DE3039210A1 - Digital display of filling height in fluidised bed - reactor using signals derived from two pressure difference meters - Google Patents
Digital display of filling height in fluidised bed - reactor using signals derived from two pressure difference metersInfo
- Publication number
- DE3039210A1 DE3039210A1 DE19803039210 DE3039210A DE3039210A1 DE 3039210 A1 DE3039210 A1 DE 3039210A1 DE 19803039210 DE19803039210 DE 19803039210 DE 3039210 A DE3039210 A DE 3039210A DE 3039210 A1 DE3039210 A1 DE 3039210A1
- Authority
- DE
- Germany
- Prior art keywords
- fluidized bed
- pressure difference
- pressure
- bulk density
- bed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1809—Controlling processes
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
- G01F23/00—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
- G01F23/14—Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measurement of pressure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00026—Controlling or regulating the heat exchange system
- B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
- B01J2208/0007—Pressure measurement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00026—Controlling or regulating the heat exchange system
- B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
- B01J2208/00079—Fluid level measurement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/0061—Controlling the level
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- General Physics & Mathematics (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
Description
a) die Apordnung als Druskdifferenz-Meßgerät pneu@ a) the arrangement as a drusk difference measuring device pneu @
HOECHST AKTIENGESELLSCHAFT HOE 80/H 030 matisch arbeitende Druckdifferenz-Transmitter aufweist; b) die preumatischen Ausgang@signele der pneumatisch 5 Digitale Anzeige der Füllhohe von arbeitenden Druckdiffenenz-Transmitter durch elek-Wirbelschichtreaktoren tro-pneumatische Umsetzer in analoge elektrische Signale umgewandelt werden; 10 Die vorliegende Erfindung betrifft eig Verfahren zur digitalen Anzeige der Füllhöhe von Wirbelschichtreaktoren, welches in einer Anordnung durchgeführt wird, d) die aus einem ersten Druckdifferenz-Meßgeräts dessen Meßronre in der Wirbelschichtzone angeordnet sind, und 15 einem zweiten Druckdifferenz-Meßgerät besteht, dessen unteres Meßrohr unten in der Wirbelschichtzone und dessen oberes Meßrohr oberhalb der Wirbelschichtzone angee) die von Pochner ermitteite Schüttdichte und die ordnet ist.HOECHST AKTIENGESELLSCHAFT HOE 80 / H 030 automatically operating differential pressure transmitters having; b) the preumatic output @ signals of the pneumatic 5 digital display the filling level of working pressure difference transmitters through elek fluidized bed reactors tro-pneumatic converters are converted into analog electrical signals; 10 The present invention relates to a method for digitally displaying the fill level of fluidized bed reactors, which is carried out in an arrangement, d) the from a first differential pressure measuring device its measuring device in the fluidized bed zone are arranged, and 15 is a second differential pressure measuring device, the lower Measuring tube below in the fluidized bed zone and its upper measuring tube above the fluidized bed zone angee) the bulk density determined by Pochner and which is ordered.
Füllhöhe der Wirbelschichtzone digital angezeigt werden. Level of the fluidized bed zone can be displayed digitally.
20 Beim Betrieb von Wirbelschichtreaktoren ist die Kenntnis der Schtlttdichte und der Füllhöhe der Wirbelschicht-1) zone von besonderer Bedeutung für die Leitung bzw. die Umsetzungsgeschwindigkeit. Bei Unkenntis dieser Werte kann es passieren, daß mit dem zugeführten Gas. körniger 25 Katalysator aus dem Reaktor ausgeblasen wird oder die Wirbelschichtzone zusammenfällt. Es ist deshalb beim Betrieb von Wirbelschichtreaktoren erforderlich, daß die Schüttdichte und die Füllhöhe der Wirbelschichtzone jederzeit kontrollierbar bleibt.20 When operating fluidized bed reactors, knowledge of the bulk density and the level of the fluidized bed zone 1) of particular importance for the line or the speed of implementation. If these values are not known, it can happen that with the supplied gas. Granular catalyst was blown out of the reactor or the fluidized bed zone collapses. It is therefore used in the operation of fluidized bed reactors required that the bulk density and the fill level of the fluidized bed zone at all times remains controllable.
