CN100399211C - Device and method for eliminating X-ray lensless Fourier transform holographic zero-order wave - Google Patents

Device and method for eliminating X-ray lensless Fourier transform holographic zero-order wave Download PDF

Info

Publication number
CN100399211C
CN100399211C CNB2004100527834A CN200410052783A CN100399211C CN 100399211 C CN100399211 C CN 100399211C CN B2004100527834 A CNB2004100527834 A CN B2004100527834A CN 200410052783 A CN200410052783 A CN 200410052783A CN 100399211 C CN100399211 C CN 100399211C
Authority
CN
China
Prior art keywords
fourier transform
ray
phase shifter
lensless fourier
transform hologram
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB2004100527834A
Other languages
Chinese (zh)
Other versions
CN1588238A (en
Inventor
陈建文
高鸿奕
何红
李儒新
徐至展
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Institute of Optics and Fine Mechanics of CAS
Original Assignee
Shanghai Institute of Optics and Fine Mechanics of CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Institute of Optics and Fine Mechanics of CAS filed Critical Shanghai Institute of Optics and Fine Mechanics of CAS
Priority to CNB2004100527834A priority Critical patent/CN100399211C/en
Publication of CN1588238A publication Critical patent/CN1588238A/en
Application granted granted Critical
Publication of CN100399211C publication Critical patent/CN100399211C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Holo Graphy (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)

Abstract

An apparatus and method for eliminating X-ray lensless Fourier transform holographic zero order wave, the apparatus is composed of: the detector comprises a wave zone plate, a pinhole diaphragm and a detector which are sequentially arranged in the advancing direction of X rays of an X-ray source, the output end of the detector is connected with a computer, a pinhole of the pinhole diaphragm is positioned at the focus of the wave zone plate, an object to be detected is positioned in another hole which is on the same plane as the pinhole of the pinhole diaphragm and is close to the pinhole, a phase shifter is arranged behind the object to be detected, and the phase shift of the phase shifter is 2k pi. The method for eliminating X-ray lens-free Fourier transform hologram zero-order waves by using the device comprises the following steps: shooting an X-ray lens-free Fourier transform hologram without inserting a phase shifter in an object beam and storing the X-ray lens-free Fourier transform hologram in a computer; inserting a phase shifter into the object beam, and shooting an X-ray lens-free Fourier transform hologram and storing the X-ray lens-free Fourier transform hologram in the computer; the computer subtracts the intensities of light reproduced by the two holograms.

