CN113287617A - Safflower seed coating agent, coating method and application thereof - Google Patents

Safflower seed coating agent, coating method and application thereof Download PDF

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Publication number
CN113287617A
CN113287617A CN202110492165.5A CN202110492165A CN113287617A CN 113287617 A CN113287617 A CN 113287617A CN 202110492165 A CN202110492165 A CN 202110492165A CN 113287617 A CN113287617 A CN 113287617A
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safflower
percent
seeds
seed
coating
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王继永
包芳
尚兴朴
曾燕
樊良帅
邓庭伟
张峰
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China Traditional Chinese Medicine Seed & Seedling Co ltd
China National Traditional Chinese Medicine Co ltd
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China Traditional Chinese Medicine Seed & Seedling Co ltd
China National Traditional Chinese Medicine Co ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/72Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
    • A01N43/74Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,3
    • A01N43/781,3-Thiazoles; Hydrogenated 1,3-thiazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C1/00Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
    • A01C1/06Coating or dressing seed
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C1/00Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
    • A01C1/08Immunising seed
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • A01N37/46N-acyl derivatives
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N51/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds having the sequences of atoms O—N—S, X—O—S, N—N—S, O—N—N or O-halogen, regardless of the number of bonds each atom has and with no atom of these sequences forming part of a heterocyclic ring

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  • Life Sciences & Earth Sciences (AREA)
  • Environmental Sciences (AREA)
  • Dentistry (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Soil Sciences (AREA)
  • Pretreatment Of Seeds And Plants (AREA)

Abstract

The invention relates to a safflower seed coating agent, a coating method and application thereof, wherein the seed coating agent comprises the following raw materials in percentage by mass: 2.09-3.48 percent of thiabendazole, 0.27-0.45 percent of metalaxyl-M, 0.35-0.58 percent of fludioxonil, 3 percent of thiamethoxam, 3 percent of agricultural emulsion 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose, 4 percent of glycol and the balance of purified water. The coating method comprises the following steps: s1, preparing a safflower seed coating agent; s2, mixing the seed coating agent and safflower seeds, stirring evenly, and drying in the air to finish the coating of the safflower seeds. The safflower seed coating provided by the invention can be used for solving pathogenic bacteria, seedling diseases and insect pests and the like carried by safflower seeds, and simultaneously increasing the root biomass of the safflower, thereby improving the germination rate of the seeds and the quality of medicinal materials thereof.

