, again it is carried out vacuum concentration then its concentration is concentrated into 24g/ml.
5) alcohol is rare: concentrate the object that obtains; Under stirring condition, adding 75% ethanol with the solid-liquid ratio of 1:4 dilutes it; Leave standstill 30min and get its supernatant, in supernatant,, carry out secondary dilution with the ethanol mix homogeneously of 1:4 ratio adding 95%; Leave standstill and let mixed liquor precipitated and separated to solid-liquid well arranged in 24 hours, get supernatant.
6) hot reflux: the rare supernatant that obtains of alcohol is carried out the boiling water reflow treatment at ambient temperature, be back to supernatant and become viscous solution, concentration is to 32g/ml.
Preferably, in the production method of described a kind of Herba Pileae Scriptae extract extractum, described Herba Pileae Scriptae is the plant with dark green Lao Ye of cutting off from 5～10 centimeters overhead.
Preferably, in the production method of described a kind of Herba Pileae Scriptae extract extractum, described size degradation is at the uniform velocity cutting under the speed of 4～6kg/s, and the order number of wearing into coarse powder is between 80～100 orders.
Preferably, in the production method of described a kind of Herba Pileae Scriptae extract extractum, described water extraction is a boiling water reflux, extract, at ambient temperature.
Preferably, in the production method of described a kind of Herba Pileae Scriptae extract extractum, said alcohol is rare to be in mass percent is respectively the alcoholic solution of 4 times of amounts of 75% and 95%, to carry out the double-steeping dilution.
The production method of Herba Pileae Scriptae extract extractum of the present invention, technology is simple, is easy to control, and product extraction rate is high, has greatly reduced the production cost of enterprise.
And become the Herba Pileae Scriptae extract extractum effective ingredient of output high, can be used for medicine, the health food industry has very vast potential for future development.
Description of drawings
Fig. 1 is the production method of Herba Pileae Scriptae extract extractum of the present invention.
The specific embodiment
Below in conjunction with accompanying drawing the present invention is done further detailed description, can implement according to this with reference to the description literal to make those skilled in the art.
The production method of embodiment 1, a kind of Herba Pileae Scriptae extract extractum comprises the steps:
1) size degradation: the raw material Herba Pileae Scriptae is cut off with the speed of 4kg/s equably, smash that to wear into 80 purpose coarse powder subsequent use.At the uniform velocity cut the raw material Herba Pileae Scriptae, purpose is to be to let the shape size of the preliminary size degradation of raw material Herba Pileae Scriptae close, and quality is well-balanced, is more or less the same thereby smash the powder size of wearing into, and helps the carrying out of water extraction process.
2) water extraction: will grind the water of good coarse powder, carry out the boiling water reflux, extract, with the corresponding times of amount of solid-liquid ratio adding of 1:10, boiling water reflux, extract, circulation 3 times, each return time is 2 hours.
3) deposition: the boiling water reflux extracting liquid was staticly settled 2 hours under the temperature of room temperature 20 degree, obtain white paste dope.Room temperature keeps not being more than under the condition of 30 degree and can guarantee that the variation of matter does not at high temperature take place original boiling water reflux extracting liquid, is settled out and produces required effective ingredient.
4) concentrate: dialogue color shape dope carries out common concentrating earlier its concentration is concentrated into 8～9g/ml, under vacuum equipment, again it is carried out vacuum concentration then its concentration is concentrated into 20g/ml.
5) alcohol is rare: concentrate the object that obtains; Under stirring condition, adding 65% ethanol with the solid-liquid ratio of 1:4 dilutes it; Leave standstill 30min and get its supernatant, in supernatant,, carry out secondary dilution with the ethanol mix homogeneously of 1:4 ratio adding 80%; Leave standstill and let mixed liquor precipitated and separated to solid-liquid well arranged in 24 hours, get supernatant.
6) hot reflux: the rare supernatant that obtains of alcohol is carried out the boiling water reflow treatment at ambient temperature, be back to supernatant and become viscous solution, concentration is to 29g/ml.Can improve the concentration of product through hot reflux.