Description

Eliminate the apparatus and method of the holographic zero order wave of X ray lensless fourier transform
Technical field
The present invention is relevant with the X ray holography, particularly a kind of apparatus and method of eliminating the holographic zero order wave of X ray lensless fourier transform, and this holography has been widely used in biomedicine.
Background technology
As far back as nineteen fifty-two, Balz just is introduced into the X ray field to the notion of holography, the effort through several years, and the X ray holography has obtained many progress.The seventies, owing to lack x-ray source, the necessary optical element of shortage and the high-resolution recording medium of high brightness, and have many problems on the formation method, cause this field progress unsatisfactory.In recent years, because the appearance of synchrotron radiation source, this formation method extensive concern of getting back.Referring to technology: Chen Jianwen formerly, Xu Zhizhan, Zhu Peiping, the king Zhijiang River, X ray holography, Proceedings in Physics, nineteen ninety-five, 15 volumes, the 2nd phase, 125~147.
The X ray holography has two kinds of recording methods at present: coaxial recording and lensless fourier transform holographic recording.We are interested to be the holography of X ray lensless fourier transform.Fourier transform hologram is meant the Fourier transform spectrum that has write down sample, i.e. the hologram of the spatial frequency spectrum of sample.When lensless Fourier transform hologram is meant with reference to point source and sample at grade, just can record the hologram of the accurate Fourier transform spectrum of sample, as shown in Figure 1.
One relevant parallel plane X ray 1 irradiation one X ray zone plate 2, this zone plate is except that the zero order wave of a part of transmission, also produce one and assemble diffracted wave, place a pin hole at its focus place, by the X ray of aperture outgoing as the reference ripple, the zero order wave of transmission irradiation testing sample 3, sample 3 scattering waves are as the thing bundle, interfere when both are overlapping, form interferogram 5.Therefore, lensless Fourier transform hologram is also referred to as quasi fourier transform hologram.The relation of Fourier transform hologram and lensless Fourier transform hologram, the relation of extraordinary image two-slit interference striped and two plane wave interference fringes.The interference fringe of two plane waves is equally spaced, and the two-slit interference striped is approximate equally spaced, and the center striped slightly is wider than the striped on both sides.For two-slit interference, interference field is far away more from double slit, and its interference fringe is similar to the interference fringe of two plane waves more.For lensless Fourier transform hologram, the record object distance is big more, and the difference of lensless Fourier transform hologram and Fourier transform hologram is more little.Record another big advantage of object distance is can improve the object point light cone and with reference to the overlapping degree of point source light cone, improve resolution.
During reproduction, in order to make one-level object wave and zero level object wave auto-correlation, and separated sample center and must be enough greatly with reference to the distance between the point source with negative first-order diffraction ripple.During record, if object wave is compared with reference wave, amplitude is enough little, and then the auto-correlation of object wave just can be ignored.Thereby, can not consider first-order diffraction ripple and the autocorrelative separation condition of object wave, sample and just can be further close with reference to point source, thereby it is minimum that lensless Fourier transform hologram is dropped to the requirement of the resolution of recording medium and X-ray beam temporal coherence, increased a lot of difficulties but do like this to experiment.
1992, people such as I.McNulty are on Brookhaven NSRL X-1AUndulator wire harness, adopt the holographic mode of lensless fourier transform, with CCD as receiver, digital method reappears, it is reported, the resolution of X ray lensless Fourier transform hologram is brought up to 60nm.They produce the higher zone plate of quality with the method for beamwriter lithography, and the narrowest endless belt width of zone plate reaches 50nm.The narrowest width of zone plate has determined the zone plate focused radius, and this focused radius is determining the resolution of lensless Fourier transform hologram.Ten between the halfhour exposure period in, guarantee the stability of system, and the temperature variation that controls environment, make its be no more than ± 1 ℃, the coherent length of the x-ray source that they are used is 0.7 μ m.
From above-mentioned discussion as can be seen, in the holography of X ray lensless fourier transform, because the existence of zero order wave has reduced the contrast and the resolution of reproduced image, so has been necessary very much zero order wave is eliminated from reproduced image.
Summary of the invention
The technical problem to be solved in the present invention is at the existing shortcoming of above-mentioned technology formerly, proposes a kind of apparatus and method of eliminating the holographic zero order wave of X ray lensless fourier transform, to improve the contrast and the resolution of reproduced image.
Technical solution of the present invention is as follows:
A kind of formation of eliminating the holographic zero order wave device of X ray lensless fourier transform: the working direction at the X ray of x-ray source is provided with zone plate successively, pinhole diaphragm and detector, the output terminal of this detector links to each other with computing machine, the pin hole of described pinhole diaphragm is positioned at the focus place of zone plate,-determinand is arranged in and the same plane of the pin hole of described pinhole diaphragm and another close hole, it is characterized in that after described determinand, being provided with a phase shifter, the phase shift of this phase shifter is 2k π, wherein k is a positive integer, when this device uses, same determinand is taken first X ray lensless Fourier transform hologram, do not insert earlier this phase shifter in the object beam, take second X ray lensless Fourier transform hologram, insert this phase shifter in the object beam.
Utilize described device to eliminate the method for the holographic zero order wave of X ray lensless fourier transform, it is characterized in that this method undertaken by following three steps:
1. in described device, do not insert phase shifter earlier in the object beam, take an X ray lensless Fourier transform hologram and also this hologram is stored in the computing machine;
2. in described device, insert phase shifter in the object beam, take an X ray lensless Fourier transform hologram again, also be stored in the computing machine;
3. in computing machine (6), the light intensity of two hologrm reconstructions is subtracted each other, can obtain to have eliminated the X ray lensless Fourier transform hologram of zero order wave.
Principle of work of the present invention is as follows: parallel X-ray illumination zone plate, through after the zone plate, an X ray part is zero order wave illumination determinand, a part ofly focused on by zone plate, and through a pinhole diaphragm as the reference ripple.Reference wave and interfered by the object wave of determinand scattering receives through detector, by the image of computer reconstruction determinand.
During recorded hologram, say in this way, when reconstruct, have the problem of a zero order wave image disruption as top.In order to address this problem, if insert a phase shifter in our the object beam light path, thereby obtain an X ray lensless Fourier transform hologram with different recording parameter, so before not adding phase shifter and add after the phase shifter, two holograms that obtain all are recorded on the detector, allow their intensity subtract each other, obtain the light intensity difference and be:
Figure C20041005278300051
In the formula: R is the reference wave amplitude, and O is the object wave amplitude,
Figure C20041005278300052
Phasic difference for object wave and reference wave.
Purpose at the intrafascicular adding phase shifter of thing is to allow Be a constant, promptly 2k π after two holograms subtract each other so, only contains RO and RO in the reconstructed image *Two, thus can reach the purpose that zero order wave is eliminated.
Compare with technology formerly: zero order wave removing method in the X ray lensless fourier transform holography of the present invention, only in object beam, add an X ray phase shifter, just can eliminate the zero order wave in the reconstructed image, thereby can improve the contrast and the resolution of reproduced image greatly.
Description of drawings
Fig. 1 is the existing schematic diagram of device that is used for the X ray lensless Fourier transform hologram.
Fig. 2 is a schematic diagram of device of eliminating zero order wave in the X ray lensless fourier transform of the present invention holography.
Embodiment
See also Fig. 2 earlier, Fig. 2 is a schematic diagram of device of eliminating zero order wave in the X ray lensless fourier transform of the present invention holography.As seen from the figure, the formation of eliminating the device of zero order wave in the X ray lensless fourier transform of the present invention holography is: the working direction at the X ray of x-ray source 1 is provided with zone plate 2 successively, pinhole diaphragm 4 and detector 5, the output terminal of this detector 5 links to each other with computing machine 6, one pin hole of described pinhole diaphragm 4 is positioned at the focus place of zone plate 2, one determinand 3 is arranged in another unthreaded hole conplane and close with the pin hole of described pinhole diaphragm 4, it is characterized in that after described determinand 3, being provided with a phase shifter 7, the phase shift of this phase shifter 7 is 2k π, and wherein k is a positive integer.
Utilize said apparatus to eliminate the method for the holographic zero order wave of X ray lensless fourier transform, undertaken by following three steps:
1. in described device, do not insert phase shifter 7 earlier in the object beam, take an X ray lensless Fourier transform hologram and also this hologram is stored in the computing machine 6;
2. in described device, insert phase shifter 7 in the object beam, take an X ray lensless Fourier transform hologram again, also be stored in the computing machine 6;
3. in computing machine 6, the light intensity of two hologrm reconstructions is subtracted each other, can obtain to have eliminated the X ray lensless Fourier transform hologram of zero order wave.

