CN101812756A - Regenerated cellulose fiber-real silk jacquard fabric for home textiles and preparation method thereof - Google Patents
Regenerated cellulose fiber-real silk jacquard fabric for home textiles and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a regenerated cellulose fiber-real silk jacquard fabric for home textiles and a preparation method thereof. The regenerated cellulose fiber-real silk jacquard fabric is woven by adopting regenerated cellulose fiber long yarns as warp yarns and real silk yarns as weft yarns in a jacquard interweaving mode. Because the regenerated cellulose fiber long yarns per se have good handfeel and soft gloss, the regenerated cellulose fiber-real silk jacquard fabric formed by interweaving the regenerated cellulose fiber long yarns and the real silk yarns has smooth handfeel comparable with that of a full real silk jacquard fabric; the regenerated cellulose fiber-real silk jacquard fabric is a jacquard fabric with different yarn-dyed effects by a later-bath yarn dyeing method; and compared with separate dyeing, the preparation method can effectively save the cost.
Description
Technical field
The present invention relates to a kind of regenerated cellulose fiber-real silk jacquard fabric that family spins and preparation method thereof that is used for, the especially a kind of jacquard fabric that forms by regenerated celulose fibre yarn and real silk braiding that is used for that family spins and the dyeing step of this jacquard fabric.
Background technology
In present stage, the fabric variety of bedding is single relatively, and mainly with silk like, conventional lining such as cotton class is main, comprises that look knits real silk jacquard fabrics, cotton jacquard fabric and silk flosssilk wadding jacquard fabric, and this three kind fabric has the following disadvantages respectively:
(1) described look is knitted the real silk jacquard fabrics, though feel is soft and smooth, drapability is good, gloss is soft and graceful, highlights class, but the price comparison costliness, and arrange difficulty, collude silk easily, service life is short, so occupation rate of market is less than normal, simultaneously, traditional look is knitted the real silk jacquard fabrics must knit effect by the method realization look of jacquard weave behind the first yarn dyeing, and it is bigger to consume energy, and efficient is on the low side; (2) described conventional cotton class jacquard fabric, feel is hard partially, lacks reflecting feel and the elegant sense of dangling, and after the arrangement dyeing of back, color is more single; (3) the silk flosssilk wadding jacquard fabric of described employing cotton yarn and silk interlaced formation jacquard fabric, though this silk flosssilk wadding jacquard fabric price decreases than authentic silk face fabric, the flexibility of its drapability and feel is all not as good as authentic silk jacquard fabric; Simultaneously, knit effect though traditional silk flosssilk wadding jacquard fabric can be realized dyeing by dyeing, the impurity processing method in the cotton yarn produces damage to real silk, and the cotton face fabric feel is stiff, be not as soft and smooth and glossy as the real silk jacquard fabrics, reduces class.
Continuous development along with society, and the improving constantly of human living standard, the requirement that people spin the bed necessaries lining for family is also harsh day by day, be generally: soft and smooth as feel such as the real silk, arrange easily, be easy to real silk, cost is lower than authentic silk face fabric, the flower type has enjoying value, and the cost performance height has environmental protection and energy saving simultaneously concurrently.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, a kind of regenerated cellulose fiber-real silk jacquard fabric that family is spun that is used for is provided, this jacquard fabric warp thread adopts good hygroscopicity, do strong and wet all superior by force than cotton fiber, the soft and smooth long yarn of regenerated celulose fibre as feel such as the real silk, weft yarn then adopts real silk yarn, the long yarn of aforementioned regenerated celulose fibre and real silk yarn interweaved according to the jacquard weave interleaving mode can form regenerated cellulose of the present invention and real silk jacquard fabric, it is not only as soft and smooth as the real silk, and the distinctive gloss of the long yarn of regenerated celulose fibre shines mutually with real silk, be that the silk flosssilk wadding jacquard fabric is incomparable, simultaneously its drapability can match in excellence or beauty with real silk, and arrange easier than authentic silk face fabric.In addition, the application of the long yarn of regenerated celulose fibre meets the trend of energy savings, and therefore, regenerated cellulose fiber-real silk jacquard fabric flower type of the present invention is beautiful, and lining is arranged easily, and cost performance height, cost are lower than authentic silk face fabric, environmental protection and energy saving simultaneously.