The production method of embodiment 2, a kind of Herba Pileae Scriptae extract extractum comprises the steps:
1) size degradation: the raw material Herba Pileae Scriptae is cut off with the speed of 5kg/s equably, smash that to wear into 90 purpose coarse powder subsequent use.At the uniform velocity cut the raw material Herba Pileae Scriptae, purpose is to be to let the shape size of the preliminary size degradation of raw material Herba Pileae Scriptae close, and quality is well-balanced, is more or less the same thereby smash the powder size of wearing into, and helps the carrying out of water extraction process.
2) water extraction: will grind the water of good coarse powder, carry out the boiling water reflux, extract, with the corresponding times of amount of solid-liquid ratio adding of 1:15, boiling water reflux, extract, circulation 3 times, each return time is 2 hours.
3) deposition: the boiling water reflux extracting liquid was staticly settled 2 hours under the temperature of room temperature 25 degree, obtain white paste dope.Room temperature keeps not being more than under the condition of 30 degree and can guarantee that the variation of matter does not at high temperature take place original boiling water reflux extracting liquid, is settled out and produces required effective ingredient.
4) concentrate: dialogue color shape dope carries out common concentrating earlier its concentration is concentrated into 10～11g/ml, under vacuum equipment, again it is carried out vacuum concentration then its concentration is concentrated into 21g/ml.
5) alcohol is rare: concentrate the object that obtains; Under stirring condition, adding 70% ethanol with the solid-liquid ratio of 1:4 dilutes it; Leave standstill 30min and get its supernatant, in supernatant,, carry out secondary dilution with the ethanol mix homogeneously of 1:4 ratio adding 85%; Leave standstill and let mixed liquor precipitated and separated to solid-liquid well arranged in 24 hours, get supernatant.
6) hot reflux: the rare supernatant that obtains of alcohol is carried out the boiling water reflow treatment at ambient temperature, be back to supernatant and become viscous solution, concentration is to 30g/ml.Can improve the concentration of product through hot reflux.
The production method of embodiment 3, a kind of Herba Pileae Scriptae extract extractum comprises the steps:
1) size degradation: the raw material Herba Pileae Scriptae is cut off with the speed of 6kg/s equably, smash that to wear into 100 purpose coarse powder subsequent use.At the uniform velocity cut the raw material Herba Pileae Scriptae, purpose is to be to let the shape size of the preliminary size degradation of raw material Herba Pileae Scriptae close, and quality is well-balanced, is more or less the same thereby smash the powder size of wearing into, and helps the carrying out of water extraction process.
2) water extraction: will grind the water of good coarse powder, carry out the boiling water reflux, extract, with the corresponding times of amount of solid-liquid ratio adding of 1:20, boiling water reflux, extract, circulation 3 times, each return time is 2 hours.
3) deposition: the boiling water reflux extracting liquid was staticly settled 2 hours under the temperature of room temperature 30 degree, obtain white paste dope.Room temperature keeps not being more than under the condition of 30 degree and can guarantee that the variation of matter does not at high temperature take place original boiling water reflux extracting liquid, is settled out and produces required effective ingredient.
4) concentrate: dialogue color shape dope carries out common concentrating earlier its concentration is concentrated into 12～13g/ml, under vacuum equipment, again it is carried out vacuum concentration then its concentration is concentrated into 22g/ml.
5) alcohol is rare: concentrate the object that obtains; Under stirring condition, adding 75% ethanol with the solid-liquid ratio of 1:4 dilutes it; Leave standstill 30min and get its supernatant, in supernatant,, carry out secondary dilution with the ethanol mix homogeneously of 1:4 ratio adding 90%; Leave standstill and let mixed liquor precipitated and separated to solid-liquid well arranged in 24 hours, get supernatant.
6) hot reflux: the rare supernatant that obtains of alcohol is carried out the boiling water reflow treatment at ambient temperature, be back to supernatant and become viscous solution, concentration is to 31g/ml.Can improve the concentration of product through hot reflux.
