CN105625037B - A kind of smooth, soft technique of cottonette - Google Patents
A kind of smooth, soft technique of cottonette Download PDFInfo
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- CN105625037B CN105625037B CN201610171671.3A CN201610171671A CN105625037B CN 105625037 B CN105625037 B CN 105625037B CN 201610171671 A CN201610171671 A CN 201610171671A CN 105625037 B CN105625037 B CN 105625037B
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- cottonette
- smooth
- soft
- polyacrylic acid
- fat liquor
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/02—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements ultrasonic or sonic; Corona discharge
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a kind of smooth, soft technique of cottonette.The smooth, soft technique comprises the following steps:S1, cottonette is placed in the environment that temperature is 50 DEG C~65 DEG C and be ultrasonically treated;S2, the cottonette after ultrasound in the step S1 is impregnated in the mixed liquor of polyacrylic acid fat liquor and bleeding agent to progress smooth, soft arrangement.The scale of wool surface is come off by being ultrasonically treated, improve the softness of wool fiber itself, be beneficial to polyacrylic acid fat liquor again and bleeding agent is entered inside wool fiber, improve its softness;Being ultrasonically treated simultaneously can also make cottonette surface the hole being randomly distributed occur, add cottonette and polyacrylic acid fat liquor and the combination degree of bleeding agent, improve the softness and washing fastness of cottonette, obtained cottonette, there is the characteristics of washing fastness is high, smooth, soft is good, attractive in appearance and comfortableness is good.
Description
Technical field
The invention belongs to cottonette technical field, and in particular to a kind of smooth, soft work of cottonette
Skill.
Background technology
Wool fiber enjoys consumer to like with its excellent comfortableness and good dyeability, but because it is produced into
This is higher, and blending is carried out frequently with wool fiber and other textile fabrics.Because cotton fiber equally there is preferable moisture absorption to lead sweat
Performance and more complete chromatogram, so as to as the more suitable fibrous material with wool fiber progress blending.Due to cotton wool
Blend fabric feel after multiple working process is hardened, and smoothness declines, and influences the attractive in appearance and comfortableness of fabric, and passes through flat
The defects of cottonette after sliding soft treatment greatly improves cotton wool fabric, improve the wearability of fabric.
At present, most of fluent movement to cottonette is impregnated using organosilicon or continuously pads work more
Skill, but the defects of certain be present in the cottonette washing fastness through the PROCESS FOR TREATMENT.Such as:Chinese patent literature CN
104358134 A disclose a kind of method of wool fabric fluent movement, and its step is as follows:By wool fabric according to bath raio 1:15
~25 immerse in 2~5%owf hydroxy-silicone-oil emulsion, and it is 4~6 to add acetic acid adjustment pH value, adds 2~4%owf infiltration
Agent, 20~40min is impregnated at 30~40 DEG C, 3~5min is dried at 80~100 DEG C, bake 3 then at 120~140 DEG C~
5min。
In above-mentioned patent document, directly wool fabric is immersed in hydroxy-silicone-oil emulsion and bleeding agent, but wool table
Face can have scale, hydroxy-silicone-oil emulsion and bleeding agent is difficult to enter into inside wool, cause most hydroxy silicon oil breasts
Liquid and bleeding agent only reside within wool fabric surface, and it is poor to ultimately result in fluent movement effect.
The content of the invention
Cottonette feel after multiple working process is hardened it is an object of the invention to solving in the prior art,
The technical problem that smoothness declines, and then provide a kind of the smooth of the cottonette that washing fastness is high, smooth, soft is good
Soft technique.
Therefore, the technical solution adopted by the present invention is,
A kind of smooth, soft technique of cottonette, comprises the following steps:
S1, cottonette is placed in the environment that temperature is 50 DEG C~65 DEG C and be ultrasonically treated;
S2, the cottonette after ultrasound in the step S1 is impregnated in the mixed of polyacrylic acid fat liquor and bleeding agent
Close and smooth, soft arrangement is carried out in liquid.
The step S2 includes:S21, the cottonette after ultrasound is impregnated in polyacrylic acid fat liquor;S22、
Organic acid for adjusting pH value is added in the polyacrylic acid fat liquor as 4.0~6.0;S23, add bleeding agent and stir.
In the step S2, the concentration of the polyacrylic acid fat liquor is 4o.w.f%-7o.w.f%, the bleeding agent
Concentration is 4g/L-6g/L.
The organic acid is acetic acid.
In the step S2, the bath raio 1 of the dried cottonette and the polyacrylic acid fat liquor:(20
~30).