Beim Verfahren gemäß der Erfindung entfallen individuelle 30 Es ist bekannt, die Dichte einer der Schwerkraft unterworfenen Flüssigkeit durch Messung der Differenz derhydrostatischen Drücke in zwei definienten unterschiedlichen Tiefen der Flüssigkeit zu bestimmen (vergl. HENG-35 STENBERG, STUREM, WINKLER: "Messen, Steuern und Regeln in der Chemischen Technik", Band II, Betriebsmeßtechnik II, - -1980, Seiten 142 bis 144>.In the method according to the invention, individual es are omitted known, the density of a liquid subjected to gravity by measurement the difference in the hydrostatic pressures at two defined different depths to determine the liquid (see HENG-35 STENBERG, STUREM, WINKLER: "Measure, Control and regulation in chemical engineering ", Volume II, Industrial measurement technology II, - -1980, pages 142 to 144>.
Weiterhin ist es bekannt, die Füllhöhe von Flüssigkeiten in Behältern mit Hilfe von hydrostatischen Meßverfahren zu ermitteln (vergl. u. a. HENGSTENBERG, STURM, WINKLER: "Messen, Steuern und Regeln in der Chemischen Technik, Band 1, Betriebsmeßtechnik I, 1980, Seiten 602 bis 608).It is also known to determine the level of liquids in containers to be determined with the help of hydrostatic measuring methods (see also HENGSTENBERG, STURM, WINKLER: "Measuring, controlling and regulating in chemical technology, Volume 1, industrial measurement technology I, 1980, pages 602 to 608).
Es ist Aufgabe der vorliegenden Erfindung, ein Verfahren zur Anzeige der Füllhöhe in Wirbelschichtreaktoren anzugeben, bei welchem die Kontrolle von Schüttdichte und Füllhöhe des körnigen Katalysators in der Wirbelschichtzone durch beispielsweise in einem Bedienungsstand direkt ablesbare Werte ständig möglich ist. Das wird erfindungsgemäß dadurch erreicht, daß die Meßwerte der Druckdifferenzen zu je einem elektrischen Analogsignal verarbeitet und die elektrischen Analogsignale einem Rechner zugeführt werden, wobei in dem Rechner in einem ersten Schritt aus dem elektrischen Analogsignal der ersten Druckdifferenzmessung die Schüttdichte der Wirbelschicht nach der Gleichung Druckdifferenz 1 1 Abstand = Abstand der Meßrohre . Erdbeschleunigung bestimmt wird und in einem zweiten Schritt aus der.It is the object of the present invention to provide a method for display indicate the filling level in fluidized bed reactors at which the control of Bulk density and filling height of the granular catalyst in the fluidized bed zone For example, values that can be read directly from a control station are always possible. This is achieved according to the invention in that the measured values of the pressure differences each processed into an electrical analog signal and the electrical analog signals be fed to a computer, the first step being in the computer the electrical analog signal of the first pressure difference measurement, the bulk density the fluidized bed according to the equation pressure difference 1 1 distance = distance between the measuring tubes . Gravitational acceleration is determined and in a second step from the.
Schüttdichte und dem elektrischen Analogsignal der zweiten Druckdifferenzmessung die Füllhöhe der Wirbelschichtzone nach der Gleichung = .. Druckdifferenz 2 1 Füllhöhe = Schüttdichte . Erdbeschleunigung errechnet wird, und die so ermittelte Schüttdichte und Füllhöhe auf einem Anzeigegerät sichtbar gemacbtwerden.Bulk density and the electrical analog signal of the second pressure difference measurement the filling level of the fluidized bed zone according to the equation = .. pressure difference 2 1 filling level = Bulk density. Gravitational acceleration is calculated, and the bulk density determined in this way and fill level can be visibly macbted on a display device.
