GB661685A - Improvements in or relating to the production of finely divided oxides of titanium, silicon, zirconium and aluminium - Google Patents
Improvements in or relating to the production of finely divided oxides of titanium, silicon, zirconium and aluminiumInfo
- Publication number
- GB661685A GB661685A GB3720/49A GB372049A GB661685A GB 661685 A GB661685 A GB 661685A GB 3720/49 A GB3720/49 A GB 3720/49A GB 372049 A GB372049 A GB 372049A GB 661685 A GB661685 A GB 661685A
- Authority
- GB
- United Kingdom
- Prior art keywords
- gas
- reaction
- oxygen
- chloride
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 title abstract 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title abstract 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 title abstract 2
- 239000004411 aluminium Substances 0.000 title abstract 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title abstract 2
- 229910052782 aluminium Inorganic materials 0.000 title abstract 2
- 229910052710 silicon Inorganic materials 0.000 title abstract 2
- 239000010703 silicon Substances 0.000 title abstract 2
- 239000010936 titanium Substances 0.000 title abstract 2
- 229910052719 titanium Inorganic materials 0.000 title abstract 2
- 229910052726 zirconium Inorganic materials 0.000 title abstract 2
- 239000007789 gas Substances 0.000 abstract 11
- 239000012495 reaction gas Substances 0.000 abstract 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 5
- 238000006243 chemical reaction Methods 0.000 abstract 5
- 239000001301 oxygen Substances 0.000 abstract 5
- 229910052760 oxygen Inorganic materials 0.000 abstract 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 4
- 239000000203 mixture Substances 0.000 abstract 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract 2
- 229910002091 carbon monoxide Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000000919 ceramic Substances 0.000 abstract 1
- 150000001805 chlorine compounds Chemical class 0.000 abstract 1
- 238000002485 combustion reaction Methods 0.000 abstract 1
- 238000007599 discharging Methods 0.000 abstract 1
- 150000002431 hydrogen Chemical class 0.000 abstract 1
- 238000007689 inspection Methods 0.000 abstract 1
- 239000003921 oil Substances 0.000 abstract 1
- 238000005192 partition Methods 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 238000009987 spinning Methods 0.000 abstract 1
- 238000000859 sublimation Methods 0.000 abstract 1
- 230000008022 sublimation Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G25/00—Compounds of zirconium
- C01G25/02—Oxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
- C01B13/14—Methods for preparing oxides or hydroxides in general
- C01B13/20—Methods for preparing oxides or hydroxides in general by oxidation of elements in the gaseous state; by oxidation or hydrolysis of compounds in the gaseous state
- C01B13/22—Methods for preparing oxides or hydroxides in general by oxidation of elements in the gaseous state; by oxidation or hydrolysis of compounds in the gaseous state of halides or oxyhalides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/181—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process
- C01B33/183—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process by oxidation or hydrolysis in the vapour phase of silicon compounds such as halides, trichlorosilane, monosilane
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/30—Preparation of aluminium oxide or hydroxide by thermal decomposition or by hydrolysis or oxidation of aluminium compounds
- C01F7/302—Hydrolysis or oxidation of gaseous aluminium compounds in the gaseous phase
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/07—Producing by vapour phase processes, e.g. halide oxidation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/02—Oxides; Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Pre-Mixing And Non-Premixing Gas Burner (AREA)
Abstract
Finely divided oxides of titanium, silicon, zirconium and aluminium are produced by discharging a mixture of the volatile chloride and oxygen-containing gas (reaction gas) at a temperature not exceeding 500 DEG C. into a reaction chamber and igniting the mixture to form a flame with the aid of an auxiliary chemical reaction delivering at least the amount of heat necessary for the ignition of the reaction mixture. The gas mixture composition, its temperature and exit velocity are preferably so chosen that the flame is kept at leat 1 mm. and up to 1 m, from the outlet opening for the gases. The oxygen-containing gas may be mixed with the chloride by feeding it to the still or sublimation chamber for the chloride, or by using it to atomize the superheated chloride. The auxiliary chemical reaction suitably consists in the combustion of hydrogen, carbon monoxide, oil vapours, &c. and the oxygen required, or a part thereof may be fed in admixture with the reaction gas. Concentric