Description

Safflower seed coating agent, coating method and application thereof
Technical Field
The invention belongs to the technical field of traditional Chinese medicine seed treatment agents, and particularly relates to a safflower seed coating agent, a coating method and application thereof.
Background
The seed coating agent is a pesticide preparation with film forming property for treating plant seeds. The seed coating agent is composed of active ingredients and auxiliary agents, and can be coated on the surface of seeds directly or after being diluted to form a protective film agent with certain strength and permeability. The seed is treated by the seed coating agent, so that the effects of protecting and strengthening the seedling, improving the stress resistance and comprehensively preventing and treating the diseases and insect pests in the seedling stage are achieved, the purposes of yield preservation and yield increase are further achieved, meanwhile, the seed coating agent is used in a concealed mode, targets are clear, centralized treatment is achieved, the environment and ecological protection is facilitated, the medicine, the time and the money are saved, the resources are saved, the cost is reduced, and the economic and ecological benefits are remarkable. In view of the above advantages, the seed coating agent is widely used.
The safflower is the flower of the safflower of the Compositae, is one of the bulk medicinal materials commonly used in China, and has the effects of activating blood, stimulating menstrual flow, dissipating blood stasis and relieving pain. Safflower is usually propagated by seeds, and the seeds are easily damaged by seeds or soil pathogenic bacteria when the rainfall amount is sufficient or the soil is too wet in the germination period, so that the emergence rate and the quality of medicinal materials are influenced. The seed coating technology can prevent and control plant diseases and insect pests in the seedling stage, promote the growth of seedlings and has obvious economic effect. The seed coating agent of the Chinese country is mainly applied to crop seeds, the research on the seed coating agent of the traditional Chinese medicinal material seeds is less, because germination inhibitors exist in the safflower seeds, the germination is slow, and the seed coating agent of common crop seeds cannot promote the germination of the safflower seeds, so the seed coating agent capable of improving the germination rate of the safflower seeds is needed.
Disclosure of Invention
Aiming at the problems, the invention provides a safflower seed coating agent, a coating method and application thereof, which are used for solving pathogenic bacteria, seedling diseases and insect pests and the like carried by safflower seeds and increasing root biomass of safflower so as to improve the germination rate of the seeds and the quality of medicinal materials.
The seed coating agent comprises the following raw materials in percentage by mass:
2.09-3.48 percent of thiabendazole, 0.27-0.45 percent of metalaxyl-M, 0.35-0.58 percent of fludioxonil, 3 percent of thiamethoxam, 3 percent of agricultural emulsion 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose, 4 percent of glycol and the balance of purified water.
A coating method of a safflower seed coating agent comprises the following steps:
s1, preparing a safflower seed coating agent;
s2, mixing the seed coating agent and safflower seeds, stirring evenly, and drying in the air to finish the coating of the safflower seeds.
Further, in step S2, the seed ratio of the safflower seed coating to the licorice seed is 1 mL: 130-220 g.
Further, the safflower seed coating agent comprises the following raw materials in percentage by mass: 3.48% of thiabendazole, 0.45% of metalaxyl-M, 0.58% of fludioxonil, 3% of thiamethoxam, 3% of agricultural milk 700, 0.3% of xanthan gum, 0.2% of sodium carboxymethylcellulose, 4% of ethylene glycol and the balance of purified water.
Further, the drug seed ratio of the safflower seed coating agent to the safflower seeds is 1 mL: 220g of the total weight of the powder.
An application of a safflower seed coating agent in seed seedling raising.
The application of a coating method, wherein the coating method can be applied to seedling raising of safflower seeds.
Compared with the prior art, the invention has the following beneficial effects:
(1) the invention provides a seed coating agent and a coating method and application thereof, the seed coating agent consists of 2.09-3.48% of thiabendazole, 0.27-0.45% of metalaxyl-M, 0.35-0.58% of fludioxonil, 3% of thiamethoxam, 3% of agricultural emulsion 700, 0.3% of xanthan gum, 0.2% of sodium carboxymethylcellulose, 4% of glycol and purified water, and the seed coating agent has simple components, convenient preparation, safety and low toxicity;
(2) the coating method is that the seed coating agent and seeds are directly mixed and stirred uniformly according to a certain medicine proportion and then dried, the coating method is simple, the seed coating agent and the coating method thereof are optimized and verified, the problems of withered and yellow safflower seedlings, damaged growing points and the like are relieved in germination box experiments, sand box experiments and field experiments, the emergence rate is effectively improved, and the synthesis of root system biomass is promoted;
(3) the seed coating agent and the coating method thereof are used for raising seedlings of safflower seeds, can effectively solve pathogenic bacteria, seedling diseases and insect pests and the like carried by the safflower seeds, and simultaneously increase the root length biomass of the safflower, thereby improving the germination rate of the safflower and the quality of medicinal materials thereof.
Additional features and advantages of the invention will be set forth in the description which follows, and in part will be obvious from the description, or may be learned by practice of the invention. The objectives and other advantages of the invention will be realized and attained by the structure particularly pointed out in the written description and claims hereof as well as the appended drawings.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, and it is obvious that the drawings in the following description are some embodiments of the present invention, and those skilled in the art can also obtain other drawings according to the drawings without creative efforts.
FIG. 1 is a front view and a rear view of a coated safflower seed according to example 3 of the present invention, wherein a is an uncoated safflower seed and b is a coated safflower seed;
FIG. 2 is a diagram showing the germination of safflower seeds in a germination box before and after coating according to example 3 of the present invention, wherein a is a diagram showing the germination of uncoated safflower seeds in a germination box, and b is a diagram showing the germination of coated safflower seeds in a germination box;
FIG. 3 is a diagram showing the germination of safflower seeds in a sand box before and after coating according to example 3 of the present invention, wherein a is a diagram showing the germination of uncoated safflower seeds in a sand box, and b is a diagram showing the germination of coated safflower seeds in a sand box;
FIG. 4 is a graph showing the results of the field experiment of the safflower seeds before and after coating according to example 3 of the present invention, wherein a is a graph showing the results of the field experiment of the uncoated safflower seeds and b is a graph showing the results of the field experiment of the coated safflower seeds;
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some, but not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The raw material components of the safflower seed coating agent in the following examples are all expressed by mass percent of effective components. In this embodiment, the agricultural emulsion 700 is used as a wetting agent, xanthan gum is used as a thickener, sodium carboxymethyl cellulose is used as a film forming agent, and ethylene glycol is used as an antifreeze.
Example 1
A coating method of a safflower seed coating agent comprises the following steps:
s1, preparing a safflower seed coating agent: is prepared by mixing 2.09 percent of thiabendazole, 0.27 percent of metalaxyl-M, 0.35 percent of fludioxonil, 3 percent of thiamethoxam, 3 percent of agricultural milk 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose and 4 percent of glycol with 86.79 percent of purified water;
s2, coating: and (4) pouring 1mL of the safflower seed coating prepared in the step S1 into a plastic bag filled with 220g of safflower seeds, fully shaking to mix uniformly, and airing to finish coating of the safflower seeds.