For realizing above technical purpose, the present invention will take following technical scheme:
A kind ofly be used for the regenerated cellulose fiber-real silk jacquard fabric that family is spun, the long yarn of regenerated celulose fibre that the warp thread of this regenerated cellulose-real silk jacquard fabric is formed by weaving for the regenerated celulose fibre long filament, the real silk yarn that weft yarn then is formed by weaving for cocoon fiber, long yarn of described regenerated celulose fibre and real silk yarn weave to form regenerated cellulose fiber-real silk jacquard fabric according to the jacquard fabric interleaving mode.
Described regenerated celulose fibre long filament is selected from day silk Tencel, a model Modal, crotalaria sp, numb Sai Er, bamboo fibre or Lay bamboo.
Another technical purpose of the present invention provides a kind of preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins, may further comprise the steps: will as the long yarn of the regenerated celulose fibre of warp thread and as the real silk yarn of weft yarn according to the jacquard weave interleaving mode knit regenerated cellulose-real silk jacquard fabric grey cloth, through after the preliminary treatment, carry out dyeing, this dyeing adopts direct dyes and the neutral ACID DYES of bathing respectively the real silk yarn in regenerated cellulose-real silk jacquard fabric and the long yarn of regenerated celulose fibre to be carried out a bath look and knit dyeing, simultaneously, add dyeing auxiliaries in dye liquor, described dyeing auxiliaries comprises glauber salt, levelling agent and bleeding agent; When one bath look is knitted dyeing; bath raio is 1: 15~1: 30; dye liquor is progressively heated to 90 ℃~95 ℃ from 60 ℃ of initial temperatures; dye liquor pH value is 6~7; dyeing duration 60~70min, after a bath look is knitted the dyeing end, add the soda ash fixation earlier; then adopt industry to soap, adopt acetic acid neutralizing acid basicity to get final product at last to finalize the design.
According to above technical scheme, can realize following beneficial effect:
The present invention adopt as the long yarn of the regenerated celulose fibre of warp thread and as the real silk yarn of weft yarn according to the braiding of jacquard fabric interleaving mode with the acquisition regenerated cellulose fiber-real silk jacquard fabric, therefore, because the long yarn of regenerated celulose fibre itself possesses good hand feeling and soft gloss, the regenerated cellulose fiber-real silk jacquard fabric that interweaves and form with real silk yarn, its soft and smooth feel can compare favourably with authentic silk jacquard fabric, and this regenerated cellulose fiber-real silk jacquard fabric can be knitted effect by later stage dyeing realization look.
The specific embodiment
To technical scheme of the present invention be disclosed without limitation by embodiment below.
Of the present inventionly be used for the regenerated cellulose fiber-real silk jacquard fabric that family is spun, the long yarn of regenerated celulose fibre that the warp thread of this regenerated cellulose-real silk jacquard fabric is formed by weaving for the regenerated celulose fibre long filament, the real silk yarn that weft yarn then is formed by weaving for cocoon fiber, long yarn of described regenerated celulose fibre and real silk yarn weave to form regenerated cellulose-real silk jacquard fabric according to the jacquard fabric interleaving mode, this regenerated celulose fibre long filament is selected from a day silk Tencel, model Modal, crotalaria sp, fiber crops Sai Er, bamboo fibre or Lay bamboo are knitted described regenerated cellulose-real silk jacquard fabric then by later stage dyeing realization look.
In general, the preparation method of regenerated cellulose-real silk jacquard fabric may further comprise the steps: the come unstuck processing → washing → of grey cloth → debatching, margin to seam → kiering → washing → pre-setting clot → alkaline oxygen bath processing → washing → enzyme is bathed look and is knitted dyeing → soft treatment → typing → preshrunk → finished product.
Specifically, earlier will as the long yarn of the regenerated celulose fibre of warp thread and as the real silk yarn of weft yarn according to the jacquard weave interleaving mode knit behind the regenerated cellulose fiber-real silk jacquard fabric grey cloth, elder generation's debatching, margin to seam, after then carrying out kiering, washing, adopt setting machine to carry out the pre-setting clot, to eliminate the internal stress of this regenerated cellulose fiber-real silk jacquard fabric grey cloth, then adopting the alkaline oxygen bath treatment formulations to carry out alkaline oxygen bath handles, carry out then enzyme come unstuck handle after, enter one and bathe look and knit dyeing.