Claims (2)

1. eliminate the device of zero order wave in the X ray lensless fourier transform holography, working direction at the X ray of x-ray source (1) is provided with zone plate (2), pinhole diaphragm (4) and detector (5), the output terminal of this detector (5) links to each other with computing machine (6), the pin hole of described pinhole diaphragm (4) is positioned at the focus place of zone plate (2), one determinand (3) is arranged in and the same plane of pin hole of described pinhole diaphragm (4) and another close unthreaded hole, it is characterized in that being provided with a phase shifter (7) afterwards at described determinand (3), the phase shift of this phase shifter (7) is 2k π, wherein k is a positive integer, when this device uses, same determinand (3) is taken first X ray lensless Fourier transform hologram, do not insert earlier this phase shifter (7) in the object beam, take second X ray lensless Fourier transform hologram, insert this phase shifter (7) in the object beam.
2. utilize the described device of claim 1 to eliminate the method for the holographic zero order wave of X ray lensless fourier transform, it is characterized in that this method undertaken by following three steps:
1. in described device, do not insert phase shifter (7) earlier in the object beam, take an X ray lensless Fourier transform hologram and be stored in the computing machine (6);
2. in described device, insert phase shifter (7) in the object beam, take an X ray lensless Fourier transform hologram again and also be stored in the computing machine (6);
3. computing machine (6) subtracts each other the light intensity of two hologrm reconstructions, can obtain to have eliminated the X ray lensless Fourier transform hologram of zero order wave.
CNB2004100527834A 2004-07-13 2004-07-13 Device and method for eliminating X-ray lensless Fourier transform holographic zero-order wave Expired - Fee Related CN100399211C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2004100527834A CN100399211C (en) 2004-07-13 2004-07-13 Device and method for eliminating X-ray lensless Fourier transform holographic zero-order wave