feed of the gases may be employed when carbon monoxide is used, this may surround the reaction gas, the separately fed oxygen-containing gas constituting the outer layer. The latter gas should however constitute the intermediate layer when hydrogen is employed. The direction of at least one of the outer gas streams suitably intersects that of the reaction gas stream, the combustible gas and oxygen-containing gas fed separately may be given a spin around the reaction gas, which also may spin in the same or opposite direction. A supply of heat additional to that provided by the exothermic chemical reaction may be furnished; thus, the walls of the reaction chamber may be heated. A variety of burner nozzles is shown consisting of three concentric tubes in which, (a) one or more is formed with helical partition walls to promote spinning of the gases, (b) the outer, or the outer and intermediate, tube terminate in a ring of small nozzles directed skew to the axis of the central tube, and (c) the outer, or the outer and intermediate ducts converge. The Specification as open to inspection under Sect. 91 is not restricted to the treatment of the four chlorides referred to above. It also comprises ignition of the reaction gas by other means. Thus, the use of a resistance heater protected by a ceramic tube, and of an electrode heater is illustrated. This subject-matter does not appear in the Specification as accepted.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH661685X | 1948-02-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB661685A true GB661685A (en) | 1951-11-28 |
Family
ID=4526948
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3720/49A Expired GB661685A (en) | 1948-02-20 | 1949-02-10 | Improvements in or relating to the production of finely divided oxides of titanium, silicon, zirconium and aluminium |
Country Status (5)
| Country | Link |
|---|---|
| CH (1) | CH265192A (en) |
| DE (1) | DE947788C (en) |
| FR (1) | FR981110A (en) |
| GB (1) | GB661685A (en) |
| NL (2) | NL145503C (en) |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2801901A (en) * | 1953-03-23 | 1957-08-06 | Cabot Godfrey L Inc | Process for making aluminum oxide from hydrated aluminum |
| US2957753A (en) * | 1958-11-05 | 1960-10-25 | American Cyanamid Co | Titanium dioxide from titanium tetrachloride |
| DE974793C (en) * | 1952-04-02 | 1961-04-27 | Degussa | Process for the production of finely divided oxides |
| US3002808A (en) * | 1957-08-07 | 1961-10-03 | Westinghouse Electric Corp | Preparation of ultrafine refractory oxide |
| US3007774A (en) * | 1955-04-14 | 1961-11-07 | Cabot Corp | Production of finely-divided aluminum oxide from bauxite |
| US3041136A (en) * | 1960-04-08 | 1962-06-26 | William H Hedley | Flame denitration and reduction of uranium nitrate to uranium dioxide |
| US3043657A (en) * | 1953-08-06 | 1962-07-10 | British Titan Products | Production of metal oxides |
| US3043656A (en) * | 1953-08-06 | 1962-07-10 | British Titan Products | Production of zirconium and hafnium oxides in a fluidized bed |
| EP0097378A2 (en) * | 1982-06-23 | 1984-01-04 | Wacker-Chemie GmbH | Process for the manufacture of pyrogenic silica with a great thickening ability |
| DE3540750A1 (en) * | 1984-11-19 | 1986-05-28 | Ube Industries Ltd., Yamaguchi | METHOD FOR THE PRODUCTION OF METAL OXIDE PARTICLES WITH A VERY SMALL AND UNIFORM GRAIN SIZE |
| CH658237A5 (en) * | 1983-08-25 | 1986-10-31 | Fuji Photo Film Co Ltd | Pyrogenic process and device for manufacturing highly conducting tin oxide powder |
| WO2005061385A2 (en) * | 2003-12-20 | 2005-07-07 | Degussa Ag | Aluminium oxide powder produced by flame hydrolysis and having a large surface area |
| WO2007127232A2 (en) * | 2006-04-28 | 2007-11-08 | Cabot Corporation | Process for the production of fumed silica |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE511837A (en) * | 1951-06-04 | |||
| DE974974C (en) * | 1953-07-19 | 1961-06-22 | Degussa | Process for the production of finely divided oxides |
| DE1221520B (en) * | 1955-07-07 | 1966-07-21 | Union Carbide Corp | Method and device for gas plating by means of a plating gas mixture obtained from a carrier gas generated by evaporation of a metal compound and a carrier gas heated to its vapor temperature |
| NL113022C (en) * | 1957-11-20 | |||
| DE1125410B (en) * | 1958-06-09 | 1962-03-15 | Julien Raick | Process and burner for the production of gas mixtures consisting essentially of carbon monoxide and hydrogen by thermal conversion of hydrocarbons |
| GB1047714A (en) * | 1962-07-17 | 1966-11-09 | Thann Fab Prod Chem | Apparatus useful inter alia for the production of finely divided metal oxides |
| NL299558A (en) * | 1962-10-23 | |||
| US3351427A (en) * | 1963-11-01 | 1967-11-07 | Cabot Corp | Vapor phase process for producing metal oxides |
| CH527890A (en) * | 1969-07-31 | 1972-09-15 | Sir Soc Italiana Resine Spa | Process for the preparation of titanium dioxide |