Alkaline oxygen bath is handled, and used alkaline oxygen bath treatment formulations is: soda ash 10~12g/L, hydrogen peroxide (perhaps 30% mass percent) 8~10g/L, bleeding agent (0.2~0.4%o.w.f neopelex, 0.35~0.55%o.w.f XP-70; Alkaline oxygen bath treatment conditions: 9.5~10,98 ℃~100 ℃ of pH values, time: 20min; The acting as of each component in the alkaline oxygen bath treatment formulations: the effect of soda ash is to make cellulose expanded, improves the fiber compliance, and the effect of hydrogen peroxide is long yarn of bleach regenerator cellulose fibre and real silk yarn; Bleeding agent, consider to adopt anionic bleeding agent and nonionic penetrant compound for cellulose and protein interwoven fabric, the present invention can adopt neopelex and XP 1 (alkylol polyoxyethylene ether series nonionic penetrant, the degree of depth of digitized representation oxygen baseization) composite; Main purpose is to make alkali lye and hydrogen peroxide effectively enter fibrous inside, so that fabric obtains capillary effect and whiteness preferably, lauryl sodium sulfate can be used as hydrogen peroxide stabilizer simultaneously.
The enzyme processing of coming unstuck adopts 3~7%o.w.f acid protease to carry out, and the enzyme treatment conditions of coming unstuck: the pH value is 4~6, bath raio 1: 30~1: 50; Temperature: 45 ℃~50 ℃, processing time 60~65min; It act as: carry out the enzyme processing of coming unstuck by the silk gum to real silk yarn in the lining, improve the real silk dye-uptake.
For dyeing, its dyeing condition and technical recipe are as follows:
Process conditions: temperature requirement dyes 60 ℃ of temperature for the beginning, progressively be warming up to 90 ℃~95 ℃, should not adopt the dyeing technique that boils, otherwise the real silk yarn surface will tarnish, the pH value is controlled at 6~7, regulates pH value, dyeing time 60~70min with acetic acid and ammoniacal liquor, glauber salt notices that as accelerant gradation adds bath raio: 1: 15~1: 30;
Dyeing recipe: direct dyes (can select vapour crust C type dye for use), dyeing auxiliaries (comprising bleeding agent, glauber salt and levelling agent), neutral ACID DYES and the industrial soap of bathing;
Dyestuff composition: direct dyes: look dyes the long yarn of regenerated celulose fibre; The neutral ACID DYES of bathing: look dyeing silk yarn; Long yarn of regenerated celulose fibre and real silk yarn interweave and recently control in the depth that described direct dyes and neutral addition of bathing ACID DYES are knitted according to the long yarn of regenerated celulose fibre and real silk yarn look respectively and the regenerated cellulose-real silk jacquard fabric, the long yarn of the regenerated celulose fibre of described regenerated cellulose-real silk jacquard fabric and real silk yarn interweave than being 90: 10~50: 50, the long yarn-dyed light direct dyes consumption 0.05~0.12o.w.f of regenerated celulose fibre, real silk yarn dyes the neutral ACID DYES 0.05~1o.w.f that bathes of light color, dark neutral bath acid dye consumption was 1~3o.w.f during dark direct dyes consumption 0.12~0.5o.w.f during regenerated celulose fibre is yarn-dyed, real silk yarn dyed; O.w.f is to be the unit of benchmark with respect to lining, and the consumption of dyestuff calculates in the lining warp thread and weft yarn component ratio because of the different differences to some extent of lining specification according to lining weight.