Das Verfahren gemäB der Erfindung kann weiterhin wahlweise dadurch ausgestaltet sein, daß a) die Anordnung als Druckdifferenz-Meßgerät pneumatisch arbeitende Druckdifferenz-Transmitter aufweist; b) die pneumatischen Ausgangssignale der pneumatisch arbeitenden Druckdifferenz-Transmitter durch elektro-pneumatische Umsetzer in analoge elektrische Signale umgewandelt werden; c) die Anordnung als Druckdifferenz-Meßgerät elektrisch arbeitende Druckdifferenz-Transmitter aufweist; d) jeweils das elektrische Analogsignal mittels eines Digital^oltmeters zu elektrischen Impulsen verarbeitet wird, die ihrerseits der Rechner zugeführt werden; e) die vom Rechner ennittelte Schüttdichte und die Füllhöhe der Wirbelschichtzone digital angezeigt werden; f) das Verfahren durchgeführt wird mit einer Anordnung, bei der die beiden Druckdifferenz-Meßgeräte an einem Stutzen gemeinsam angeschlossen sind.The method according to the invention can furthermore optionally thereby be designed that a) the arrangement as a pressure differential measuring device has pneumatically operating differential pressure transmitters; b) the pneumatic Output signals of the pneumatically operating differential pressure transmitters by means of electro-pneumatic ones Converters are converted into analog electrical signals; c) the order as Differential pressure measuring device has electrically operating differential pressure transmitters; d) in each case the electrical analog signal to electrical by means of a digital oltmeter Pulses are processed, which in turn are fed to the computer; e) from Computer averaged bulk density and the filling level of the fluidized bed zone digitally displayed will; f) the procedure is carried out with an arrangement in which the two Differential pressure gauges are jointly connected to a nozzle.
Das erfindungsgemäBe Verfahren zeichnet sich durch Einfachheit und kostengünstige Anwendung bekannter Bauelemente aus.The inventive method is characterized by simplicity and inexpensive application of known components.
Beim Verfahren gemäß der Erfindung entfallen individuelle Ablesefehler bei der Feststellung der Meßwerte der Druckdifferenzen. Vielmehr werden bei diesem Verfahren die ermittelten Meßwerte mit hoher Auflösung direkt weiterverarbeitet.In the method according to the invention, there are no individual reading errors when determining the measured values of the pressure differences. Rather, be at this Method directly processes the determined measured values with high resolution.
Beim erfindungsgemäßen Verfahren stehen die für den Betrieb eines Wirbelschichtreaktors besonders wichtigen Werte "Füllhöhe" und "Schüttdichte" als kontinuierliche Anzeige jederzeit zur Verfügung.In the method according to the invention, the stand for the operation of a Fluidized bed reactor particularly important values "filling height" and "bulk density" as continuous display available at any time.
In der beigefügten Zeichnung ist eine Anordnung zur Durchführung des erfindungsgemäßen Verfahrens schematisch dargestellt.-Ein Reaktor 2 enthält eine Wirbelschichtzone 1, in welcher sich fluidisierter körniger Katalysator befindet.In the accompanying drawing is an arrangement for performing the Process according to the invention shown schematically.-A reactor 2 contains a Fluidized bed zone 1, in which there is fluidized granular catalyst.
Am Reaktor 2 sind mehrere Meßrohre (3, 4, 6, 7) von Druckdifferenz-Meßgeräten (5, 8) angeordnet, welche mit Spülgas aus einer Druckgasleitung 9 beaufschlagt werden. Die von dem ersten Druckdifferenz-Meßgerät 5 ermittelten pneumatischen Meßgrößen werden in den elektro-pneumatischen Umsetzer 10 übergeben, dessen elektrischer Ausgangswert in einem Digitalvoltmeter 11 in elektrische Impulse umgewandelt wird. Aus diesen elektrischen Impulsen wird in einem Rechner 14 die Schüttdichte berechnet, gespeichert und in einem Anzeigegerät 15 digital sichtbar gemacht.At the reactor 2 there are several measuring tubes (3, 4, 6, 7) of differential pressure measuring devices (5, 8) are arranged, which are acted upon with flushing gas from a compressed gas line 9. The pneumatic measured variables determined by the first pressure difference measuring device 5 are transferred to the electro-pneumatic converter 10, its electrical output value is converted into electrical impulses in a digital voltmeter 11. From these electrical impulses, the bulk density is calculated in a computer 14, stored and made digitally visible in a display device 15.
