CN104179312A - Thermo-sensitive color-changing rich-mineral-paper-based fireproof flame-retardant wallpaper and preparation method thereof - Google Patents
Thermo-sensitive color-changing rich-mineral-paper-based fireproof flame-retardant wallpaper and preparation method thereof Download PDFInfo
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- CN104179312A CN104179312A CN201410341992.4A CN201410341992A CN104179312A CN 104179312 A CN104179312 A CN 104179312A CN 201410341992 A CN201410341992 A CN 201410341992A CN 104179312 A CN104179312 A CN 104179312A
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Abstract
A piece of thermo-sensitive color-changing rich-mineral-paper-based fireproof flame-retardant wallpaper comprises a rich mineral paper base material layer, a flame-retardant coating layer and a color-changing printing decoration layer, wherein the flame-retardant coating layer is laid on the upper surface of the rich mineral paper base material layer, and the color-changing printing decoration layer is laid on the upper surface of the flame-retardant coating layer. The wallpaper takes a piece of inorganic powder highly-filled mineral paper as a paper base material and has certain fireproof and flame-retardant functions, combustion tests are performed according to GB8624-2006, and the fire rating reaches the B-s1, d0, t0 grade. The wallpaper is simple in production technology, the environmental pollution is avoided, a large number of petroleum resources and forest resources are saved, the cost is low, the safety guarantee coefficient is greatly increased, and meanwhile, the harm caused by toxic and harmful substances such as dioxin, hydrogen chloride and the like to the human health is completely eradicated. Thermo-sensitive color-changing slurry is used, so that the wallpaper can change into different colors at different temperatures, has the characteristic of personalization and integrates personalization, art and functionalization.
Description
Technical field
The present invention relates to functional technical field of construction and decoration materials, particularly relate to a kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper and preparation method thereof.
Background technology
Wallpaper claims again wallpaper, is a kind of application indoor hardware fitting quite widely.Originate from Britain, occur that since generation nineteen fifty PVC wallpaper, wallpaper start universal the coming in the whole world.Wallpaper approaches 100% in Japan, the civilian popularity rate of Russia at present, also has the popularity rate of 50%-60% in American-European countries.The form of expression of wallpaper is very abundant, and for adapting to different spaces or place, different hobby, different functional requirement and different price levels, wallpaper also has polytype for you to choose.
At present popular main wallpaper type has PVC plastic wallpaper, full paper wallpaper, non-woven paper wallpaper, natural fabric wallpaper and some to have the novel wallpaper of specific function.Wherein PVC plastic wallpaper is the one of wallpaper market share amount maximum, accounts for 95% left and right of the total market size.PVC plastic wallpaper, due to a large amount of petrochemical industry raw material such as polyvinyl chloride that use, very easily burns in the time of house breaking out of fire, discharges a large amount of poisonous and harmful smog such as bioxin, hydrogen chloride, brings huge hidden danger to resident's safety of life and property.The fireproof flame-retardation wallpaper the present invention relates to, adopts the high filling mineral paper of inorganic particle (stone paper) as paper base material.Its manufacturing process is pollution-free, technique is simple, carries out combustion testing according to GB 8624-2006, and fire-protection rating reaches B-s1, d0, and t0 level, has increased the safety factor using greatly.The wallpaper that at present also has some to have fire protection flame retarding function, relates generally to traditional wallpaper field, and its manufacture method remains in complex process, the shortcoming such as cost of production is higher, safety factor is low.
Along with improving constantly of socioeconomic high speed development and living standard, people pursue attractive in appearance in, be more tending towards focusing on the diversity, functional and personalized of wall paper.Temperature sensitive type variable color wallpaper, by personalized and art up design, utilizes the variation of environment temperature to give wallpaper turn colors, has realized the function that uses a wallpaper to have multiple decorative effect.This wallpaper can be realized the conversion of color under different indoor or environment temperatures, when interior temperature is a kind of colour match and pattern during lower than certain value, in the time that raising, temperature presents another kind of colour match and pattern, art up and personalization are combined together, allow people obtain aesthetic experience and happy sensation, allow the dwelling environment be full of intention and charm, met people and pursue the home decoration theory of warmth, individual character and intention.