Example 2
A coating method of a safflower seed coating agent comprises the following steps:
s1, preparing a safflower seed coating agent: is prepared by mixing 2.28 percent of thiabendazole, 0.36 percent of metalaxyl-M, 0.46 percent of fludioxonil, 3 percent of thiamethoxam, 3 percent of agricultural milk 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose and 4 percent of glycol with 86.4 percent of purified water;
s2, coating: and (4) pouring 1mL of the safflower seed coating prepared in the step S1 into a plastic bag filled with 220g of safflower seeds, fully shaking to mix uniformly, and airing to finish coating of the safflower seeds.
Example 3
A coating method of a safflower seed coating agent comprises the following steps:
s1, preparing a safflower seed coating agent: is prepared by mixing 3.48 percent of thiabendazole, 0.45 percent of metalaxyl-M, 0.58 percent of fludioxonil, 3 percent of thiamethoxam, 3 percent of agricultural emulsion 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose and 4 percent of glycol with 84.99 percent of purified water;
s2, coating: and (4) pouring 1mL of the safflower seed coating prepared in the step S1 into a plastic bag filled with 220g of safflower seeds, fully shaking to mix uniformly, and airing to finish coating of the safflower seeds. The before and after coating of the safflower seed of this example is shown in fig. 1, and fig. 1 is before and after coating of the safflower seed according to example 3 of the present invention, wherein a is uncoated safflower seed and b is coated safflower seed.
Example 4
A coating method of a safflower seed coating agent comprises the following steps:
s1, preparing a safflower seed coating agent: is prepared by mixing 3.48 percent of thiabendazole, 0.45 percent of metalaxyl-M, 0.58 percent of fludioxonil, 3 percent of thiamethoxam, 3 percent of agricultural emulsion 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose and 4 percent of glycol with 84.99 percent of purified water;
s2, coating: and (4) pouring 1mL of the safflower seed coating prepared in the step S1 into a plastic bag filled with 130g of safflower seeds, fully shaking until the mixture is uniformly mixed, and airing to finish coating of the safflower seeds.
Example 5
A coating method of a safflower seed coating agent comprises the following steps:
s1, preparing a safflower seed coating agent: is prepared by mixing 3.48 percent of thiabendazole, 0.45 percent of metalaxyl-M, 0.58 percent of fludioxonil, 3 percent of thiamethoxam, 3 percent of agricultural emulsion 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose and 4 percent of glycol with 84.99 percent of purified water;
s2, coating: and (4) pouring 1mL of the safflower seed coating prepared in the step S1 into a plastic bag filled with 165g of safflower seeds, fully shaking to mix uniformly, and airing to finish coating of the safflower seeds.
Verification example
1) Germination Box experiment
Randomly placing 50 coated safflower seeds on a paper bed of a germination box, alternately performing 12-hour illumination and 12-hour dark culture every day, keeping the temperature at 20 ℃, regularly spraying a proper amount of water every day to keep the germination paper moist, counting the germination rate (the length of a radicle exceeds the length of the seeds) on the third day of the experiment, and recording the germination rate and the mold growth rate when two leaves grow out, wherein the germination rate is regarded as the end of germination;
wherein the coated safflower seeds are obtained by adopting the coating method of any one of embodiments 1 to 5; uncoated safflower seeds were used as controls, and each set of experiments was repeated five times; the results are shown in Table 1, wherein each example refers to the coated safflower seeds obtained by the coating method of the corresponding numbered example; wherein, the diagram of the germination box for safflower seeds before and after coating of the embodiment 3 is shown in fig. 2, fig. 2 is the diagram of the germination box for safflower seeds before and after coating of the embodiment 3 according to the invention, wherein a is the diagram of the germination box for uncoated safflower seeds, and b is the diagram of the germination box for coated safflower seeds.
TABLE 1 germination and mold growth before and after coating of safflower seeds
Figure BDA0003052841780000051
The results in table 1 show that the safflower seeds are coated by the safflower seed coating agent and the coating method thereof, after the safflower seeds are coated, the germination rate is improved by 25-35% and the mildew rate is reduced by 25-35%, namely the safflower seed coating agent can obviously improve the germination rate of the safflower seeds and reduce the mildew rate of the safflower seeds by matching with the coating method with a proper drug seed ratio.
2) Sandbox experiment
Randomly placing 100 coated safflower seeds in a sand box, alternately performing 12-hour illumination and 12-hour dark culture every day, keeping the temperature at 20 ℃, regularly spraying a proper amount of water every day to keep the sand box moist, beginning to emerge from the earth, counting the emergence rate, and recording and counting the emergence rate and the mildew rate when three leaves grow out, namely the end of germination;
wherein the coated safflower seeds are obtained by adopting the coating method of any one of embodiments 1 to 5; uncoated safflower seeds were used as controls, and each set of experiments was repeated five times; the results are shown in Table 2, wherein each example refers to the coated safflower seeds obtained by the coating method according to the corresponding numbered example; wherein, the sand box map of safflower seeds before and after coating of example 3 is shown in fig. 3, fig. 3 is the germination map of safflower seeds in the sand box before and after coating of example 3 according to the invention, wherein a is the germination map of uncoated safflower seeds in the sand box, and b is the germination map of coated safflower seeds in the sand box.
TABLE 2 emergence rate and mildew rate before and after coating of safflower seeds
Figure BDA0003052841780000061
The results in table 2 show that the safflower seeds are coated by the safflower seed coating agent and the coating method thereof, after the safflower seeds are coated, the emergence rate of the safflower seeds is improved by 6-12 percent, the mildew rate is reduced by 9-12 percent, and the emergence rate of the safflower seeds can be obviously improved.
3) Field experiment
Randomly and uniformly mixing 200 coated safflower seeds with sand, uniformly sowing the seeds in a sample prescription (1m multiplied by 1m), covering sand by about 1-2 cm, watering a proper amount, regarding the seeds as seedling emergence when three leaves grow, counting the rate of emergence, and measuring the main root length, the root thickness, the side root number and the bud head number after 60 days of seedling emergence; wherein the coated safflower seeds are obtained by adopting the coating method of any one of embodiments 1 to 5; uncoated safflower seeds were used as controls, and each set of experiments was repeated five times; the experimental results are shown in table 3 below. Wherein, the plot of the field experiment results of the safflower seeds before and after coating of example 3 is shown in fig. 4, fig. 4 is the plot of the field experiment detection results of the safflower seeds before and after coating of example 3 according to the present invention, wherein a is the plot of the results of the field experiment of the uncoated safflower seeds, and b is the plot of the results of the field experiment of the coated safflower seeds.
TABLE 3 detection results of safflower seeds before and after coating in field experiment
Figure BDA0003052841780000071
As can be seen from the results in Table 3, when the safflower seeds are coated by adopting the safflower seed coating agent and the coating method thereof, the emergence rate of the safflower seeds is improved by 2-9 percentage points, the main root length is increased by 0.6-2.8 cm, the root thickness is increased by 0.58-2.25 mm, the stem thickness is increased by 0.25-1.56 mm, the bud number is increased by 1-2, the problems of withered and yellow safflower seedlings, damage to growing points and the like are relieved, the emergence rate of the safflower is effectively improved, and the robust growth of safflower roots and the synthesis of biomass are promoted.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; and such modifications or substitutions do not depart from the spirit and scope of the corresponding technical solutions of the embodiments of the present invention.