Die von dem zweiten Druckdifferenz-Meßgerät 8 ermittelten pneumatischen Meßgrößen werden in den elektro-pneumatischen Umsetzer 12 übergeben, dessen elektrischer Ausgangswert in einem Digitalvoltmeter 13 in elektrische Impulse umgewandelt wird. Aus diesen elektrischen Impulsen und dem gespeicherten Wert der Schüttdichte wird im Rechner 14 die Füllhöhe berechnet und in dem Anzeigegerät 16 digital sichtbar gemacht.The determined by the second pressure difference measuring device 8 pneumatic Measured variables are transferred to the electro-pneumatic converter 12, its electrical Output value is converted into electrical pulses in a digital voltmeter 13. From these electrical impulses and the stored value, the bulk density becomes the filling level is calculated in the computer 14 and is digitally visible in the display device 16 made.
Claims (7)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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DE19803039210 DE3039210C2 (en) | 1980-10-17 | 1980-10-17 | Digital display of the bulk density and fill level of granular catalysts in a fluidized bed reactor |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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DE19803039210 DE3039210C2 (en) | 1980-10-17 | 1980-10-17 | Digital display of the bulk density and fill level of granular catalysts in a fluidized bed reactor |
Publications (2)
Publication Number | Publication Date |
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DE3039210A1 true DE3039210A1 (en) | 1982-05-06 |
DE3039210C2 DE3039210C2 (en) | 1992-02-27 |
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Application Number | Title | Priority Date | Filing Date |
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DE19803039210 Expired DE3039210C2 (en) | 1980-10-17 | 1980-10-17 | Digital display of the bulk density and fill level of granular catalysts in a fluidized bed reactor |
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0093801A2 (en) * | 1982-05-11 | 1983-11-16 | KRW Energy Systems Inc. | Control of bed height in a fluidized bed gasification system |
EP0112105A1 (en) * | 1982-12-16 | 1984-06-27 | The Babcock & Wilcox Company | Fluidised bed level measurement |
EP0145379A2 (en) * | 1983-11-23 | 1985-06-19 | Transitron Electronics Corp. | Tank level measuring system |
EP0183154A2 (en) * | 1984-11-23 | 1986-06-04 | BASF Aktiengesellschaft | Method for the continuous measurement of the degree of filling fluidised-powder apparatuses |
DE3525455A1 (en) * | 1985-07-17 | 1987-01-29 | Helmut Haiges | Control device for fermenting temperature |
EP0214801A1 (en) * | 1985-08-22 | 1987-03-18 | Parmade Instruments C.C. | A method of monitoring the liquid contents of a container vessel, monitoring apparatus for use in such method, and an installation including such apparatus |
DE3728042A1 (en) * | 1987-08-22 | 1989-03-02 | Bosch Gmbh Robert | Filling-level indicator for closable containers |
FR2678398A1 (en) * | 1991-06-28 | 1992-12-31 | Champagne Moet Chandon | Process for delivering a specified quantity of particles in suspension in a fluid and apparatus for the execution of this process |
DE19714168A1 (en) * | 1997-04-07 | 1998-10-08 | Rossendorf Forschzent | Device for hydrostatic filling measurement in pressure container |
EP1092958A1 (en) * | 1999-10-14 | 2001-04-18 | Wagner International Ag | Method and device for measuring the quantity of powder or the change of the quantity of powder in a container |
CN107782403A (en) * | 2017-10-23 | 2018-03-09 | 福建龙净脱硫脱硝工程有限公司 | A kind of apparatus for measuring charge level and material level measuring method |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2124702C1 (en) * | 1995-07-10 | 1999-01-10 | Чангмин Ко., Лтд. | Process measuring level of water or liquid ( versions ) and bubbling level indicator |
CN104089680B (en) * | 2014-07-25 | 2018-01-12 | 赵云华 | The measuring method and device of liquid level height |
Citations (2)
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DE2248315A1 (en) * | 1972-10-02 | 1974-04-25 | Rheinische Braunkohlenw Ag | DEVICE FOR MEASURING DIFFERENTIAL PRESSURES AND DETERMINING THE WATER LEVEL IN WELLS, GROUNDWATER MEASURING POINTS AND THE LIKE |