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB2004100527834A CN100399211C (en) 2004-07-13 2004-07-13 Device and method for eliminating X-ray lensless Fourier transform holographic zero-order wave

Publications (2)

Publication Number Publication Date
CN1588238A CN1588238A (en) 2005-03-02
CN100399211C true CN100399211C (en) 2008-07-02

Family

ID=34602601

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2004100527834A Expired - Fee Related CN100399211C (en) 2004-07-13 2004-07-13 Device and method for eliminating X-ray lensless Fourier transform holographic zero-order wave

Country Status (1)

Country Link
CN (1) CN100399211C (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101976031A (en) * 2010-08-27 2011-02-16 昆明理工大学 Method for optimizing reproduced holographic images of digital micro-mirror
CN102589695B (en) * 2012-02-27 2014-02-26 苏州大学 Method and system for imaging spectrum
CN104808469B (en) * 2015-04-28 2017-09-12 中国科学院上海光学精密机械研究所 High resolution ratio digital holographic microscopic imaging device and imaging method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1343242A1 (en) * 1985-06-05 1987-10-07 МВТУ им.Н.Э.Баумана Interferometer for checking shape of spherical surfaces
US5074667A (en) * 1988-08-15 1991-12-24 Sumitomo Heavy Industries Co. Ltd. Position detector employing a sector fresnel zone plate
CN1136587C (en) * 2001-06-01 2004-01-28 中国科学院上海光学精密机械研究所 X-ray holographic microscope with preamplification

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1343242A1 (en) * 1985-06-05 1987-10-07 МВТУ им.Н.Э.Баумана Interferometer for checking shape of spherical surfaces
US5074667A (en) * 1988-08-15 1991-12-24 Sumitomo Heavy Industries Co. Ltd. Position detector employing a sector fresnel zone plate
CN1136587C (en) * 2001-06-01 2004-01-28 中国科学院上海光学精密机械研究所 X-ray holographic microscope with preamplification

Also Published As

Publication number Publication date
CN1588238A (en) 2005-03-02

Similar Documents

Publication Publication Date Title
CN102981390B (en) Apparatus for the exact reconstruction of the object wave in off-axis digital holography
US20220121152A1 (en) Holographic reconstruction device and method
Kakue et al. Digital holographic high-speed 3D imaging for the vibrometry of fast-occurring phenomena
US11314204B2 (en) Holographic reconstruction apparatus and method
CN101957171B (en) Coaxial digital holography method capable of effectively inhibiting zero-order and conjugate images
CN110488397B (en) Single-frame imaging device capable of coding and imaging method
CN112666815B (en) Continuous terahertz wave lens-free Fourier transform digital holographic imaging method
CN100399211C (en) Device and method for eliminating X-ray lensless Fourier transform holographic zero-order wave
CN109283821B (en) Phase-shift digital holographic single-exposure imaging device and method based on vortex lens
JP6309384B2 (en) Digital holography apparatus and digital holography method
Dubey et al. Interferenceless coded aperture correlation holography with point spread holograms of isolated chaotic islands for 3D imaging
Wang et al. An interference iterative reconstruction algorithm based on a single off-axis digital hologram
Monroy et al. Quantitative assessment of lateral resolution improvement in digital holography
Li et al. Single-shot phase-shifting radial-shearing digital holography with Fibonacci-sieve array irrespective of initial phases
Zhang et al. Incoherent frequency-selective phase coded holography and axial overlap information stripping
Zhang et al. Phase-shifting digital holography with vortex beam in one single exposure
Reddy et al. Space bandwidth product analysis of digital holography and image reconstruction process
CN117850185B (en) Off-axis digital holographic zero-order item suppression method based on binary phase modulation
CN219435223U (en) Coaxial single-pixel reference light non-interference type phase reading optical system
HALAQ et al. ZERO ORDER AND CONJUGATE IMAGES ELIMINATION FOR DIGITAL HOLOGRAMS
Halaq et al. Zero order elimination for digital holograms: Study of setup dependent methods
Kim et al. In-line digital holography using a quarter wave plate and averaging method
CN100464180C (en) Amplitude-splitting off-axis X-ray holographic device
Kelly et al. Analyzing Digital Holographic Systems with the LCT
SU263770A1 (en)

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20080702

Termination date: 20100713