Summary of the invention
The object of this invention is to provide a kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper that shows different colours effect under different temperatures and preparation method thereof.
The technical scheme adopting is:
A kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper, comprises stone paper substrate layer, fire-retardant coating layer and variable color printed decoration layer.Described stone paper substrate layer upper surface is equipped with fire-retardant coating layer, and fire-retardant coating layer upper surface is laid variable color printed decoration layer.
Above-mentioned stone paper substrate layer adopts the high filling mineral stone paper of inorganic particle substrate layer, and its prescription quality percentage is configured to:
Inorganic mineral powder: 70-83%
Polyvinyl resin: 15-30%
Each analog assistant: account for inorganic mineral powder 2-5%
Described inorganic mineral powder comprises one or more in powdered whiting, French chalk, flyash, calcium silicate powder, titanium dioxide, titanium dioxide, clay, mica, wollastonite in powder;
Described each analog assistant comprises coupling agent, dispersing agent, sliding agent, antioxidant, flexibilizer.
Inorganic particle in above-mentioned fire-retardant coating layer is kaolin or precipitated calcium carbonate or kieselguhr or titanium dioxide.Fire retardant is tetrabromobisphenol,, decabromodiphenyl oxide and antimony oxide.
Above-mentioned variable color printed decoration layer consists of cylinder press printing temperature sensing color changing slurry on fire-retardant coating layer, the printing ink that temperature sensing color changing slurry is is 10-22:1 by mass ratio: temperature sensing color changing powder forms.
The discoloring temperature of described temperature sensing color changing powder, between 18-40 DEG C, can be changed into redness, yellow, blueness.
A preparation method for temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper, comprises the following steps:
(1) first prepare the high filling mineral stone paper of inorganic particle, the above-mentioned inorganic particle of 70-83% is joined in high-speed mixer, be heated to 120-130 DEG C, survey after hydration lattice, add again coupling agent, dispersing agent activates dispersion treatment, temperature is controlled at 110 DEG C ± 5 DEG C, processing time is 15-22 minute, add again polyvinyl resin and other auxiliary agents of 15-30%, mix and take the dish out of the pot after 7 minutes, then drop in banbury, heating-up temperature is 90-190 DEG C, rotor speed is turn/min of 20-40, stand up exhaust 2-5 time, the banburying time is 12-18 minute, then be transported in the single screw extrusion machine that draw ratio is 20:1, heating-up temperature is 140-165 DEG C, screw speed is turn/min of 20-40, the speed of double-cone feeding is turn/min of 10-20, obtain stone paper pellet,
(2) stone paper pellet is joined in three-layer co-extruded blown film unit, heating-up temperature is 160-195 DEG C, the paper base material that T-shaped mould is extruded carries out through corona treatment the surface tension that sided corona treatment improves goods again and improves printing performance after traction sizing, and rolling obtains stone paper wallpaper base material through cutting edge again;
(3) utilize coating machine, fire-retardant coating layer is laid on stone paper wallpaper base material.Coating machine transmission speed is 20-50m/min, applies anti-flaming dope, then be dried through drying tunnel through anilox roll and anilox roller, and bake out temperature is 70-100 DEG C, and spread is 25-35g/m
2;
(4) utilize cylinder printing machine or ink-jet printer, temperature sensing color changing printed decoration slurry is coated in fire-retardant printed layers, described cylinder printing machine transmission speed is 10-50m/min, cylinder scraper pressure is 0.1-1.5Mpa, the angle of scraper is 60 °-100 °, then traction enters baking oven, at the temperature of 60-100 DEG C, dries; Described ink-jet printer, unwinding tension 30-50Mpa, unreels speed 10-40m/h, through two-way 4-12pas inkjet printing, baking and curing color at the temperature of 50-90 DEG C.Last rolling obtains temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper.
Feature of the present invention is: adopting the high filling mineral paper of inorganic particle is paper base material, because inorganic powder filled amount is high, paper base material has had certain fire protection flame retarding function, utilize anti-flaming dope, more ensured the fire protection flame retarding ability of this wallpaper, carried out combustion testing according to GB 8624-2006, fire-protection rating reaches B-s1, d0, t0 level.Production technology of the present invention is simple, free from environmental pollution, has saved a large amount of petroleum resources and the forest reserves, with low cost, has greatly improved safety guarantee coefficient, has stopped the injury of the venomous injurant such as bioxin, hydrogen chloride confrontation health simultaneously.By using temperature sensing color changing slurry, make wallpaper under different temperatures can change different colors, to give this wallpaper and there is personalized feature, union personalization, art up, functionalization are.