In the step S2, the temperature that the smooth, soft arranges is 35 DEG C -45 DEG C, according to being actually needed, can be selected
The time that the smooth, soft arranges, e.g., 0.75h~1h can be selected.
Before the step S2, in addition to the cottonette after ultrasound in the step S1 is carried out to dry for the first time
The step of, drying temperature is 80 DEG C~100 DEG C, and is dried to constant weight.
In the step S1, the ultrasonic power of the ultrasonic step is 200W-250W;After the step S2, in addition to
Second of drying steps is carried out to the cottonette after dipping.
Further, second of dry step is as follows:By the cottonette after dipping prior to 85 DEG C~95
4min-6min is dried at DEG C, is dried at 104 DEG C -106 DEG C to constant weight.
The bleeding agent is JFC bleeding agents (AEO).
Present invention also offers the cottonette as made from above-mentioned smooth, soft technique.
Compared with prior art, the present invention has the advantages that:
1) the smooth, soft technique for the cottonette that the embodiment of the present invention is provided, by the way that cottonette is put
It is ultrasonically treated in the environment that temperature is 50 DEG C~65 DEG C, the scale of wool surface is come off by being ultrasonically treated, that is, carry
The high softness of wool fiber itself, the polyacrylic acid fat liquor and bleeding agent being beneficial to again in subsequent handling enter wool
Fibrous inside, improve its softness;The cotton fiber and wool surface of cottonette can also be made by being ultrasonically treated simultaneously
There is the hole being randomly distributed, add cottonette and the combination journey of follow-up polyacrylic acid fat liquor and bleeding agent
Degree, improves the softness of cottonette, also improves cottonette washing fastness, by smooth, soft technique
Front and rear cottonette is arranged to be tested, find the cottonette after arranging static friction angle, creasy recovery angle,
Be superior in terms of stiffness and feel it is unfinished, even if after washing 50 times, still better than unfinished;Polyacrylic acid is used again
Fat liquor and bleeding agent, with reference to above-mentioned supersound process, finally give the llama that washing fastness is high, smooth, soft is good and knit
Thing.
2) the smooth, soft technique for the cottonette that the embodiment of the present invention is provided, by by the ultrasound of ultrasonic step
Power setting is 200W-250W, you can the scale of wool surface is come off, the cotton fiber of cottonette and wool it is fine
There is the hole being randomly distributed in dimension table face, while also avoids ultrasonic power excessive, is broken cottonette.
3) the smooth, soft technique for the cottonette that the embodiment of the present invention is provided, by the way that the cotton wool after ultrasound is mixed
Yarn fabric is impregnated in polyacrylic acid fat liquor;Added in the polyacrylic acid fat liquor organic acid for adjusting pH value for 4.0~
6.0;Add bleeding agent and stir, polyacrylic acid fat liquor and bleeding agent is given full play to each self-applying, improve llama and knit
Washing fastness, the smooth, soft of thing.
4) cottonette as made from above-mentioned smooth, soft technique that the embodiment of the present invention is provided, there is washing jail
The characteristics of degree is high, smooth, soft is good, attractive in appearance and comfortableness is good.
Embodiment
In order to which the object, technical solutions and advantages of the present invention are better described, below in conjunction with specific embodiment to this hair
It is bright to be described further.The present invention can be embodied in many different forms, and should not be construed as limited to set forth herein
Embodiment.Conversely, there is provided these embodiments so that the disclosure will be thorough and complete, and the design of the present invention will be filled
Divide and be communicated to those skilled in the art, the present invention will only be defined by the appended claims.
Bleeding agent in the application is workable all bleeding agents when handling fabric at present, for ease of describing, the application
Bleeding agent marque used in following each embodiments and comparative example is penetrating agent JFC, purchased from Jiangsu Province Hai'an petrochemical industry
Factory;Cottonette used is (longitude and latitude yarn count is 32s, longitude and latitude is 482/10cm, and 368/10cm, laboratory is certainly
Row weaving);
Embodiment 1
The present embodiment provides a kind of cottonette and its smooth, soft technique, and it comprises the following steps:
S1, cottonette is placed in the environment that temperature is 50 DEG C, ultrasonic power is 250W it is ultrasonically treated 0.5h;
S2, the cottonette after ultrasound in step S1 is dried to constant weight at 80 DEG C, dried cotton wool is mixed
Yarn fabric presses bath raio 1:20 are impregnated in the polyacrylic acid fat liquor that concentration is 4o.w.f%;And add in polyacrylic acid fat liquor
Enter second acid for adjusting pH value for 6.0;Add the JFC bleeding agents that concentration is 4g/L and stir, by cottonette at 35 DEG C
Smooth, soft handles 1h, and 5min is finally dried at 85 DEG C, is dried at 105 DEG C to constant weight, after obtaining smooth, soft processing
Cottonette.
