KR880011019A - 24면체상 규산질입자 및 그 제법 - Google Patents

24면체상 규산질입자 및 그 제법 Download PDF

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Publication number
KR880011019A
KR880011019A KR1019880003663A KR880003663A KR880011019A KR 880011019 A KR880011019 A KR 880011019A KR 1019880003663 A KR1019880003663 A KR 1019880003663A KR 880003663 A KR880003663 A KR 880003663A KR 880011019 A KR880011019 A KR 880011019A
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South Korea
Prior art keywords
acid
zeolite
amorphous silica
active
siliceous
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KR1019880003663A
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English (en)
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KR950007159B1 (ko
Inventor
타다히사 나까가와
마사히데 오가와
아베끼요시
가즈히고 스즈끼
준 스즈끼
Original Assignee
원본미기재
미즈자와 카가쿠 코오교오 가부시기 가이샤
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Priority claimed from JP62076395A external-priority patent/JPS63242913A/ja
Priority claimed from JP63067223A external-priority patent/JPH06645B2/ja
Application filed by 원본미기재, 미즈자와 카가쿠 코오교오 가부시기 가이샤 filed Critical 원본미기재
Publication of KR880011019A publication Critical patent/KR880011019A/ko
Application granted granted Critical
Publication of KR950007159B1 publication Critical patent/KR950007159B1/ko

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
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    • C01—INORGANIC CHEMISTRY
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    • C01B33/00—Silicon; Compounds thereof
    • C01B33/20—Silicates
    • C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25—Silicon; Compounds thereof
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    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
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    • C01B33/28—Base exchange silicates, e.g. zeolites
    • C01B33/2807—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures
    • C01B33/2869—Zeolitic silicoaluminates with a tridimensional crystalline structure possessing molecular sieve properties; Isomorphous compounds wherein a part of the aluminium ore of the silicon present may be replaced by other elements such as gallium, germanium, phosphorus; Preparation of zeolitic molecular sieves from molecular sieves of another type or from preformed reacting mixtures of other types characterised by an X-ray spectrum and a definite composition
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Abstract

내용 없음

Description

24면체상 규산질입자 및 그 제법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명에 의한 활성 아날사임(anaicime)입자 (시료 No. 1-4)의 X선회절도
제2도는 원료 아날사임형 제올라이트(시료 No. 1-0)의 ,X선 회절도
제3도는 원료 아날사임형 제올라이트를 철저하게 산처리한 것(시료 No. 1-7)의 X선 회절도

Claims (20)

  1. 아날사임에 특유한 x-선회절상을 가지며 또한 개개의 입자가 24면체 내지는 모퉁이가 둥굴게 된 24면체 형상을 갖는 제올라이트 입자를 합성하는 공정과, 이 제올라이트를 산처리에 붙여 이 제올라이트중의 Al2O3분 및 Na2O 의 최소한 일부를 제거하는 공정으로 이루어진 24면체 내지 모퉁이가 둥글게 된 24면체의 형상을 갖는 규산질 입자의 제조법.
  2. 제1항에 있어서, 아날사임형 제올라이트가 SiO249 내지 59중량％,Al2O321내지25중량 ％, Na2O 12 내지 14중량 ％ 및 H2O 7내지 10중량 ％의 산화물기준의 조성을 갖는 것을 특징으로 하는 규산질 입자의 제조법.
  3. 제1항에 있어서, 산이 염산 또는 황산인 것을 특징으로 하는 규산질 입자의 제조법
  4. 제1항에 있어서, 상기 제올라이트를 수성슬러리로 하고, 이것에 산을 첨가하여 산처리를 하는 것을 특징으로 하는 규산질 입자의 제조법.
  5. 제1항에 있어서, 산처리를 20 내지 100℃의 온도에서 하는 것을 특징으로 하는 규산질 입자의 제조법.
  6. 제1항에 있어서, 산처리를 제올라이트를 비정질화하는데 충분한 양의 Al2O3분 및 Na2O분이 제거되도록 하고, 또한 규산질 입자가 비정질 실리카임을 특징으로 하는 규산질입자의 제조법.
  7. 제6항에 있어서, 제올라이트중의 Al2O3분 및 Na2O 분당 1.5몰 당량 이상의 산을 사용하여 산처리를 하는 것을 특징으로 하는 규산질 입자의 제조법.
  8. 제1항에 있어서, 제올라이트중의 Al2O3분 및 Na2O분의 합계 몰수당 0.1내지 1,2몰당량의 산을 사용하여 아날사임을 결정구조가 잔류하는 조견하에서 산처리를 하며 또한 규산질 입자가 활성아날사임인 것을 특징으로하는 규산질 입자의 제조법.
  9. 3성분 기준으로 SiO260내지 95중량％, Al2O30.3내지 20중량％ 및 Na2O0.02 내지 11중량％의 화학조성과,아날사임에 특유한 X-선회절상 및 90％ RH 및 25℃의 분위기중 24시간의 조건으로 측정하여 5내지 30중량 ％의 흡습량을 가지며 또한 개개의 입자가 24면체 내지는 모통이가 두울게 된 24면체의 입자형상과 전자현미경법으로 측정하여 0.1내지 50㎛의 1차입경을 갖는 것을특징으로 하는 활성아날사임.
  10. 제9항에 있어서, 50 내지 500㎡/ｇ의 BET 비표면적을 갖는 것을 특징으로 하는 활성아나라임.
  11. 제9항에 있어서, 1％고형분의 수성분산체로 했을 때,4내지8의 pH를 가지며 또한 고체산으로서의 특성을 갖는 것을 특징으로 하는 활성아날사임.
  12. 제9항에 있어서, 산강도 함수가 +4.8까지의 산량이 0.2 내지 1.0m-mol/ｇ인것을 특징으로 하는 활성아날사임.
  13. 제9항에 있어서, 파수1000내지1130 ㎝ -1 에 Si(Al)O의 신축진동에 의거한 시프트피크를 갖는 적외흡수 스펙트럼을 갖는 것을 특징으로 하는 활성아날사임.
  14. 제9항에 있어서, .5이하의 1차 입경의 표준편차(6)를 갖는 것을 특징으로 하는활성아날사임.
  15. 제올라이트의 산처리에 의해 얻어진 X-선 회절학적으로 실질상 비정질의 실리카로서, 개개의 입자가 24면체 내지는 모퉁이가 둥글게 된 24면체의 형상을하고 있으며 또한 1차 입경이 0.1 내지 50㎛의 범위에 있는 것을 특징으로 하는 비정질실리카.
  16. 제15항에 있어서, 파수900㎝-1에 비정질 실리카에 특유한 적외흡수피크를 갖는 것을 특징으로 하는 비정질 실리카.
  17. 제15항에 있어서, 0.5이하의 1차 입경의 표준편차(5)를 갖는 것을 특징으로 하는 비정질 실리카.
  18. 제9항 기재의 활성아날사임으로 이루어진 것을 특징으로 하는 무기충전제.
  19. 제15항 기재의 비정질 실리카로 이루어진 것을 특징으로 하는 무기충전제.
  20. 제9항 기재의 활성아날사임을 함유하는 것을 특징으로 하는 전기점성유체.
    ※참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019880003663A 1987-03-31 1988-03-31 24면체상 규산질 입자 및 그 제법 KR950007159B1 (ko)