Soda ash: play tint retention, dying light fabric consumption is 7~8g/L, and the deep-colour fabric consumption is 8~24g/L in dying;
Glauber salt: play and short dye effect, electronegative in dye liquor because of direct dyes, can not add too soon too much, otherwise specking is taken an advanced study into very much in the colouring of local dyestuff; Should fully melt before using, just can add dye bath after filtering, more need the limit to stir the dye liquor limit and add.When dying light fabric, the addition of glauber salt is 55~56g/L, in dying during deep-colour fabric, the addition of glauber salt is 56~80g/L, and in addition, glauber salt should add in dyeing course in batches, in dyeing course, play the short effect of dying, direct dyes colourings was very fast when temperature was lower, and the glauber salt that add this moment is urged to dye to the long yarn of regenerated celulose fibre; Along with the rising of temperature, the colouring of neutral bath ACID DYES is very fast, and the glauber salt that add this moment is urged to dye to real silk yarn;
Levelling agent: direct dyes are sorptive big to cellulose fibre, dyeing speed is fast, therefore and easily form specking, the effect of levelling agent is the colouring speed of dyestuff that slows down, the non-ionic surface active agent of the most frequently used alkyl polyoxyethylene ether (being peregal 0, levelling agent 0 or leveler 102), addition is 2~3g/L in the dye liquor;
Bleeding agent: under the neutral dye liquor condition, adopt anionic bleeding agent neopelex, have effect wetting, that permeate and wash, can remove impurity and oil stain, have advantages of higher stability, reduce the surface tension of dye liquor, make dye liquor to the speeding up of fiber pervasion, thereby help the carrying out of whole dyeing, the use of bleeding agent helps to control the lining dyeing quality in the dyeing, improve the dyefastness of lining, typical concentrations is 0.2~0.75o.w.f;
Industrial soap: improve fabric color fastness and gorgeous degree, washing is carried out without the dyestuff of fixation, used dyeing auxiliaries etc. in the lining surface under the condition of closely boiling.
In the technical scheme for above-mentioned record, used technical term bleeding agent, bath raio, the o.w.f of unit and the g/L meaning are respectively:
Bleeding agent: be a class can make liquid rapidly and uniformly penetrating to the surfactant of certain material inside, generally in dyeing and finishing pre-treatment process and dye process, use.
Bath raio: contaminate fabric and dye liquor weight ratio.
Assistant concentration o.w.f (On weight the fabric): concentration is benchmark with the fabric weight in the dyeing and finishing technology, relatively the percentage of fabric.
Auxiliary agent unit: g/L refers to every liter of adjuvant used quality of dye liquor.
Embodiment 1
The door width of cloth: 108 inches Tencel LF 60S * Silk 22D/2/173 * 200; Formation is knitted effect through the pale yellow filling satin look of light gray weft yarn;
The yarn that sky silk Tencel is spun into as warp thread with as the real silk yarn of weft yarn according to the jacquard weave interleaving mode knit behind day silk-real silk jacquard fabric grey cloth, elder generation's debatching, margin to seam, after then carrying out kiering, washing, adopt setting machine to carry out the pre-setting clot, to eliminate the internal stress of this day silk-real silk jacquard fabric grey cloth, then adopt the alkaline oxygen bath treatment formulations to carry out alkaline oxygen bath and handle, carry out then enzyme come unstuck handle after, enter one and bathe look and knit dyeing.
(1) alkaline oxygen bath is handled
Alkaline oxygen bath treatment formulations: soda ash 10g/L, hydrogen peroxide 8g/L, 0.2%o.w.f neopelex, 0.35%o.w.fXP-70;
The alkaline oxygen bath treatment conditions: adopt ammoniacal liquor or vinegar acid for adjusting pH value, and make that the pH value of alkaline oxygen bath treatment fluid is 9.5~10, temperature is controlled at about 98.5 ℃ in the processing procedure, and handling duration is about 20min.
(2) the enzyme processing of coming unstuck
The enzyme treatment formulations of coming unstuck: 3%o.w.f acid protease;
The enzyme treatment conditions of coming unstuck: the pH value is 4~6, bath raio 1: 30; Temperature is controlled at about 45 ℃ in the processing procedure, and the processing time is about 60min.
(3) dyeing
Dyeing recipe
Direct dyes vapour crust C type dye 0.05o.w.f
The neutral ACID DYES 2.5o.w.f that bathes
Soda ash 7.2g/L
Neopelex 0.23o.w.f
Glauber salt 55g/L
Levelling agent 2.3g/L
Industrial soap 5g/L
The dyeing condition: bath raio is about 1: 15, temperature requirement dyes 60 ℃ of temperature for the beginning, in body lotion, add direct dyes vapour crust C type dye and the neutral ACID DYES of bathing, progressively heat up, about dyeing 10min, add the accelerant glauber salt in batches and handle about 20min, add soda ash again and carry out fixation treatment 30min, then adopt industrial soap lye to boil and wash, adopt acetic acid neutralizing acid basicity, can go out cloth behind the cold water washing.In the whole dyeing course, regulate the pH value, make the pH value be controlled at 6~7 with acetic acid and ammoniacal liquor.