Embodiment 2
The present embodiment provides a kind of cottonette and its smooth, soft technique, and it comprises the following steps:
S1, cottonette is placed in the environment that temperature is 65 DEG C, ultrasonic power is 200W it is ultrasonically treated 0.5h;
S2, the cottonette after ultrasound in step S1 is dried to constant weight at 100 DEG C, dried cotton wool is mixed
Yarn fabric presses bath raio 1:30 are impregnated in the polyacrylic acid fat liquor that concentration is 7o.w.f%;And add in polyacrylic acid fat liquor
Enter second acid for adjusting pH value for 4.0;Add the JFC bleeding agents that concentration is 5g/L and stir, by cottonette at 45 DEG C
Smooth, soft handles 0.75h, and 5min is finally dried at 95 DEG C, is dried at 106 DEG C to constant weight, obtains smooth, soft processing
Cottonette afterwards.
Embodiment 3
The present embodiment provides a kind of cottonette and its smooth, soft technique, and it comprises the following steps:
S1, cottonette is placed in the environment that temperature is 58 DEG C, ultrasonic power is 225W it is ultrasonically treated 0.5h;
S2, the cottonette after ultrasound in step S1 is dried to constant weight at 90 DEG C, dried cotton wool is mixed
Yarn fabric presses bath raio 1:25 are impregnated in the polyacrylic acid fat liquor that concentration is 5.5o.w.f%;And in polyacrylic acid fat liquor
It is 5.0 to add second acid for adjusting pH value;Add the JFC bleeding agents that concentration is 6g/L and stir, by cottonette at 40 DEG C
Lower smooth, soft handles 0.85h, and 5min is finally dried at 90 DEG C, dries to constant weight, is obtained at smooth, soft at 104 DEG C
Cottonette after reason.
Comparative example 1
This comparative example provides a kind of cottonette and its smooth, soft technique, and it comprises the following steps:
Cottonette is pressed into bath raio 1:20 are impregnated in the polyacrylic acid fat liquor that concentration is 4o.w.f%;And poly-
It is 6.0 that second acid for adjusting pH value is added in acrylate emulsion;Add the JFC bleeding agents that concentration is 4g/L and stir, by cotton wool
Blend fabric smooth, soft at 35 DEG C handles 1h, and 5min is finally dried at 85 DEG C, dries to constant weight, obtains at 105 DEG C
Cottonette to after smooth, soft processing.
Comparative example 2
This comparative example provides a kind of cottonette and its smooth, soft technique, and it comprises the following steps:
S1, cottonette is placed in the environment that temperature is 30 DEG C, ultrasonic power is 250W it is ultrasonically treated 0.5h;
S2, the cottonette after ultrasound in step S1 is dried to constant weight at 100 DEG C, dried cotton wool is mixed
Yarn fabric presses bath raio 1:30 are impregnated in the polyacrylic acid fat liquor that concentration is 7o.w.f%;And add in polyacrylic acid fat liquor
Enter second acid for adjusting pH value for 4.0;Add the JFC bleeding agents that concentration is 5g/L and stir, by cottonette at 45 DEG C
Smooth, soft handles 0.75h, and 5min is finally dried at 95 DEG C, is dried at 106 DEG C to constant weight, obtains smooth, soft processing
Cottonette afterwards.
Comparative example 3
This comparative example provides a kind of cottonette and its smooth, soft technique, and it comprises the following steps:
S1, cottonette is placed in the environment that temperature is 80 DEG C, ultrasonic power is 200W it is ultrasonically treated 0.5h;
S2, the cottonette after ultrasound in step S1 is dried to constant weight at 100 DEG C, dried cotton wool is mixed
Yarn fabric presses bath raio 1:30 are impregnated in the polyacrylic acid fat liquor that concentration is 7o.w.f%;And add in polyacrylic acid fat liquor
Enter second acid for adjusting pH value for 4.0;Add the JFC bleeding agents that concentration is 5g/L and stir, by cottonette at 45 DEG C
Smooth, soft handles 0.75h, and 5min is finally dried at 95 DEG C, is dried at 106 DEG C to constant weight, obtains smooth, soft processing
Cottonette afterwards.