The production method of embodiment 4, a kind of Herba Pileae Scriptae extract extractum comprises the steps:
1) size degradation: the raw material Herba Pileae Scriptae is cut off with the speed of 5kg/s equably, smash that to wear into 100 purpose coarse powder subsequent use.At the uniform velocity cut the raw material Herba Pileae Scriptae, purpose is to be to let the shape size of the preliminary size degradation of raw material Herba Pileae Scriptae close, and quality is well-balanced, is more or less the same thereby smash the powder size of wearing into, and helps the carrying out of water extraction process.
2) water extraction: will grind the water of good coarse powder, carry out the boiling water reflux, extract, with the corresponding times of amount of solid-liquid ratio adding of 1:20, boiling water reflux, extract, circulation 3 times, each return time is 2 hours.
3) deposition: the boiling water reflux extracting liquid was staticly settled 2 hours under the temperature of room temperature 25 degree, obtain white paste dope.Room temperature keeps not being more than under the condition of 30 degree and can guarantee that the variation of matter does not at high temperature take place original boiling water reflux extracting liquid, is settled out and produces required effective ingredient.
4) concentrate: dialogue color shape dope carries out common concentrating earlier its concentration is concentrated into 14～15g/ml, under vacuum equipment, again it is carried out vacuum concentration then its concentration is concentrated into 24g/ml.
5) alcohol is rare: concentrate the object that obtains; Under stirring condition, adding 75% ethanol with the solid-liquid ratio of 1:4 dilutes it; Leave standstill 30min and get its supernatant, in supernatant,, carry out secondary dilution with the ethanol mix homogeneously of 1:4 ratio adding 95%; Leave standstill and let mixed liquor precipitated and separated to solid-liquid well arranged in 24 hours, get supernatant.
6) hot reflux: the rare supernatant that obtains of alcohol is carried out the boiling water reflow treatment at ambient temperature, be back to supernatant and become viscous solution, concentration is to 32g/ml.Can improve the concentration of product through hot reflux.
Although embodiment of the present invention are open as above; But it is not restricted to listed utilization in description and the embodiment; It can be applied to various suitable the field of the invention fully, for being familiar with those skilled in the art, can easily realize other modification; Therefore under the general concept that does not deviate from claim and equivalency range and limited, the legend that the present invention is not limited to specific details and illustrates here and describe.
Claims (5)
1. the production method of a Herba Pileae Scriptae extract extractum is characterized in that, may further comprise the steps:
1) size degradation: the raw material Herba Pileae Scriptae is cut off with even velocity, smash that to wear into coarse powder subsequent use;
2) water extraction: will grind the water of good coarse powder, carry out the boiling water reflux, extract, with the corresponding times of amount of solid-liquid ratio adding of 1:20, boiling water reflux, extract, circulation 3 times, each return time is 2 hours;
3) deposition: with the boiling water reflux extracting liquid room temperature be not more than 30 the degree temperature under staticly settled 2 hours, obtain white paste dope;
4) concentrate: dialogue color shape dope carries out common concentrating earlier its concentration is concentrated into 14～15g/ml, under vacuum equipment, again it is carried out vacuum concentration then its concentration is concentrated into 24g/ml;
5) alcohol is rare: concentrate the object that obtains; Under stirring condition, adding 75% ethanol with the solid-liquid ratio of 1:4 dilutes it; Leave standstill 30min and get its supernatant, in supernatant,, carry out secondary dilution with the ethanol mix homogeneously of 1:4 ratio adding 95%; Leave standstill and let mixed liquor precipitated and separated to solid-liquid well arranged in 24 hours, get supernatant;
6) hot reflux: the rare supernatant that obtains of alcohol is carried out the boiling water reflow treatment at ambient temperature, be back to supernatant and become viscous solution, concentration is to 32g/ml.
2. the extractum production method of a kind of Herba Pileae Scriptae extract as claimed in claim 1 is characterized in that, described Herba Pileae Scriptae is the plant with dark green Lao Ye of cutting off from 5～10 centimeters overhead.
3. the production method of a kind of Herba Pileae Scriptae extract extractum as claimed in claim 1 is characterized in that, described size degradation is at the uniform velocity cutting under the speed of 4～6kg/s, and the order number of wearing into coarse powder is between 80～100 orders.