Claims (7)

1. The safflower seed coating is characterized by comprising the following raw materials in percentage by mass:
2.09-3.48 percent of thiabendazole, 0.27-0.45 percent of metalaxyl-M, 0.35-0.58 percent of fludioxonil, 3 percent of thiamethoxam, 3 percent of agricultural emulsion 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose, 4 percent of glycol and the balance of purified water.
2. A coating method of a safflower seed coating agent is characterized by comprising the following steps:
s1, preparing the safflower seed coating agent of claim 1;
s2, mixing the seed coating agent and safflower seeds, stirring evenly, and drying in the air to finish the coating of the safflower seeds.
3. The coating process according to claim 2, characterized in that: in step S2, the drug seed ratio of the safflower seed coating to the licorice seed is 1 mL: 130-220 g.
4. The coating process according to claim 2, characterized in that: the safflower seed coating agent comprises the following raw materials in percentage by mass: 3.48% of thiabendazole, 0.45% of metalaxyl-M, 0.58% of fludioxonil, 3% of thiamethoxam, 3% of agricultural milk 700, 0.3% of xanthan gum, 0.2% of sodium carboxymethylcellulose, 4% of ethylene glycol and the balance of purified water.
5. The coating method according to claim 4, wherein: the medicine seed ratio of the safflower seed coating agent to the safflower seeds is 1 mL: 220g of the total weight of the powder.
6. The use of the safflower seed coating of claim 1, wherein said use is in seed seedling.
7. The use of the coating method according to any one of claims 2 to 5, wherein the coating method can be used for raising seedlings of safflower seeds.
CN202110492165.5A 2021-05-06 2021-05-06 Safflower seed coating agent, coating method and application thereof Pending CN113287617A (en)

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Application publication date: 20210824