Brief description of the drawings
Fig. 1 is wallpaper structural representation of the present invention.
In figure: 1, stone paper substrate layer; 2, fire-retardant coating layer; 3, variable color printed decoration layer.
Detailed description of the invention
Embodiment mono-
(1) first prepare the high filling mineral stone paper of inorganic particle, 70% above-mentioned inorganic particle is joined in high-speed mixer, be heated to 120 DEG C, survey after hydration lattice, add again coupling agent, dispersing agent activates dispersion treatment, temperature is controlled at 110 DEG C ± 5 DEG C, processing time is 15 minutes, add again 30% polyvinyl resin and other auxiliary agents, mix and take the dish out of the pot after 7 minutes, then drop in banbury, heating-up temperature is 90 DEG C, rotor speed is 20 turn/min, stand up exhaust 2 times, the banburying time is 12 minutes, then be transported in the single screw extrusion machine that draw ratio is 20:1, heating-up temperature is 140 DEG C, screw speed is 20 turn/min, the speed of double-cone feeding is 10 turn/min, obtain stone paper pellet,
(2) stone paper pellet is joined in three-layer co-extruded blown film unit, heating-up temperature is
160 DEG C, the paper base material that T-shaped mould is extruded carries out through corona treatment the surface tension that sided corona treatment improves goods again and improves printing performance after traction sizing, and rolling obtains stone paper wallpaper base material through cutting edge again;
(3) utilize coating machine, fire-retardant coating layer is laid on paper base material.Coating machine transmission speed is 20m/min, applies anti-flaming dope, then be dried through drying tunnel through anilox roll and anilox roller, and bake out temperature is 70 DEG C, and spread is 25g/m
2;
(4) utilize cylinder printing machine or ink-jet printer, temperature sensing color changing printed decoration slurry is coated in fire-retardant printed layers, described cylinder printing machine transmission speed is 10m/min, cylinder scraper pressure is 0.1Mpa, the angle of scraper is 60 °, then traction enters baking oven, at the temperature of 60 DEG C, dries; Described ink-jet printer, unwinding tension 30Mpa, unreels speed 10m/h, through two-way 4-12pas inkjet printing, baking and curing color at the temperature of 50 DEG C.Last rolling obtains temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper.
Embodiment bis-
(1) first prepare the high filling mineral stone paper of inorganic particle, 83% above-mentioned inorganic particle is joined in high-speed mixer, be heated to 130 DEG C, survey after hydration lattice, add again coupling agent, dispersing agent activates dispersion treatment, temperature is controlled at 110 DEG C ± 5 DEG C, processing time is 22 minutes, add again 15% polyvinyl resin and other auxiliary agents, mix and take the dish out of the pot after 7 minutes, then drop in banbury, heating-up temperature is 190 DEG C, rotor speed is 40 turn/min, stand up exhaust 5 times, the banburying time is 18 minutes, then be transported in the single screw extrusion machine that draw ratio is 20:1, heating-up temperature is 165 DEG C, screw speed is 40 turn/min, the speed of double-cone feeding is 20 turn/min, obtain stone paper pellet,
(2) stone paper pellet is joined in three-layer co-extruded blown film unit, heating-up temperature is
195 DEG C, the paper base material that T-shaped mould is extruded carries out through corona treatment the surface tension that sided corona treatment improves goods again and improves printing performance after traction sizing, and rolling obtains stone paper wallpaper base material through cutting edge again;
(3) utilize coating machine, fire-retardant coating layer is laid on stone paper wallpaper base material.Coating machine transmission speed is 50m/min, applies anti-flaming dope, then be dried through drying tunnel through anilox roll and anilox roller, and bake out temperature is 100 DEG C, and spread is 35g/m
2;
(4) utilize cylinder printing machine or ink-jet printer, temperature sensing color changing printed decoration slurry is coated in fire-retardant printed layers, described cylinder printing machine transmission speed is 50m/min, cylinder scraper pressure is 1.5Mpa, the angle of scraper is 100 °, then traction enters baking oven, at the temperature of 100 DEG C, dries; Described ink-jet printer, unwinding tension 50Mpa, unreels speed 40m/h, through two-way 4-12pas inkjet printing, baking and curing color at the temperature of 90 DEG C.Last rolling obtains temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper.