Embodiment 2
The door width of cloth: 108 inches Lyocell Bamboo 60S * Silk 22D/3/173 * 180; Warp thread adopts the Lay bamboo fibre, and weft yarn adopts real silk; Formation is knitted effect through sky blue weft yarn plum filling satin look; Because of the Lay bamboo fibre not only possesses day the good characteristic of silk, the process environmental protection more possessed the natural antibacterial effect of bamboo pulp, so this embodiment is a fabrics and fibers;
Dyeing recipe:
Direct dyes vapour crust C type dye 0.12o.w.f
The neutral ACID DYES 1.0o.w.f that bathes
Soda ash 16g/L
Neopelex 0.4o.w.f
Glauber salt 66g/L
Levelling agent 2.0g/L
Industrial soap 5g/L
Surplus is a water
The dyeing condition: bath raio is about 1: 20, temperature requirement dyes 60 ℃ of temperature for the beginning, in body lotion, add direct dyes vapour crust C type dye and the neutral ACID DYES of bathing, progressively heat up, about dyeing 10min, add the accelerant glauber salt in batches and handle about 20min, add soda ash again and carry out fixation treatment 30min, then adopt industrial soap lye to boil and wash, adopt acetic acid neutralizing acid basicity, can go out cloth behind the cold water washing.In the whole dyeing course, regulate the pH value, make the pH value be controlled at 6~7 with acetic acid and ammoniacal liquor.
Embodiment 3
The door width of cloth: 108 inches Silk 22D/3 * air-conditioning viscose glue 40S/200 * 95; Formation is knitted effect through dark red grey weft yarn light red filling satin look; Warp thread adopts real silk, and weft yarn adopts the air-conditioning spun rayon to form jacquard effect; Annotate: the air-conditioning viscose glue is the functional form regenerated celulose fibre that possesses temperature adjustment function;
Dyeing recipe:
Direct dyes vapour crust C type dye 0.15o.w.f
The neutral ACID DYES 3.0o.w.f that bathes
Soda ash 24g/L
Neopelex 0.4o.w.f
Glauber salt 80g/L
Levelling agent 3.0g/L
Industrial soap 5g/L
Surplus is a water
The dyeing condition:
Bath raio is about 1: 30, temperature requirement dyes 60 ℃ of temperature for the beginning, in body lotion, add direct dyes vapour crust C type dye and the neutral ACID DYES of bathing, progressively heat up, about dyeing 10min, add the accelerant glauber salt in batches and handle about 20min, add soda ash again and carry out fixation treatment 30min, then adopt industrial soap lye to boil and wash, adopt acetic acid neutralizing acid basicity, can go out cloth behind the cold water washing.In the whole dyeing course, regulate the pH value, make the pH value be controlled at 6~7 with acetic acid and ammoniacal liquor.
Claims (10)
1. one kind is used for the regenerated cellulose fiber-real silk jacquard fabric that family is spun, it is characterized in that, the long yarn of regenerated celulose fibre that the warp thread of this regenerated cellulose-real silk jacquard fabric is formed by weaving for the regenerated celulose fibre long filament, after weaving according to the jacquard fabric interleaving mode, the real silk yarn that weft yarn then is formed by weaving for cocoon fiber, long yarn of described regenerated celulose fibre and real silk yarn knit dyeing to form regenerated cellulose-real silk jacquard fabric through look.
2. be used for the regenerated cellulose fiber-real silk jacquard fabric that family is spun according to claim 1 is described, it is characterized in that, described regenerated celulose fibre long filament is selected from day silk Tencel, a model Modal, crotalaria sp, numb Sai Er, bamboo fibre or Lay bamboo.
3. one kind based on the described preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins of claim 1, it is characterized in that, may further comprise the steps: will as the long yarn of the regenerated celulose fibre of warp thread and as the real silk yarn of weft yarn according to the jacquard weave interleaving mode knit regenerated cellulose-real silk jacquard fabric grey cloth, through after the preliminary treatment, carry out dyeing, this dyeing adopts direct dyes and the neutral ACID DYES of bathing respectively the real silk yarn in regenerated cellulose-real silk jacquard fabric and the long yarn of regenerated celulose fibre to be carried out a bath look and knit dyeing, simultaneously, add dyeing auxiliaries in dye liquor, described dyeing auxiliaries comprises glauber salt, levelling agent and bleeding agent; When one bath look is knitted dyeing; bath raio is 1: 15~1: 30; dye liquor is progressively heated to 90 ℃~95 ℃ from 60 ℃ of initial temperatures; dye liquor pH value is 6~7; dyeing duration 60~70min, after a bath look is knitted the dyeing end, add the soda ash fixation earlier; then adopt industry to soap, adopt acetic acid neutralizing acid basicity to get final product at last to finalize the design.