4. the production method of a kind of Herba Pileae Scriptae extract extractum as claimed in claim 1 is characterized in that, described water extraction is a boiling water reflux, extract, at ambient temperature.
5. the production method of a kind of Herba Pileae Scriptae extract extractum as claimed in claim 1 is characterized in that, said alcohol is rare to be in mass percent is respectively the alcoholic solution of 4 times of amounts of 75% and 95%, to carry out the double-steeping dilution.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210287030.6A CN102772456B (en) | 2012-08-13 | 2012-08-13 | Manufacturing method of sarcandra glabra extraction extractum |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210287030.6A CN102772456B (en) | 2012-08-13 | 2012-08-13 | Manufacturing method of sarcandra glabra extraction extractum |
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| CN102772456B CN102772456B (en) | 2014-06-11 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103638123A (en) * | 2013-11-26 | 2014-03-19 | 宋爱民 | External traditional Chinese medicine preparation for treating lumbar myofascitis |
| CN106635421A (en) * | 2016-12-09 | 2017-05-10 | 广西壮族自治区药用植物园 | Preparation method of glabrous sarcandra herb volatile oil and prevention and treatment effect of glabrous sarcandra herb volatile oil on panax notoginseng gray mold |
| CN118286278A (en) * | 2024-06-05 | 2024-07-05 | 江西草珊瑚口腔护理用品有限公司 | A method for preparing herba Pileae Scriptae extract by instant pressurizing process |
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|---|---|---|---|---|
| CN1220148A (en) * | 1997-12-16 | 1999-06-23 | 李光喜 | Method for preparing sarcandra oral ointment |
| CN1277852A (en) * | 2000-06-14 | 2000-12-27 | 邓开仲 | Pharmaceutical for preventing and treating senile dementia and depression, and its prepn. process |
| CN101574381A (en) * | 2009-02-02 | 2009-11-11 | 江中药业股份有限公司 | Extractive of effective part of chloranthus glaber and preparation method thereof |
| CN101721334A (en) * | 2008-11-03 | 2010-06-09 | 杨来香 | Sunscreen cream containing sarcandra glabra fluid extract |
| CN101856489A (en) * | 2010-05-28 | 2010-10-13 | 西南大学 | Swine health granules and preparation process thereof |
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2012
- 2012-08-13 CN CN201210287030.6A patent/CN102772456B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1220148A (en) * | 1997-12-16 | 1999-06-23 | 李光喜 | Method for preparing sarcandra oral ointment |
| CN1277852A (en) * | 2000-06-14 | 2000-12-27 | 邓开仲 | Pharmaceutical for preventing and treating senile dementia and depression, and its prepn. process |
| CN101721334A (en) * | 2008-11-03 | 2010-06-09 | 杨来香 | Sunscreen cream containing sarcandra glabra fluid extract |
| CN101574381A (en) * | 2009-02-02 | 2009-11-11 | 江中药业股份有限公司 | Extractive of effective part of chloranthus glaber and preparation method thereof |
| CN101856489A (en) * | 2010-05-28 | 2010-10-13 | 西南大学 | Swine health granules and preparation process thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103638123A (en) * | 2013-11-26 | 2014-03-19 | 宋爱民 | External traditional Chinese medicine preparation for treating lumbar myofascitis |
| CN103638123B (en) * | 2013-11-26 | 2016-04-13 | 宋爱民 | The Chinese medicine for outer use for the treatment of lumbar muscle fasciitis |
| CN106635421A (en) * | 2016-12-09 | 2017-05-10 | 广西壮族自治区药用植物园 | Preparation method of glabrous sarcandra herb volatile oil and prevention and treatment effect of glabrous sarcandra herb volatile oil on panax notoginseng gray mold |
| CN118286278A (en) * | 2024-06-05 | 2024-07-05 | 江西草珊瑚口腔护理用品有限公司 | A method for preparing herba Pileae Scriptae extract by instant pressurizing process |
| CN118286278B (en) * | 2024-06-05 | 2024-09-17 | 江西草珊瑚口腔护理用品有限公司 | A method for preparing herba Pileae Scriptae extract by instant pressurizing process |
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| CN102772456B (en) | 2014-06-11 |
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