Embodiment tri-
(1) first prepare the high filling mineral stone paper of inorganic particle, 80% above-mentioned inorganic particle is joined in high-speed mixer, be heated to 125 DEG C, survey after hydration lattice, add again coupling agent, dispersing agent activates dispersion treatment, temperature is controlled at 110 DEG C ± 5 DEG C, processing time is 20 minutes, add again 20% polyvinyl resin and other auxiliary agents, mix and take the dish out of the pot after 7 minutes, then drop in banbury, heating-up temperature is 150 DEG C, rotor speed is 30 turn/min, stand up exhaust 4 times, the banburying time is 15 minutes, then be transported in the single screw extrusion machine that draw ratio is 20:1, heating-up temperature is 150 DEG C, screw speed is 30 turn/min, the speed of double-cone feeding is 15 turn/min, obtain stone paper pellet,
(2) stone paper pellet is joined in three-layer co-extruded blown film unit, heating-up temperature is
180 DEG C, the paper base material that T-shaped mould is extruded carries out through corona treatment the surface tension that sided corona treatment improves goods again and improves printing performance after traction sizing, and rolling obtains stone paper wallpaper base material through cutting edge again;
(3) utilize coating machine, fire-retardant coating layer is laid on stone paper wallpaper base material.Coating machine transmission speed is 40m/min, applies anti-flaming dope, then be dried through drying tunnel through anilox roll and anilox roller, and bake out temperature is 90 DEG C, and spread is 30g/m
2;
(4) utilize cylinder printing machine or ink-jet printer, temperature sensing color changing printed decoration slurry is coated in fire-retardant printed layers, described cylinder printing machine transmission speed is 30m/min, cylinder scraper pressure is 1.1Mpa, the angle of scraper is 80 °, then traction enters baking oven, at the temperature of 80 DEG C, dries; Described ink-jet printer, unwinding tension 40Mpa, unreels speed 30m/h, through two-way 4-12pas inkjet printing, baking and curing color at the temperature of 70 DEG C.Last rolling obtains temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper.
Claims (8)
1. a temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper, comprise stone paper substrate layer (1), fire-retardant coating layer (2) and variable color printed decoration layer (3), it is characterized in that described stone paper substrate layer (1) upper surface is equipped with fire-retardant coating layer (2), fire-retardant coating layer (2) upper surface is laid variable color printed decoration layer (3).
2. a kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper according to claim 1, is characterized in that described stone paper substrate layer (1) adopts the high filling mineral stone paper of inorganic particle substrate layer, and its prescription quality percentage is configured to:
Inorganic mineral powder: 70-83%
Polyvinyl resin: 15-30%
Each analog assistant: account for inorganic mineral powder 2-5%.
3. a kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper according to claim 2, is characterized in that described inorganic mineral powder comprises one or more in powdered whiting, French chalk, flyash, calcium silicate powder, titanium dioxide, titanium dioxide, clay, mica, wollastonite in powder.
4. a kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper according to claim 2, is characterized in that described each analog assistant comprises coupling agent, dispersing agent, sliding agent, antioxidant, flexibilizer.
5. a kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper according to claim 1, is characterized in that the inorganic particle in described fire-retardant coating layer (2) is kaolin or precipitated calcium carbonate or kieselguhr or titanium dioxide; Fire retardant is tetrabromobisphenol,, decabromodiphenyl oxide or antimony oxide.
6. a kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper according to claim 1, it is characterized in that described variable color printed decoration layer (3), on fire-retardant coating layer, formed the printing ink that temperature sensing color changing slurry is is 10-22:1 by mass ratio by cylinder press printing by temperature sensing color changing slurry: temperature sensing color changing powder forms.