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JP62076395A JPS63242913A (ja) 1987-03-31 1987-03-31 非晶質シリカ及びその製法
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JP63067223A JPH06645B2 (ja) 1988-03-23 1988-03-23 活性アナルサイム及びその製法
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JPH02150494A (ja) * 1988-12-01 1990-06-08 Bridgestone Corp 電気粘性液体
GB9011151D0 (en) * 1990-05-18 1990-07-04 Secr Defence Zeolites
EP0583763A3 (de) * 1992-08-20 1994-03-16 Hoechst Aktiengesellschaft Elektrorheologische Fluide auf der Basis synthetischer Schichtsilikate
JP3393885B2 (ja) * 1992-11-02 2003-04-07 信之 高橋 粉末分散放電加工液および放電加工法
AU5964296A (en) * 1995-05-26 1996-12-11 W.R. Grace & Co.-Conn. High-loading adsorbent/organic matrix composites
US5935891A (en) * 1995-05-26 1999-08-10 W. R. Grace & Co.-Conn. High-loading adsorbent/organic matrix composites
US5879764A (en) * 1996-11-06 1999-03-09 W. R. Grace & Co.-Conn. Desiccation using polymer-bound desiccant beads
US6263958B1 (en) 1998-02-23 2001-07-24 William H. Fleishman Heat exchangers that contain and utilize fluidized small solid particles
CN103418295B (zh) 2007-06-21 2015-11-18 简.探针公司 用于混合检测腔室的内容物的仪器和方法
EP3268423B1 (en) * 2015-03-13 2018-08-15 Bridgestone Corporation "method for the preparation of rubber compounds containing silicon dioxide for the production of tyres"
CN114920264B (zh) * 2022-06-28 2023-10-20 安阳工学院 不同形貌Analcime分子筛及其上晶面大小的可控制备方法

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1932832A (en) * 1925-02-18 1933-10-31 John W Turrentine Decolorizing, purifying, and adsorbing agent, and method of making the same
GB284245A (en) * 1928-01-25 1929-05-27 Arthur Rosenheim Improvements in and relating to the manufacture of adsorbing agents
GB574911A (en) * 1943-09-22 1946-01-25 Richard Maling Barrer Improvements in and relating to the manufacture of molecular sieve absorbents
US3836561A (en) * 1965-05-20 1974-09-17 Union Oil Co Method of treating alumina containing oxides
GB1245349A (en) * 1969-07-05 1971-09-08 Texaco Development Corp Extended zeolitic structures
FR2279668A1 (fr) * 1974-07-25 1976-02-20 Basf Ag Procede de preparation de zeolithes resistant a la chaleur et aux acides, a partir de faujasites alcalines
DE2510700C2 (de) * 1975-03-12 1983-01-27 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Zeolithen mit verbesserter Hochtemperatur- und Säurebeständigkeit
US4343723A (en) * 1980-03-14 1982-08-10 Uop Inc. Catalytic composite from partially crystallized clay
AU2066483A (en) * 1982-11-06 1984-05-10 British Petroleum Company Plc, The Ultra pure high crystallinity silicas
JPS59213616A (ja) * 1983-05-19 1984-12-03 Nippon Kogaku Kk <Nikon> 非晶質アルミノ珪酸塩及びその製法
US4689315A (en) * 1984-04-14 1987-08-25 Redco N.V. Amorphous silica particles, a method for producing same, and catalyst thereof
DE3536934A1 (de) * 1985-10-17 1987-04-23 Bayer Ag Elektroviskose fluessigkeiten
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