ATE2T1 - PROCESS FOR PRODUCTION OF CIS-2,6DIMETHYLMORPHOLINE - Google Patents
PROCESS FOR PRODUCTION OF CIS-2,6DIMETHYLMORPHOLINEInfo
- Publication number
- ATE2T1 ATE2T1 AT79102376T AT79102376T ATE2T1 AT E2 T1 ATE2 T1 AT E2T1 AT 79102376 T AT79102376 T AT 79102376T AT 79102376 T AT79102376 T AT 79102376T AT E2 T1 ATE2 T1 AT E2T1
- Authority
- AT
- Austria
- Prior art keywords
- cis
- production
- dimethylmorpholine
- trans
- catalyst
- Prior art date
Links
- HNVIQLPOGUDBSU-OLQVQODUSA-N (2s,6r)-2,6-dimethylmorpholine Chemical compound C[C@H]1CNC[C@@H](C)O1 HNVIQLPOGUDBSU-OLQVQODUSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- HNVIQLPOGUDBSU-PHDIDXHHSA-N (2r,6r)-2,6-dimethylmorpholine Chemical compound C[C@@H]1CNC[C@@H](C)O1 HNVIQLPOGUDBSU-PHDIDXHHSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000006317 isomerization reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
- C07D295/027—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements containing only one hetero ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Abstract
A process for the preparation of cis-2,6-dimethylmorpholine from trans-2,6-dimethylmorpholine by isomerization over a catalyst in the presence of hydrogen.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19782830998 DE2830998A1 (en) | 1978-07-14 | 1978-07-14 | METHOD FOR PRODUCING CIS-2,6-DIMETHYLMORPHOLINE |
EP79102376A EP0007520B1 (en) | 1978-07-14 | 1979-07-11 | Process for the preparation of cis-2.6-dimethylmorpholine |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE2T1 true ATE2T1 (en) | 1981-02-15 |
Family
ID=6044395
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT79102376T ATE2T1 (en) | 1978-07-14 | 1979-07-11 | PROCESS FOR PRODUCTION OF CIS-2,6DIMETHYLMORPHOLINE |
Country Status (7)
Country | Link |
---|---|
US (1) | US4212972A (en) |
EP (1) | EP0007520B1 (en) |
JP (1) | JPS5515464A (en) |
AT (1) | ATE2T1 (en) |
CA (1) | CA1111035A (en) |
DE (2) | DE2830998A1 (en) |
HU (1) | HU182848B (en) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2938698A1 (en) * | 1979-09-25 | 1981-04-09 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING CIS-2,6-DIMETHYLMORPHOLINE |
DE3217964A1 (en) * | 1982-05-13 | 1983-11-17 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING CIS-2-, 6-DIMETHYLMORPHOLIN |
DE3322939A1 (en) * | 1983-06-25 | 1985-01-03 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING CIS-2,6-DIMETHYLMORPHOLINE |
DE3342009A1 (en) * | 1983-11-22 | 1985-05-30 | Chemische Werke Hüls AG, 4370 Marl | METHOD FOR THE DRAINAGE OF 2,6-DIMETHYLMORPHOLINE |
DE3708931A1 (en) * | 1987-03-19 | 1988-09-29 | Huels Chemische Werke Ag | METHOD FOR PRODUCING CIS-2,6-DIMETHYLMORPHOLINE |
DE4228885A1 (en) * | 1992-08-29 | 1994-03-03 | Basf Ag | Process for the preparation of 2,6-dimethylmorpholine from N- (2-hydroxypropyl) -2,6-dimethylmorpholine |
EP3269703B1 (en) | 2015-03-09 | 2021-03-24 | Mitsubishi Gas Chemical Company, Inc. | Method of isomerizing diaminodicyclohexylmethane |
CN108101860B (en) * | 2018-02-08 | 2021-11-23 | 苏州敬业医药化工有限公司 | Preparation method of cis-2, 6-dimethyl morpholine |
CN111499590A (en) * | 2020-04-07 | 2020-08-07 | 新乡市锦源化工有限公司 | Preparation method of high-purity cis-2, 6-dimethylmorpholine |
CN111825630B (en) * | 2020-06-24 | 2022-08-23 | 江苏富比亚化学品有限公司 | Synthesis process of cis-2, 6-dimethylmorpholine |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3083202A (en) * | 1960-06-06 | 1963-03-26 | Monsanto Chemicals | Isomerization of 2, 6-dimethylmorpholine |
-
1978
- 1978-07-14 DE DE19782830998 patent/DE2830998A1/en not_active Withdrawn
-
1979
- 1979-05-18 US US06/040,200 patent/US4212972A/en not_active Expired - Lifetime
- 1979-05-30 CA CA328,741A patent/CA1111035A/en not_active Expired
- 1979-06-26 JP JP7978179A patent/JPS5515464A/en active Granted
- 1979-07-11 EP EP79102376A patent/EP0007520B1/en not_active Expired
- 1979-07-11 AT AT79102376T patent/ATE2T1/en active
- 1979-07-11 DE DE7979102376T patent/DE2960127D1/en not_active Expired
- 1979-07-13 HU HU79BA3815A patent/HU182848B/en unknown
Also Published As
Publication number | Publication date |
---|---|
US4212972A (en) | 1980-07-15 |
CA1111035A (en) | 1981-10-20 |
DE2960127D1 (en) | 1981-02-26 |
JPH039111B2 (en) | 1991-02-07 |
EP0007520A1 (en) | 1980-02-06 |
DE2830998A1 (en) | 1980-01-31 |
JPS5515464A (en) | 1980-02-02 |
HU182848B (en) | 1984-03-28 |
EP0007520B1 (en) | 1981-01-07 |
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