7. a kind of temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper according to claim 6, is characterized in that the discoloring temperature of described temperature sensing color changing powder, between 18-40 DEG C, can be changed into redness, yellow, blueness.
8. a preparation method for temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper, is characterized in that comprising the following steps:
(1) first prepare the high filling mineral stone paper of inorganic particle, the above-mentioned inorganic particle of 70-83% is joined in high-speed mixer, be heated to 120-130 DEG C, survey after hydration lattice, add again coupling agent, dispersing agent activates dispersion treatment, temperature is controlled at 110 DEG C ± 5 DEG C, processing time is 15-22 minute, add again polyvinyl resin and other auxiliary agents of 15-30%, mix and take the dish out of the pot after 7 minutes, then drop in banbury, heating-up temperature is 90-190 DEG C, rotor speed is turn/min of 20-40, stand up exhaust 2-5 time, the banburying time is 12-18 minute, then be transported in the single screw extrusion machine that draw ratio is 20:1, heating-up temperature is 140-165 DEG C, screw speed is turn/min of 20-40, the speed of double-cone feeding is turn/min of 10-20, obtain stone paper pellet,
(2) stone paper pellet is joined in three-layer co-extruded blown film unit, heating-up temperature is 160-195 DEG C, the paper base material that T-shaped mould is extruded carries out through corona treatment the surface tension that sided corona treatment improves goods again and improves printing performance after traction sizing, and rolling obtains stone paper wallpaper base material through cutting edge again;
(3) utilize coating machine, fire-retardant coating layer is laid on stone paper wallpaper base material, coating machine transmission speed is 20-50m/min, apply anti-flaming dope through anilox roll and anilox roller, be dried through drying tunnel, bake out temperature is 70-100 DEG C again, and spread is 25-35g/m
2;
(4) utilize cylinder printing machine or ink-jet printer, temperature sensing color changing printed decoration slurry is coated in fire-retardant printed layers, described cylinder printing machine transmission speed is 10-50m/min, cylinder scraper pressure is 0.1-1.5Mpa, the angle of scraper is 60 °-100 °, then traction enters baking oven, at the temperature of 60-100 DEG C, dries; Described ink-jet printer, unwinding tension 30-50Mpa, unreels speed 10-40m/h, through two-way 4-12pas inkjet printing, baking and curing color at the temperature of 50-90 DEG C, last rolling obtains temperature sensitive type variable color stone paper substrate fireproof flame-retardation wallpaper.
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Cited By (8)
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| CN105220576A (en) * | 2015-08-31 | 2016-01-06 | 刘惠强 | A kind of fire-retardant mica sheet wallpaper typography |
| CN105235406A (en) * | 2015-11-20 | 2016-01-13 | 浙江维涅斯装饰材料股份有限公司 | Rotary-screen printing process |
| CN105888171A (en) * | 2014-12-05 | 2016-08-24 | 遵义市美仑空间个性艺术装饰材料中心 | Functional wallpaper |
| CN106378999A (en) * | 2016-08-30 | 2017-02-08 | 桐乡嘉力丰实业股份有限公司 | Flame-retardant color-changing wall cloth |
| CN107031244A (en) * | 2016-11-03 | 2017-08-11 | 鸿圣（江西）彩印包装实业有限公司 | The preparation method of stone paper copybook |
| CN107386008A (en) * | 2017-07-27 | 2017-11-24 | 安徽宽居电器有限公司 | A kind of manufacturing process of Environment-friendlywallpaper wallpaper |
| CN108824070A (en) * | 2018-06-01 | 2018-11-16 | 合肥昂诺新材料有限公司 | A kind of cover paper and preparation method thereof with fire protection flame retarding function |
| CN110939014A (en) * | 2019-11-25 | 2020-03-31 | 浙江华丰纸业科技有限公司 | Printing colored cigarette paper and manufacturing method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108824070A (en) * | 2018-06-01 | 2018-11-16 | 合肥昂诺新材料有限公司 | A kind of cover paper and preparation method thereof with fire protection flame retarding function |
| CN110939014A (en) * | 2019-11-25 | 2020-03-31 | 浙江华丰纸业科技有限公司 | Printing colored cigarette paper and manufacturing method thereof |
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Application publication date: 20141203 |