DE2849066A1 (en) * | 1978-11-11 | 1980-05-22 | Vdo Schindling | Vehicle fuel tank level indicator - uses low-pass filter to eliminate interference caused by vehicle movement mounted between tank transducer and indicators |
-
1980
- 1980-10-17 DE DE19803039210 patent/DE3039210C2/en not_active Expired
Patent Citations (2)
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---|---|---|---|---|
DE2248315A1 (en) * | 1972-10-02 | 1974-04-25 | Rheinische Braunkohlenw Ag | DEVICE FOR MEASURING DIFFERENTIAL PRESSURES AND DETERMINING THE WATER LEVEL IN WELLS, GROUNDWATER MEASURING POINTS AND THE LIKE |
DE2849066A1 (en) * | 1978-11-11 | 1980-05-22 | Vdo Schindling | Vehicle fuel tank level indicator - uses low-pass filter to eliminate interference caused by vehicle movement mounted between tank transducer and indicators |
Non-Patent Citations (2)
Title |
---|
Daizo Kunii, Octave Levenspiel "FLUIDIZATION ENGINEERING", Robert E. Krieger Publishing Company Huntington, New York, 1977, S. 407-409 * |
Hengstenberg: Messen, Steuern und Regeln in der chem. Technik- Bd. 1, S. 602-606, Bd. 2, S. 142-144, Berlin 1980.- * |
Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0093801A3 (en) * | 1982-05-11 | 1984-10-03 | Westinghouse Electric Corporation | Control of bed height in a fluidized bed gasification system |
EP0093801A2 (en) * | 1982-05-11 | 1983-11-16 | KRW Energy Systems Inc. | Control of bed height in a fluidized bed gasification system |
EP0112105A1 (en) * | 1982-12-16 | 1984-06-27 | The Babcock & Wilcox Company | Fluidised bed level measurement |
EP0145379A3 (en) * | 1983-11-23 | 1987-06-24 | Transitron Electronics Corp. | Tank level measuring system |
EP0145379A2 (en) * | 1983-11-23 | 1985-06-19 | Transitron Electronics Corp. | Tank level measuring system |
EP0183154A2 (en) * | 1984-11-23 | 1986-06-04 | BASF Aktiengesellschaft | Method for the continuous measurement of the degree of filling fluidised-powder apparatuses |
EP0183154A3 (en) * | 1984-11-23 | 1987-06-16 | BASF Aktiengesellschaft | Method for the continuous measurement of the degree of filling fluidised-powder apparatuses |
DE3525455A1 (en) * | 1985-07-17 | 1987-01-29 | Helmut Haiges | Control device for fermenting temperature |
EP0214801A1 (en) * | 1985-08-22 | 1987-03-18 | Parmade Instruments C.C. | A method of monitoring the liquid contents of a container vessel, monitoring apparatus for use in such method, and an installation including such apparatus |
DE3728042A1 (en) * | 1987-08-22 | 1989-03-02 | Bosch Gmbh Robert | Filling-level indicator for closable containers |
FR2678398A1 (en) * | 1991-06-28 | 1992-12-31 | Champagne Moet Chandon | Process for delivering a specified quantity of particles in suspension in a fluid and apparatus for the execution of this process |
EP0526278A1 (en) * | 1991-06-28 | 1993-02-03 | CHAMPAGNE MOET & CHANDON | Process for delivering a predetermined quantity of particles suspended in a fluid and apparatus for carrying out this process |
US5323930A (en) * | 1991-06-28 | 1994-06-28 | Champagne Moet & Chandon | Method of dispensing a determined amount of particles suspended in a fluid and device for carrying out this method |
DE19714168A1 (en) * | 1997-04-07 | 1998-10-08 | Rossendorf Forschzent | Device for hydrostatic filling measurement in pressure container |
DE19714168C2 (en) * | 1997-04-07 | 2000-05-25 | Rossendorf Forschzent | Arrangement for hydrostatic level measurement in a pressure vessel |
EP1092958A1 (en) * | 1999-10-14 | 2001-04-18 | Wagner International Ag | Method and device for measuring the quantity of powder or the change of the quantity of powder in a container |
US6494645B1 (en) | 1999-10-14 | 2002-12-17 | Wagner International Ag | Method and device for determining a powder quantity or change in powder quantity in a container |
CN107782403A (en) * | 2017-10-23 | 2018-03-09 | 福建龙净脱硫脱硝工程有限公司 | A kind of apparatus for measuring charge level and material level measuring method |
Also Published As
Publication number | Publication date |
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DE3039210C2 (en) | 1992-02-27 |
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Owner name: VINNOLIT MONOMER GMBH & CO. KG, 85737 ISMANING, DE |