| US4292290A (en) * | 1980-04-16 | 1981-09-29 | Cabot Corporation | Process for the production of finely-divided metal and metalloid oxides |
| DE4009299A1 (en) * | 1989-04-19 | 1990-10-25 | Degussa | (ALPHA) ALUMINUM OXIDE AND METHOD FOR THE PRODUCTION THEREOF |
| DE19530339A1 (en) * | 1995-08-18 | 1997-02-20 | Degussa | Fumed silica, process for its production and use |
| AU2003215291A1 (en) | 2002-02-19 | 2003-09-09 | Tal Materials | Mixed-metal oxide particles by liquid feed flame spray pyrolysis of oxide precursors in oxygenated solvents |
| US7427577B2 (en) | 2006-04-06 | 2008-09-23 | Nanocerox Inc | Sintered polycrystalline terbium aluminum garnet and use thereof in magneto-optical devices |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB258313A (en) * | 1900-01-01 | |||
| US1552786A (en) * | 1922-07-14 | 1925-09-08 | Kalmus Comstock & Wescott Inc | Process of treating ores containing irom |
| FR572890A (en) * | 1923-01-20 | 1924-06-14 | Process for preparing titanium oxide | |
| US1850286A (en) * | 1925-05-20 | 1932-03-22 | Ig Farbenindustrie Ag | Process for making finely divided metal oxides |
| GB314075A (en) * | 1928-06-22 | 1930-12-18 | Sulphur And Smelting Corp | Improvements in the production of ferric oxide |
| GB535213A (en) * | 1939-05-04 | 1941-04-02 | Pittsburgh Plate Glass Co | Preparation of titanium dioxide |
| US2367118A (en) * | 1940-06-07 | 1945-01-09 | Heinen Josef | Manufacture of titanium dioxide |
-
0
- NL NL80078D patent/NL80078C/xx active
- NL NL145503D patent/NL145503C/xx active
-
1948
- 1948-02-20 CH CH265192D patent/CH265192A/en unknown
-
1949
- 1949-01-07 DE DEP31061A patent/DE947788C/en not_active Expired
- 1949-02-10 GB GB3720/49A patent/GB661685A/en not_active Expired
- 1949-02-19 FR FR981110D patent/FR981110A/en not_active Expired
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE974793C (en) * | 1952-04-02 | 1961-04-27 | Degussa | Process for the production of finely divided oxides |
| US2801901A (en) * | 1953-03-23 | 1957-08-06 | Cabot Godfrey L Inc | Process for making aluminum oxide from hydrated aluminum |
| US3043657A (en) * | 1953-08-06 | 1962-07-10 | British Titan Products | Production of metal oxides |
| US3043656A (en) * | 1953-08-06 | 1962-07-10 | British Titan Products | Production of zirconium and hafnium oxides in a fluidized bed |
| US3007774A (en) * | 1955-04-14 | 1961-11-07 | Cabot Corp | Production of finely-divided aluminum oxide from bauxite |
| US3002808A (en) * | 1957-08-07 | 1961-10-03 | Westinghouse Electric Corp | Preparation of ultrafine refractory oxide |
| US2957753A (en) * | 1958-11-05 | 1960-10-25 | American Cyanamid Co | Titanium dioxide from titanium tetrachloride |
| US3041136A (en) * | 1960-04-08 | 1962-06-26 | William H Hedley | Flame denitration and reduction of uranium nitrate to uranium dioxide |
| EP0097378A2 (en) * | 1982-06-23 | 1984-01-04 | Wacker-Chemie GmbH | Process for the manufacture of pyrogenic silica with a great thickening ability |
| EP0097378A3 (en) * | 1982-06-23 | 1986-03-12 | Wacker-Chemie GmbH | Process for the manufacture of pyrogenic silica with a great thickening ability |
| CH658237A5 (en) * | 1983-08-25 | 1986-10-31 | Fuji Photo Film Co Ltd | Pyrogenic process and device for manufacturing highly conducting tin oxide powder |
| DE3540750A1 (en) * | 1984-11-19 | 1986-05-28 | Ube Industries Ltd., Yamaguchi | METHOD FOR THE PRODUCTION OF METAL OXIDE PARTICLES WITH A VERY SMALL AND UNIFORM GRAIN SIZE |
| GB2168967A (en) * | 1984-11-19 | 1986-07-02 | Ube Industries | Process for producing metal oxide particles having a very small and uniform size |
| US4721610A (en) * | 1984-11-19 | 1988-01-26 | Ube Industries, Ltd. | Process for producing metal oxide particles having a very small and uniform size |
| WO2005061385A2 (en) * | 2003-12-20 | 2005-07-07 | Degussa Ag | Aluminium oxide powder produced by flame hydrolysis and having a large surface area |
| WO2005061385A3 (en) * | 2003-12-20 | 2005-11-24 | Degussa | Aluminium oxide powder produced by flame hydrolysis and having a large surface area |
| US7749322B2 (en) | 2003-12-20 | 2010-07-06 | Evonik Degussa Gmbh | Aluminium oxide powder produced by flame hydrolysis and having a large surface area |
| WO2007127232A2 (en) * | 2006-04-28 | 2007-11-08 | Cabot Corporation | Process for the production of fumed silica |
| WO2007127232A3 (en) * | 2006-04-28 | 2009-10-01 | Cabot Corporation | Process for the production of fumed silica |
| US7910081B2 (en) | 2006-04-28 | 2011-03-22 | Cabot Corporation | Process for the production of fumed silica |
Also Published As
| Publication number | Publication date |
|---|---|
| CH265192A (en) | 1949-11-30 |
| NL145503C (en) | |
| NL80078C (en) | |
| FR981110A (en) | 1951-05-22 |
| DE947788C (en) | 1956-09-13 |
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