Comparative example 4
This comparative example provides a kind of cottonette and its smooth, soft technique, and it comprises the following steps:
S1, cottonette is placed in the environment that temperature is 58 DEG C, ultrasonic power is 225W it is ultrasonically treated 0.5h;
S2, the cottonette after ultrasound in step S1 is dried to constant weight at 90 DEG C, dried cotton wool is mixed
Yarn fabric presses bath raio 1:25 are impregnated in the polyacrylic acid fat liquor that concentration is 5.5o.w.f%;And in polyacrylic acid fat liquor
It is 5.0 to add second acid for adjusting pH value;Add the JFC bleeding agents that concentration is 6g/L and stir, by cottonette at 60 DEG C
Lower smooth, soft handles 0.85h, and 5min is finally dried at 90 DEG C, dries to constant weight, is obtained at smooth, soft at 104 DEG C
Cottonette after reason.
Following each performance tests are carried out to above-mentioned each embodiment and comparative example:
Static friction angle is tested:With reference to FZT 40001-1992《Silk fabrics smoothness test method inclined-plane sliding scale》;Wrinkle
Recovery angle is tested:National standard:GB/T3819-1997《The measure of textile -- fabric folds recovery replys horn cupping》;It is stiffening
Degree test:National standard ZB W04003《Fabric stiffness test method inclined-plane cantilever method》;Feel is tested:AATCCEP52007
Fabric feeling;Washing:It is 1% that cottonette after arrangement, which is launched in mass fraction, and temperature is to enter in 20 DEG C of soap lye
The capable 10min that soaps, bath raio 1:20, the cottonette after soaping is placed into after temperature is dried to constant weight for 105 DEG C again
It is secondary to soap, until 50 times.
Shown in the following Tables 1 and 2 of corresponding test data:
Table 1, cottonette smooth, soft before and after fabric property contrast
Cottonette after table 2, smooth, soft wash 50 times after fabric property
It can be learnt from table 1:Smooth, the soft and feel of embodiment cottonette is above comparative example, illustrates smooth
Soft technique can play good smooth, soft effect to cottonette.
It can be learnt from table 2:The washing fastness of embodiment cottonette is above comparative example, illustrates smooth, soft work
Enough arranged to cottonette smooth, soft of artistic skill can keep good washing fastness.
Obviously, above-described embodiment is only intended to clearly illustrate example, and is not the restriction to embodiment.It is right
For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of change or
Change.There is no necessity and possibility to exhaust all the enbodiments.And the obvious change thus extended out or
Among changing still in the protection domain of the invention.
Claims (9)
1. a kind of smooth, soft technique of cottonette, comprises the following steps:
S1, cottonette is placed in the environment that temperature is 50 DEG C ~ 65 DEG C and be ultrasonically treated, the ultrasonic work(of the ultrasonic step
Rate is 200w-250w;
S2, the mixed liquor that the cottonette after ultrasound in the step S1 is impregnated in polyacrylic acid fat liquor and bleeding agent
Middle progress smooth, soft arrangement, the concentration of the polyacrylic acid fat liquor is 4 o.w.f %-7o.w.f %, the bleeding agent
Concentration is 4 g/L-6 g/L.
2. smooth, soft technique according to claim 1, it is characterised in that the step S2 includes:
S21, the cottonette after ultrasound is impregnated in polyacrylic acid fat liquor;
S22, organic acid for adjusting pH value is added as 4.0~6.0 in the polyacrylic acid fat liquor;
S23, add bleeding agent and stir.
3. smooth, soft technique according to claim 2, it is characterised in that the organic acid is acetic acid.
4. smooth, soft technique according to claim 1 or 2, it is characterised in that before the step S2, in addition to institute
The step that the cottonette in step S1 after ultrasound dry for the first time is stated, drying temperature is 80 DEG C ~ 100 DEG C, and is done
It is dry to constant weight.
5. smooth, soft technique according to claim 4, it is characterised in that in the step S2, the first time is dried
The bath raio 1 of cottonette afterwards and the polyacrylic acid fat liquor:(20~30).
6. smooth, soft technique according to claim 1 or 2, it is characterised in that in the step S2, the smooth, soft
The temperature of arrangement is 35 DEG C -45 DEG C.
7. smooth, soft technique according to claim 4, it is characterised in that after the step S2, in addition to dipping
Cottonette afterwards carries out second of drying steps.
8. smooth, soft technique according to claim 7, it is characterised in that second of dry step is as follows:Will
Cottonette after dipping prior to 85 DEG C ~ 95 DEG C at dry 4min-6min, dried at 104 DEG C -106 DEG C to perseverance
Weight.
9. cottonette made from the smooth, soft technique any one of a kind of claim 1-8.
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