4. the preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins according to claim 3, it is characterized in that, long yarn of regenerated celulose fibre and real silk yarn interweave and recently control in the depth that described direct dyes and neutral addition of bathing ACID DYES are knitted according to the long yarn of regenerated celulose fibre and real silk yarn look respectively and the regenerated cellulose-real silk jacquard fabric, the long yarn of regenerated celulose fibre and real silk yarn interweave than being 90: 10~50: 50 in described regenerated cellulose-real silk jacquard fabric, when the long yarn of hypochromatic regenerated celulose fibre, neutral concentration of bathing ACID DYES is 0.05~1o.w.f, when the long yarn of hyperchromatic regenerated celulose fibre, neutral concentration of bathing ACID DYES then is 1~3o.w.f; When hypochromatic real silk yarn, the concentration of direct dyes is 0.05~0.12o.w.f, and when hyperchromatic real silk yarn, direct dyes concentration is 0.12~0.5o.w.f.
5. the preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins according to claim 3, it is characterized in that, the addition of described glauber salt and soda ash is controlled according to the depth that regenerated cellulose-the real silk jacquard fabric look is knitted, the addition of glauber salt and soda ash corresponds to 55~56g and 7~8g respectively in the regenerated cellulose-real silk jacquard fabric knitted for light color, every liter of dye liquor; The addition of glauber salt and soda ash corresponds to 56~80g and 8~24g respectively in the regenerated cellulose-real silk jacquard fabric knitted for dark color, every liter of dye liquor.
6. the preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins according to claim 3, it is characterized in that, described levelling agent is non-ionic surface active agent peregal 0, levelling agent 0 or the leveler 102 of alkyl polyoxyethylene ether, and the addition of levelling agent is 2~3g in every liter of dye liquor.
7. the preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins according to claim 3, it is characterized in that, described bleeding agent is an anionic bleeding agent neopelex, its addition is 0.2~0.75o.w.f, o.w.f represents that concentration is benchmark with the fabric weight in the dyeing and finishing technology, relatively the percentage of fabric.
8. the preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins according to claim 3 is characterized in that, in the dyeing course, adopts acetic acid and ammoniacal liquor to regulate the pH value of dye liquor.
9. the preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins according to claim 3 is characterized in that, before carrying out dyeing, also comprises following regenerated cellulose fiber-real silk jacquard fabric grey cloth pre-treatment step:
(1) pre-setting is handled and is adopted setting machine that regenerated cellulose fiber-real silk jacquard fabric is carried out the pre-setting processing, to eliminate the internal stress of this regenerated cellulose fiber-real silk jacquard fabric grey cloth;
(2) alkaline oxygen bath is handled and is adopted the alkaline oxygen bath treatment formulations that regenerated cellulose fiber-real silk jacquard fabric is carried out the alkaline oxygen bath processing, this alkaline oxygen bath treatment formulations comprises soda ash, hydrogen peroxide and bleeding agent, when carrying out the alkaline oxygen bath processing, the pH value is 9.5~10,98 ℃~100 ℃ of temperature, handling duration 20min;
(3) enzyme comes unstuck and handle to adopt acid protease that the silk gum of real silk yarn in the regenerated cellulose fiber-real silk jacquard fabric is carried out enzyme processings of coming unstuck, and when enzyme came unstuck processing, the pH value was 4~6, bath raio 1: 30~1: 50; 45 ℃~50 ℃ of temperature, handling duration 60~65min.
10. the preparation method who is used for the regenerated cellulose fiber-real silk jacquard fabric that family spins according to claim 9, it is characterized in that, in the alkaline oxygen bath treatment formulations, the concentration of soda ash is 10-12g/L, the concentration of hydrogen peroxide is 8-10g/L, bleeding agent adopts composite that sodium dodecyl benzenylsulfonate and XP-70 form, and sodium dodecyl benzenylsulfonate and XP-70 addition are respectively 0.2~0.4%o.w.f and 0.35~0.55%o.w.f; In addition, carry out enzyme and come unstuck when handling, the acidic protein enzyme dosage is 3~7%o.w.f.
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